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Prediction of batch heat transfer coefficients for pseudoplastic fluids ...

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166<br />

rive different temperatures; about 17~<br />

25, 40, 60 and 82 °e.<br />

The fluid Has maintained at the desired temperature by<br />

iramersing the 600 ml ..<br />

beaker in a constant temperature<br />

bath..<br />

The constant temperature bath was placed on a magnetic<br />

stirrer (the stirring bar Has in the 600 ml.. beru-rer)<br />

which was run l'lhile bringing the fluid up to temperature,<br />

but Has shut <strong>of</strong>f while rheological data 14ere being taJcen.<br />

The temperature could be held constant 1AJ"ithin 0.1 degree<br />

Centigrade,<br />

A grooved cast acrylic lid was also fabricated<br />

to cover the 600 mI. beaker Hhile the Carbopol solutions<br />

were at the higher temperatures to prevent evaporation<br />

losses..<br />

The apparatus is sh01m in Figure A-3.<br />

The average <strong>of</strong> the three readings <strong>of</strong> torque 1...ras used<br />

to calCUlate the shear stress. nn, the slope <strong>of</strong> the logaritlLmic<br />

plot <strong>of</strong> torque (or shear stress) versus rotational<br />

speed, ""'las needed to calculate the shear rate. n ll v-Jas evaluated<br />

<strong>for</strong> each fluid at each temperature using a linear regression.<br />

The actual calcu~ations Here per<strong>for</strong>med by the IB}1<br />

1620 digital computer. The computer programs are enclosed<br />

at the End <strong>of</strong> this Appendix.<br />

The slope <strong>for</strong> each condition<br />

is listed in Table A-4.<br />

The shear rate at each point was then calculated using<br />

equation 2-12.<br />

The apparent viscosi t·y Has calculated using<br />

(2-23

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