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11. Measure by AAS<br />

Methodology<br />

Compounds are atomized by flame of air –acethyline in 3000 0 C. The elements can absorb<br />

only the wave, which has special length. Then it is possible to determine the element using the<br />

lamp which can emit the special wave.<br />

Materials<br />

Atomic absorption spectrometer<br />

Stock metal solutions, 1000mg L -1<br />

Working metal solutions prepared by dilution of the stock solution<br />

Experimental procedure.<br />

Prepare stock metal solutions and the instrument for analyse (See measures of parameters on<br />

this page). Measure stock metal solutions and construct a calibration graph. Do measurement<br />

on samples.<br />

Measures of parameters<br />

Cupper<br />

Current ; 6mA/0mA Burner height ; 7mm<br />

Wave length ; 324.8nm Burner angle ; 0 deg<br />

Slit width ; 0.5nm Fuel gas flow ; 1.8 l/min<br />

Lighting mode ; BGC –D 2 Type of oxidant ; air<br />

Iron<br />

Current ; 12mA/0mA Burner height ; 7mm<br />

Wave length ; 248.3nm Burner angle ; 0deg<br />

Slit width ; 0.2nm Fuel gas flow ; 2.2 l/min<br />

Lighting mode ; BGC –D 2 Type of oxidant ; air<br />

Manganese<br />

Current ; 10mA/0mA Burner height ; 7mm<br />

Wave length ; 279.5nm Burner angle ; 0 deg<br />

Slit width ; 0.2nm Fuel gas flow ; 2.0 l/min<br />

Lighting mode ; BGC –D 2 Type of oxidant ; air<br />

68

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