Allure⢠Acidix HPLC Column - Chromtech.com.au
Allure⢠Acidix HPLC Column - Chromtech.com.au Allure⢠Acidix HPLC Column - Chromtech.com.au
Cocaine (COC) and Ecgonine Methyl Ester (EME) on Allure PFP Propyl Peak List: 1. EME (ecgonine methyl ester) 2. COC (Cocaine) Sample: Inj.: 10µL Conc.: 1µg/mL Solvent: water Temp.: 4°C XIC of +MRM (3 pairs) for 200.0 / 182.0 amu XIC of +MRM (3 pairs) for 304.0 / 182.0 amu 1 0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 min. 0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 min. 2 1.30e3 cps 2.35e3 cps Application Note: LC_0126 Column: Allure PFP Propyl Catalog#: 9169532 Dimensions: 30mm x 2.1mm Particle size: 5µm Pore size: 60Å Conditions: Mobile phase: Flow: Column temp.: 5mM pH 3.0 ammonium formate:acetonitrile (10:90) 0.6mL/min. ambient Det.: PE/Sciex API 3000 Interface: Turbo Ion Spray, ESI Interface temp.: 150°C Ion mode: positive ESI probe voltage: 5000V Orifice: + 71V Ring: + 265V Collision gas: Nitrogen Collision gas pressure: 2.2 mTorr Collision gas energy(COC): 28 eV Collision gas energy(EME): 26 eV Electron multiplier: 2100 volts Auxillary gas flow: 7000cc/min. Nebulizer gas setting: 15lb/in. 2 Curtain gas setting: 12lb/in. 2 Data Courtesy of Shane Needham, Pfizer Inc Restek Corporation 110 Benner Circle Bellefonte, PA 16823 • 814-353-1300 • 800-356-1688 • Fax: 814-353-1309 • www.restekcorp.com
Carbamates on Ultra IBD Peak List: 1. Aldicarb Sulfoxide 2. Aldicarb Sulfone 3. Oxamyl 4. Methomyl 5. 3-hydroxycarbofuran 6. Aldicarb 7. Propoxur 8. Carbofuran 9. Carbaryl 10. Methiocarb Sample: Inj.: 5µL Conc.: 1 mg/mL each component Solvent: Methanol 9 Application Note: LC_0134 Column: Ultra IBD Catalog #: 9175565 Dimensions: 150 x 4.6mm Particle Size: 5µm Pore Size: 100Å Conditions: Mobile Phase: Flow: Temp.: Det.: Gradient A: Water B: Methanol Initial: 80% A: 20% B 15 min.: 20% B: 80% B 1.0mL/min ambient UV @ 220nm 10 1 2 3 4 5 6 7 8 0 2 4 6 8 10 12 14 16 18 min. Restek Corporation 110 Benner Circle Bellefonte, PA 16823 • 814-353-1300 • 800-356-1688 • Fax: 814-353-1309 • www.restekcorp.com
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- Page 21 and 22: Restek Advantage, Fall 2000: Ultra
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- Page 25 and 26: Restek -- HPLC Methods Development
- Page 27 and 28: Restek -- HPLC Applications (PDF) H
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- Page 35 and 36: Acetaminophen on Allure Acidix Pea
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- Page 39 and 40: Tricyclic Antidepressants on Allure
- Page 41 and 42: Ibuprofen and 1 Application Note:00
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- Page 45 and 46: Metoprolol on Allure Basix Peak Li
- Page 47 and 48: Cyclobenzaprine on Allure Basix Pe
- Page 49 and 50: Norethindrone and 1 Application Not
- Page 51 and 52: Sertraline HCI on Allure Basix Pea
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- Page 55 and 56: Atenolol on Allure Basix Peak List
- Page 57 and 58: Trycyclic Antidepressants Applicati
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- Page 61 and 62: Norgestrel and Ethynyl Estradiol on
- Page 63 and 64: EPA Method 8330 Application Note:00
- Page 65: Benzaldehyde, Hydrocortisone, and P
- Page 69 and 70: Thymine, Thymidine, TTP, TDP, and T
- Page 71 and 72: Cytosine, Cytidine, CTP, CDP, and C
- Page 73 and 74: 11 Component Mixture of Nucleotides
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- Page 77 and 78: Cephaloridine by Normal Phase on Ul
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- Page 81 and 82: Digoxin on Ultra IBD Peak List: 1.
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- Page 85 and 86: Acids and Bases @ pH3 Application N
- Page 87 and 88: Levothyroxine on Ultra PFP Peak Lis
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Cocaine (COC) and<br />
Ecgonine Methyl Ester (EME)<br />
on Allure PFP Propyl<br />
Peak List:<br />
1. EME (ecgonine methyl ester)<br />
2. COC (Cocaine)<br />
Sample:<br />
Inj.: 10µL<br />
Conc.: 1µg/mL<br />
Solvent: water<br />
Temp.: 4°C<br />
XIC of +MRM (3 pairs) for 200.0 / 182.0 amu<br />
XIC of +MRM (3 pairs) for 304.0 / 182.0 amu<br />
1<br />
0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 min.<br />
0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 min.<br />
2<br />
1.30e3 cps<br />
2.35e3 cps<br />
Application Note: LC_0126<br />
<strong>Column</strong>:<br />
Allure PFP Propyl<br />
Catalog#: 9169532<br />
Dimensions: 30mm x 2.1mm<br />
Particle size: 5µm<br />
Pore size: 60Å<br />
Conditions:<br />
Mobile phase:<br />
Flow:<br />
<strong>Column</strong> temp.:<br />
5mM pH 3.0 ammonium<br />
formate:acetonitrile (10:90)<br />
0.6mL/min.<br />
ambient<br />
Det.: PE/Sciex API 3000<br />
Interface:<br />
Turbo Ion Spray, ESI<br />
Interface temp.: 150°C<br />
Ion mode:<br />
positive<br />
ESI probe voltage: 5000V<br />
Orifice:<br />
+ 71V<br />
Ring:<br />
+ 265V<br />
Collision gas:<br />
Nitrogen<br />
Collision gas pressure: 2.2 mTorr<br />
Collision gas energy(COC): 28 eV<br />
Collision gas energy(EME): 26 eV<br />
Electron multiplier: 2100 volts<br />
Auxillary gas flow: 7000cc/min.<br />
Nebulizer gas setting: 15lb/in. 2<br />
Curtain gas setting: 12lb/in. 2<br />
Data Courtesy of Shane Needham, Pfizer Inc<br />
Restek Corporation 110 Benner Circle Bellefonte, PA 16823 • 814-353-1300 • 800-356-1688 • Fax: 814-353-1309 • www.restekcorp.<strong>com</strong>
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