FINAL REPORT
FINAL REPORT
FINAL REPORT
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11. Measure by AAS<br />
Methodology<br />
Compounds are atomized by flame of air –acethyline in 3000 0 C. The elements can absorb<br />
only the wave, which has special length. Then it is possible to determine the element using the<br />
lamp which can emit the special wave.<br />
Materials<br />
Atomic absorption spectrometer<br />
Stock metal solutions, 1000mg L -1<br />
Working metal solutions prepared by dilution of the stock solution<br />
Experimental procedure.<br />
Prepare stock metal solutions and the instrument for analyse (See measures of parameters on<br />
this page). Measure stock metal solutions and construct a calibration graph. Do measurement<br />
on samples.<br />
Measures of parameters<br />
Cupper<br />
Current ; 6mA/0mA Burner height ; 7mm<br />
Wave length ; 324.8nm Burner angle ; 0 deg<br />
Slit width ; 0.5nm Fuel gas flow ; 1.8 l/min<br />
Lighting mode ; BGC –D 2 Type of oxidant ; air<br />
Iron<br />
Current ; 12mA/0mA Burner height ; 7mm<br />
Wave length ; 248.3nm Burner angle ; 0deg<br />
Slit width ; 0.2nm Fuel gas flow ; 2.2 l/min<br />
Lighting mode ; BGC –D 2 Type of oxidant ; air<br />
Manganese<br />
Current ; 10mA/0mA Burner height ; 7mm<br />
Wave length ; 279.5nm Burner angle ; 0 deg<br />
Slit width ; 0.2nm Fuel gas flow ; 2.0 l/min<br />
Lighting mode ; BGC –D 2 Type of oxidant ; air<br />
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