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Prediction of batch heat transfer coefficients for pseudoplastic fluids ...

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'11<br />

The flow behavior index and fluid consistency index<br />

expressed i~ the proper units are given iE. Table A-8. The<br />

data are pletted in Figures A-4, A-5 and A-6.<br />

li~es<br />

The solid<br />

are the values <strong>for</strong> the shear stress calettlated using<br />

equations A-9 and A-IO with the constants in Table A-6 while<br />

the plotted points are the data from which the constants<br />

were es.leulated ..<br />

The effects <strong>of</strong> turbulence were noticed when measur~<br />

the 0.15% Carbopol at high speed. H.:noJever, these r'llE.S were<br />

then redone using a smaller diameter spindle as suggested<br />

in. Chapter 2.. . The data Has also che eked .<strong>for</strong> tem]5erature<br />

rise due to <strong>heat</strong> generation..<br />

The <strong>heat</strong> generated per unit<br />

vol~ can be calculated using equation 2-16.<br />

""""',..}J<br />

Heat Generation = / ~ (2-16<br />

The most viscous fluid at the highest shear rate generated<br />

8 .. 31 x 10- 5 cale/see.. A series <strong>of</strong> measurements at aay one<br />

tem.1gerature at any s]'ced took about five minutes at the<br />

longe s t. This amoUJ:71.ts to a maximum temperature rise <strong>of</strong><br />

0.025°0. which is negligible. Not only was this rise<br />

calculated on the basis <strong>of</strong> the conditions most prone to give<br />

I<br />

hi~~ rates <strong>of</strong> <strong>heat</strong> generation, but alsG the system was considered<br />

to be adiabatic, whiCh is untrue..<br />

did not influence the rheological :m.easurem.emts ..<br />

Thus, <strong>heat</strong> generation<br />

The torque required to rotat~<br />

the spindle at a constant

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