Extraction Technologies for Medicinal and Aromatic ... - Capacity4Dev
Extraction Technologies for Medicinal and Aromatic ... - Capacity4Dev Extraction Technologies for Medicinal and Aromatic ... - Capacity4Dev
1 AN OVERVIEW OF EXTRACTION TECHNIQUES FOR MEDICINAL AND AROMATIC PLANTS emulsion absorbed by the sponge was removed by squeezing it into the concolina or some other container. It is reported that oil produced this way contains more of the fruit odor character than oil produced by any other method. A second method known as equaling (or the scodella method), uses a shallow bowl of copper (or sometimes brass) with a hollow central tube; the equaling tool is similar in shape to a shallow funnel. The bowl is equipped with brass points with blunt ends across which the whole citrus fruit is rolled by hand with some pressure until all of the oil glands have burst. The oil and aqueous cell contents are allowed to dribble down the hollow tube into a container from which the oil is separated by decantation. Obviously, hand pressing is impractical because it is an extremely slow process, e.g. on average only 2-4 lbs oil per day can be produced by a single person using one of these hand methods. As a result, over the years a number of machines have been designed to either crush the peel of a citrus fruit or crush the whole fruit and then separate the oil from the juice. 1.3.5.3.4.1 Pelatrice Process In the pelatrice process, citrus fruits are fed from a hopper into the abrasive shell of the machine. The fruits are rotated against the abrasive shell by a slow-moving Archimedian screw whose surface rasps the fruit surfaces causing some of the essential oil cavities on the peel to burst and release their oil-water emulsion. This screw further transports the fruit into a hopper in which rollers covered with abrasive spikes burst the remaining oil cavities. The oil and water emulsion is washed away from the fruit by a fi ne spray of water. The emulsion next passes through a separator where any solids are removed, after which it passes through two centrifugal separators working in series to yield the pure oil. Most bergamot oil and some lemon oil are produced this way in Italy. 1.3.5.3.4.2 Sfumatrice Process The sfumatrice equipment consists of a metallic chain that is drawn by two horizontal ribbed rollers. The peels are conveyed through these rollers during which time they are pressed and bent to release their oil. As in pelatrice, the oil is washed away from the sfumatrice rollers by fi ne sprays of water. Again, the oil is initially passed through a separator prior to being sent to two centrifuges in series, so that purifi ed oil can be produced. At one time, sfumatrice was the most popular process for citrus oil isolation in Italy; however, today the pelatrice method appears more popular. 1.3.5.3.5 Essential Oil Extraction with Cold Fat (Enfleurage) Despite the introduction of the modern process of extraction with volatile solvents, the old fashioned method of enfl eurage, as passed on 48
EXTRACTION TECHNOLOGIES FOR MEDICINAL AND AROMATIC PLANTS from father to son and perfected in the course of generations, still plays an important role. Enfl eurage on a large scale is today carried out only in the Grasse region of France, with the possible exception of isolated instances in India where the process has remained primitive. The principles of enfl eurage are simple. Certain fl owers (e.g. tuberose and jasmine) continue the physiological activities of developing and giving off perfume even after picking. Every jasmine and tuberose fl ower resembles, so to speak, a tiny factory continually emitting minute quantities of perfume. Fat possesses a high power of absorption and, when brought in contact with fragrant fl owers, readily absorbs the perfume emitted. This principle, methodically applied on a large scale, constitutes enfl eurage. During the entire period of harvest, which lasts for eight to ten weeks, batches of freshly picked fl owers are strewn over the surface of a specially prepared fat base (corps), let there (for 24 h in the case of jasmine and longer in the case of tuberose), and then replaced by fresh fl owers. At the end of the harvest, the fat, which is not renewed during the process, is saturated with fl ower oil. Thereafter, the oil is extracted from the fat with alcohol and then isolated. The success of enfl eurage depends to a great extent upon the quality of the fat base employed. Utmost care must be exercised when preparing the corps. It must be practically odorless and of proper consistency. If the corps is too hard, the blossoms will not have suffi cient contact with the fat, curtailing its power of absorption and resulting in a subnormal yield of fl ower oil. On the other, if it is too soft, it will tend to engulf the fl owers and the exhausted ones will adhere; when removed, the fl owers will retain adhering fat, resulting in considerable shrinkage and loss of corps. The consistency of the corps must, therefore, be such that it offers a semihard surface from which the exhausted fl owers can easily be removed. The process of enfl eurage is carried out in cool cellars, and every manufacturer must prepare the corps according to the prevailing temperature in the cellars during the months of the fl ower harvest. Many years of experience have proved that a mixture of one part of highly purifi ed tallow and two parts of lard is eminently suitable for enfl eurage. This mixture assures a suitable consistency of the corps in conjunction with high power of absorption. The fat corps thus prepared is white, smooth, absolutely of uniform consistency, free of water and practically odorless. Some manufacturers also add small quantities of orange fl ower or rose water when preparing the corps. This seems to be done for the sake of convention. Such additions somewhat shade the odor of the fi nished product by imparting a slight orange blossom or rose note. 49
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1 AN OVERVIEW OF EXTRACTION TECHNIQUES FOR MEDICINAL AND AROMATIC PLANTS<br />
emulsion absorbed by the sponge was removed by squeezing it into the<br />
concolina or some other container. It is reported that oil produced this way<br />
contains more of the fruit odor character than oil produced by any other<br />
method.<br />
A second method known as equaling (or the scodella method),<br />
uses a shallow bowl of copper (or sometimes brass) with a hollow central<br />
tube; the equaling tool is similar in shape to a shallow funnel. The bowl is<br />
equipped with brass points with blunt ends across which the whole citrus<br />
fruit is rolled by h<strong>and</strong> with some pressure until all of the oil gl<strong>and</strong>s have<br />
burst. The oil <strong>and</strong> aqueous cell contents are allowed to dribble down the<br />
hollow tube into a container from which the oil is separated by decantation.<br />
Obviously, h<strong>and</strong> pressing is impractical because it is an extremely slow process,<br />
e.g. on average only 2-4 lbs oil per day can be produced by a single person<br />
using one of these h<strong>and</strong> methods. As a result, over the years a number<br />
of machines have been designed to either crush the peel of a citrus fruit or<br />
crush the whole fruit <strong>and</strong> then separate the oil from the juice.<br />
1.3.5.3.4.1 Pelatrice Process<br />
In the pelatrice process, citrus fruits are fed from a hopper into<br />
the abrasive shell of the machine. The fruits are rotated against the abrasive<br />
shell by a slow-moving Archimedian screw whose surface rasps the fruit<br />
surfaces causing some of the essential oil cavities on the peel to burst <strong>and</strong><br />
release their oil-water emulsion. This screw further transports the fruit into<br />
a hopper in which rollers covered with abrasive spikes burst the remaining<br />
oil cavities. The oil <strong>and</strong> water emulsion is washed away from the fruit by a<br />
fi ne spray of water. The emulsion next passes through a separator where any<br />
solids are removed, after which it passes through two centrifugal separators<br />
working in series to yield the pure oil. Most bergamot oil <strong>and</strong> some lemon<br />
oil are produced this way in Italy.<br />
1.3.5.3.4.2 Sfumatrice Process<br />
The sfumatrice equipment consists of a metallic chain that is<br />
drawn by two horizontal ribbed rollers. The peels are conveyed through these<br />
rollers during which time they are pressed <strong>and</strong> bent to release their oil. As<br />
in pelatrice, the oil is washed away from the sfumatrice rollers by fi ne sprays<br />
of water. Again, the oil is initially passed through a separator prior to being<br />
sent to two centrifuges in series, so that purifi ed oil can be produced. At one<br />
time, sfumatrice was the most popular process <strong>for</strong> citrus oil isolation in Italy;<br />
however, today the pelatrice method appears more popular.<br />
1.3.5.3.5 Essential Oil <strong>Extraction</strong> with Cold Fat (Enfleurage)<br />
Despite the introduction of the modern process of extraction<br />
with volatile solvents, the old fashioned method of enfl eurage, as passed on<br />
48