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No. 1, 1998 - Tribology in Industry

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at ciepth /r;<br />

b) the width 8211 of (2,/1) diffraction l<strong>in</strong>e correspond<strong>in</strong>g<br />

to lrirrtensits phase from case-ltarden<strong>in</strong>g steel (8211 is a<br />

size proporl ioirill to tetragonality degree, cia, of martensite<br />

phase;<br />

c) the rvidth 8220 of (220) diffrtrction l<strong>in</strong>e of ferrito-perlitic<br />

phase from steel (8226 is a size proportional to <strong>in</strong>ner<br />

second order tension, .t11 from crystall<strong>in</strong>e lattice);<br />

d) the ratio (l,,,<strong>in</strong>ll,rn) which is proportional to dislocation<br />

density,p, from crystall<strong>in</strong>e lattice (1,r,;, and I,nor) are<br />

respectively m<strong>in</strong>imum and maximumot Q20) diffraction<br />

l<strong>in</strong>e.<br />

Fig.2. Used tibonndel<br />

<strong>in</strong> accordance rvith SKF standarcl and it had the value<br />

1900 MPa, 3300 MPa, 4700 MPa. Dur<strong>in</strong>g the pitt<strong>in</strong>g test<br />

of up to 106 cvcles the l<strong>in</strong>ear-contact benveen triboelements<br />

were cont<strong>in</strong>uously lubricated with a special oil,<br />

ensur<strong>in</strong>g a thermostatic control ii c\0't- lnC.<br />

5. EVALUATION OF THE STR.UCTUITAL<br />

CHANGES, EXPERIMENTAL RESULTS.<br />

From all parameters of the surface layer, x;, i=1-6, only<br />

tension state, -rJ, and structure, -r5, have been studied.<br />

Thus, their distribLrtions (as value) over the depth, /r, of<br />

the surface laYer after pitt<strong>in</strong>g lcst were <strong>in</strong>vestigatecl. In<br />

this aim, the tested rollers u,ere electrochemically polished<br />

us<strong>in</strong>g a spccialii.' nranutactured <strong>in</strong>stallation.<br />

The chemical composition of the electrolyte was: II jPOa<br />

- 750 cnts; H2SCa-t8A on]; Croj-100g; H2O-280 rnl.<br />

Density of electric:tl cr.lrrent of electrolytic cell rvas l=0.7<br />

Alcrn2.Dur<strong>in</strong>g polish<strong>in</strong>g the sample (anocle) by means of<br />

an eng<strong>in</strong>e wris rotat<strong>in</strong>g rvith frec;rrency of 6.25 Hz. T'his<br />

motion assures lr homogeneity of both cclncentration and<br />

temperature of electrolytic bath. Also, a cool<strong>in</strong>g coil did<br />

not allow heat<strong>in</strong>g of the solution. By apply<strong>in</strong>g an electrolytic<br />

polish<strong>in</strong>g technique, lal,ers of 50tr<strong>in</strong>r thickness',vere<br />

successively rernoved from the tested triboelement.<br />

Alier eacl: polish<strong>in</strong>g, the tested roller was mounted on a<br />

X-ray diffraction equipment, type DP.ON-3 (XMoKe,<br />

tl=38kV, I:22 rrt4, .91=l mnt, Sz.=0.1p74). From the13<br />

andx5 parameters, have been evaiuated:<br />

a) relative percentage of residual austenite, YR(o/o),<br />

us<strong>in</strong>g the relation: VR(%) = ftul(a/o)]n*s [R4(%)]1,=0<br />

is the percentage of resiCual austenite at sample surface.<br />

IRA(%)]n*o is the si'rme size <strong>in</strong>sicle of the surface layer<br />

In figure -3 it is presented the depen

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