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Chapter 3<br />

Synthesis of trisubstituted pyrazoles/isoxazoles<br />

IR spectrum of compound 5b<br />

90<br />

%T<br />

75<br />

60<br />

3294.53<br />

3279.10<br />

3259.81<br />

3153.72<br />

3099.71<br />

3020.63<br />

2953.12<br />

2895.25<br />

2839.31<br />

1728.28<br />

1681.98<br />

1589.40<br />

1429.30<br />

1400.37<br />

1350.22<br />

1309.71<br />

1251.84<br />

1091.75<br />

1006.88<br />

898.86<br />

759.98<br />

732.97<br />

690.54<br />

661.61<br />

626.89<br />

45<br />

30<br />

9<br />

1639.55<br />

1508.38<br />

1485.24<br />

821.70<br />

592.17<br />

497.65<br />

516.94<br />

470.65<br />

4000<br />

3500<br />

3000<br />

2500<br />

2000<br />

1750<br />

1500<br />

1250<br />

1000<br />

750<br />

500<br />

1/cm<br />

IR spectrum of compound 6b<br />

100<br />

%T<br />

80<br />

1695.49<br />

60<br />

1095.60<br />

1058.96<br />

968.30<br />

40<br />

2895.25<br />

1558.54<br />

1350.22<br />

1253.77<br />

1004.95<br />

896.93<br />

759.98<br />

715.61<br />

690.54<br />

430 14<br />

20<br />

0<br />

3294.53<br />

3277.17<br />

3149.86<br />

3093.92<br />

3018.70<br />

1633.76<br />

1591.33<br />

1516.10<br />

1496.81<br />

1404.22<br />

1311.64<br />

810.13<br />

-20<br />

4000<br />

3500<br />

3000<br />

2500<br />

2000<br />

1750<br />

1500<br />

1250<br />

1000<br />

750<br />

500<br />

1/cm<br />

Department of Chemistry <strong>Saurashtra</strong> university, Rajkot-360005 117

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