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Chiral Stationary Phases<br />
Crown Ether Phase<br />
SiO 2 O Si<br />
O<br />
Product Particle Size Column Dimensions <strong>Catalog</strong><br />
ChiroSil ®<br />
Analytical to Preparative Columns<br />
The ChiroSil ® RCA(+) and SCA(-) chiral<br />
Product<br />
Spherical Silica:<br />
ChiroSil ® SCA(-)<br />
Particle Size<br />
5 µm, 100Å<br />
Column Dimensions<br />
15 cm x 4.6 mm i.d.<br />
<strong>Catalog</strong> #<br />
799101<br />
stationary phases were developed by<br />
ChiroSil<br />
RStech Corporation in Daejeon, South<br />
SCA(-) 5 µm, 100Å 25 cm x 4.6 mm i.d. 799102<br />
Korea. This phase is prepared by a covalent<br />
ChiroSil ® SCA(-) 5 µm, 100Å 25 cm x 10.0 mm i.d. 799106<br />
trifunctional bonding of (+) or (-)-<br />
(18-Crown-6)-tetracarboxylic acid as the<br />
chiral selector. The covalent bonding<br />
ensures universal solvent compatibility<br />
and allows operation under ambient<br />
conditions. Columns are available in<br />
both enantiomeric forms to allow the<br />
ChiroSil ® SCA(-)<br />
ChiroSil ® SCA(-)<br />
ChiroSil ® RCA(+)<br />
ChiroSil ® RCA(+)<br />
ChiroSil ® RCA(+)<br />
5 µm, 100Å<br />
5 µm, 100Å<br />
5 µm, 100Å<br />
5 µm, 100Å<br />
5 µm, 100Å<br />
25 cm x 21.1 mm i.d.<br />
25 cm x 30.0 mm i.d.<br />
15 cm x 4.6 mm i.d.<br />
25 cm x 4.6 mm i.d.<br />
25 cm x 10.0 mm i.d.<br />
799105<br />
799107<br />
799001<br />
799002<br />
799006<br />
scientist to invert elution order by<br />
ChiroSil<br />
simply switching columns.<br />
RCA(+) 5 µm, 100Å 25 cm x 21.1 mm i.d. 799005<br />
ChiroSil ® RCA(+) 5 µm, 100Å 25 cm x 30.0 mm i.d. 799007<br />
This chiral stationary phase is the choice<br />
for the separation of amino acids and<br />
compounds containing primary amines<br />
on the analytical or preparative scale.<br />
Phenylglycine<br />
Column:<br />
ChiroSil ® RCA(+) or SCA(-) 15 cm x 4.6 mm<br />
Mobile Phase:<br />
O<br />
(70/30) CH 3 OH/H2O +10 mM H 2 SO 4 and 0.1% TEA<br />
H<br />
Flow Rate:<br />
SiO 2 O Si<br />
N O<br />
1.0 mL/min<br />
C<br />
O<br />
HOOC<br />
Detection: UV 210 nm<br />
O O<br />
Run Time<br />
13.1 min<br />
k’ 1 3.14<br />
O<br />
O<br />
2.60<br />
O O<br />
O<br />
COOH<br />
C<br />
O<br />
N<br />
H<br />
To request a copy of the Chiral HPLC<br />
Application Guide containing additional<br />
Chiral Applications contact us by phone,<br />
800.323.8144 ext. 662<br />
847.967.6000 ext. 662<br />
or e-mail,<br />
sales@registech.com<br />
16<br />
For more information visit www.registech.com/chiral<br />
ChiroSil ® is a trademark of RStech Corporation of Daejeon, South Korea