Optimizing the Analysis of Volatile Organic Compounds

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68 Method 624 624 Internal Standard Mix bromochloromethane 1,4-dichlorobutane 2-bromo-1-chloropropane 1,500µg/mL each in P&T methanol, 1mL/ampul Each 5-pk. 10-pk. 30023 30023-510 — w/data pack 30023-500 30023-520 30123 624 Surrogate Standard Mix 4-bromofluorobenzene pentafluorobenzene fluorobenzene 2,000µg/mL each in P&T methanol, 1mL/ampul Each 5-pk. 10-pk. 30243 30243-510 — w/data pack 30243-500 30243-520 30343 Surrogate Standard 1,4-bromofluorobenzene α,α,α-trifluorotoluene 2,500µg/mL each in P&T methanol, 1mL/ampul Each 5-pk. 10-pk. 30484 30484-510 — w/data pack 30484-500 30484-520 30584 624 Calibration Mix #1 bromomethane chloroethane chloromethane 624 Calibration Mix #2 benzene carbon tetrachloride chlorobenzene 2-chloroethyl vinyl ether dibromochloromethane 1,1-dichloroethane trichlorofluoromethane vinyl chloride 2,000µg/mL each in P&T methanol, 1mL/ampul Each 5-pk. 10-pk. 30020 30020-510 w/data pack — 30020-500 30020-520 30120 1,1-dichloroethene 1,2-dichloropropane methylene chloride tetrachloroethene 1,1,2-trichloroethane trichloroethene 2,000µg/mL each in P&T methanol, 1mL/ampul Each 5-pk. 10-pk. 30021 30021-510 — w/data pack 30021-500 30021-520 30121 www.restekcorp.com 624 Calibration Mix #3 bromodichloromethane bromoform chloroform 1,2-dichlorobenzene 1,3-dichlorobenzene 1,4-dichlorobenzene 1,2-dichloroethane trans-1,2-dichloroethene cis-1,3-dichloropropene trans-1,3-dichloropropene ethylbenzene 1,1,2,2-tetrachloroethane toluene 1,1,1-trichloroethane 2,000µg/mL each in P&T methanol, 1mL/ampul Each 5-pk. 10-pk. 30022 30022-510 — w/data pack 30022-500 30022-520 30122 624 Kit 30020: 624 Calib. Mix #1 30022: 624 Calib. Mix #3 30021: 624 Calib. Mix #2 30023: 624 Int. Standard Mix Contains 1mL each of these mixtures. Kit Kit w/Data Pack 30055 30055-500 624 Complete Kit 30020: 624 Calib. Mix #1 30021: 624 Calib. Mix #2 30022: 624 Calib. Mix #3 Contains 1mL each of these mixtures. 30023: 624 Int. Standard Mix 30243: 624 Surrogate Standard Mix Kit Kit w/Data Pack 30244 30244-500 Method 601 & 602 601/602 Purgeable Halocarbons Kit 30042: 502.2 Calib. Mix #1 30022: 624 Calib. Mix #3 30021: 624 Calib. Mix #2 Contains 1mL each of these mixtures. benzene chlorobenzene 1,2-dichlorobenzene 1,3-dichlorobenzene Kit Kit w/Data Pack 30061 30061-500 602 Purgeable Aromatics Calibration Mix 1,4-dichlorobenzene ethylbenzene toluene 2,000µg/mL each in P&T methanol, 1mL/ampul Each 5-pk. 10-pk. 30035 30035-510 — w/data pack 30035-500 30035-520 30135 Method 502.2 502.2 CAL2000 MegaMix Mixture benzene 2,2-dichloropropane bromobenzene 1,1-dichloropropene bromochloromethane cis-1,3-dichloropropene bromodichloromethane trans-1,3-dichloropropene bromoform ethylbenzene n-butylbenzene hexachlorobutadiene sec-butylbenzene isopropylbenzene tert-butylbenzene p-isopropyltoluene carbon tetrachloride methylene chloride chlorobenzene naphthalene chloroform n-propylbenzene 2-chlorotoluene styrene 4-chlorotoluene 1,1,1,2-tetrachloroethane dibromochloromethane 1,1,2,2-tetrachloroethane 1,2-dibromo-3-chloropropane tetrachloroethene 1,2-dibromoethane toluene dibromomethane 1,2,3-trichlorobenzene 1,2-dichlorobenzene 1,2,4-trichlorobenzene 1,3-dichlorobenzene 1,1,1-trichloroethane 1,4-dichlorobenzene 1,1,2-trichloroethane 1,1-dichloroethane trichloroethene 1,2-dichloroethane 1,2,3-trichloropropane 1,1-dichloroethene 1,2,4-trimethylbenzene cis-1,2-dichloroethene 1,3,5-trimethylbenzene trans-1,2-dichloroethene m-xylene 1,2-dichloropropane o-xylene 1,3-dichloropropane p-xylene 2,000µg/mL each in P&T methanol, 1mL/ampul Each 5-pk. 10-pk. 30431 30431-510 — w/data pack 30431-500 30431-520 30531 200µg/mL each in P&T methanol, 1mL/ampul Each 5-pk. 10-pk. 30432 30432-510 w/data pack — 30432-500 30432-520 30532 1-Chloro-2-fluorobenzene 1-chloro-2-fluorobenzene 2,000µg/mL in P&T methanol, 1mL/ampul Each 5-pk. 10-pk. 30040 30040-510 w/data pack — 30040-500 30040-520 30140 502.2 Internal Standard Mix #2 2-bromo-1-chloropropane fluorobenzene 2,000µg/mL each in P&T methanol, 1mL/ampul Each 5-pk. 10-pk. 30041 30041-510 w/data pack — 30041-500 30041-520 30141
8021/502.2 Surrogate Mix #1 1-bromo-2-chloroethane fluorobenzene 1-chloro-3-fluorobenzene 2,000µg/mL each in P&T methanol, 1mL/ampul Each 5-pk. 10-pk. 30463 30463-510 — w/data pack 30463-500 30463-520 30563 8021/502.2 Surrogate Mix #2 1-bromo-2-chloroethane 1-chloro-3-fluorobenzene 4-bromochlorobenzene fluorobenzene 2,000µg/mL each in P&T methanol, 1mL/ampul Each 5-pk. 10-pk. 30464 30464-510 — w/data pack 30464-500 30464-520 30564 502.2 VOA Calib. Kit #2 (2000ppm) 30042: 502.2 Calib. Mix #1 30431: 502.2 CAL2000 MegaMix Contains 1mL each of these mixtures. Kit Kit w/Data Pack 30445 30445-500 502.2 VOA Calib. Kit #3 (200ppm) 30439: 502.2 Calib. Mix #1A 30432: 502.2 CAL200 MegaMix Contains 1mL each of these mixtures. Kit Kit w/Data Pack 30446 30446-500 502.2 Calibration Mix #1 (gases) bromomethane chloroethane chloromethane dichlorodifluoromethane trichlorofluoromethane vinyl chloride 2,000µg/mL each in P&T methanol, 1mL/ampul Each 5-pk. 10-pk. 30042 30042-510 w/data pack 30042-500 30042-520 30142 502.2 Calibration Mix #1A bromomethane chloroethane chloromethane dichlorodifluoromethane trichlorofluoromethane vinyl chloride 200µg/mL each in P&T methanol, 1mL/ampul Each 5-pk. 10-pk. 30439 30439-510 — w/data pack 30439-500 30439-520 30539 04.2, 04.1, & 3/90 SOW CLP 04.1 VOA Internal Standard/SMC Spike Mix bromochloromethane 4-bromofluorobenzene chlorobenzene-d5 VOA Internal Standard Mix bromochloromethane chlorobenzene-d5 1,4-difluorobenzene 2,500µg/mL each in P&T methanol, 1mL/ampul Each 5-pk. 10-pk. 30011 30011-510 — w/data pack 30011-500 30011-520 30111 VOA Surrogate Spike Mix 4-bromofluorobenzene toluene-d8 1,2-dichloroethane-d4 2,500µg/mL each in P&T methanol, 1mL/ampul Each 5-pk. 10-pk. 30004 30004-510 — w/data pack 30004-500 30004-520 30104 VOA Matrix Spike Mix benzene chlorobenzene 1,1-dichloroethene toluene trichloroethene 2,500µg/mL each in P&T methanol, 1mL/ampul Each 5-pk. 10-pk. 30005 30005-510 — w/data pack 30005-500 30005-520 30105 VOA Screening Mix #1 benzene ethylbenzene toluene 1,2-dichloroethane-d4 1,4-difluorobenzene toluene-d8 2,500µg/mL each in P&T methanol, 1mL/ampul Each 5-pk. 10-pk. 30457 30457-510 — w/data pack 30457-500 30457-520 30557 o-xylene p-xylene 1,000µg/mL each in P&T methanol, 1mL/ampul Each 5-pk. 10-pk. 30001 30001-510 — w/data pack 30001-500 30001-520 30101 69 VOA Screening Mix #2 n-dodecane n-nonane 1,000µg/mL each in P&T methanol, 1mL/ampul Each 5-pk. 10-pk. 30002 30002-510 w/data pack — 30002-500 30002-520 30102 VOA Tuning Compound 4-bromofluorobenzene 5,000µg/mL in P&T methanol, 1mL/ampul Each 5-pk. 10-pk. 30003 30003-510 w/data pack — 30003-500 30003-520 30103 PFTBA (MS Tuning Compound) perfluorotributylamine (PFTBA) 1mL/ampul, neat Each 30482 U DID KNOW? Restek reference materials include a silanized vial for sample transfer. www.restekcorp.com
Page 1 and 2:
Optimizing the Analysis of Volatile
Page 3 and 4:
EPA Method Definitions Many EPA met
Page 5 and 6:
Table I. State gasoline methods inc
Page 7 and 8:
Purge and Trap Theory Concentration
Page 9 and 10:
Step 5. Desorb Once the desorb preh
Page 11 and 12:
Adsorbent Materials Tenax ® Adsorb
Page 13 and 14:
Table II. Compositions and characte
Page 15 and 16:
Troubleshooting Common Problems Ass
Page 17 and 18: Broad Peaks: Peak broadening is ano
Page 19 and 20: Figure 14. Configuring your GC is s
Page 21 and 22: Narrow-bore Systems (0.18mm ID - 0.
Page 23 and 24: Detection Systems VOCs can be analy
Page 25 and 26: FID Operation The flame ionization
Page 27 and 28: Figure 22. Cross-section of the The
Page 29 and 30: Similarly, the PTFE transfer line b
Page 31 and 32: Figure 29. Electromagnetic fields f
Page 33 and 34: Abundance 320000 280000 240000 2000
Page 35 and 36: Connect the capillary column, 0.25m
Page 37 and 38: Applications Using GC Detection Sys
Page 39 and 40: Figure 39B. An Rtx ® -VGC primary
Page 41 and 42: Rtx ® -502.2 75m, 0.45mm ID, 2.55
Page 43 and 44: Figure 41B. Analytes listed in EPA
Page 45 and 46: Figure 42B. An Rtx ® -VGC / Rtx ®
Page 47 and 48: Purge and Trap Applications Using P
Page 49 and 50: Gasoline Analysis with Oxygenates a
Page 51 and 52: Figure 47. Volatile organics by US
Page 53 and 54: 1. dichlorodifluoromethane 2. chlor
Page 55 and 56: 1. chloromethane 2. vinyl chloride
Page 57 and 58: Table IX Volatile organic compounds
Page 59 and 60: Table XI. Choosing a Volatiles GC C
Page 61 and 62: Ordering Information | Rtx ® Rtx -
Page 63 and 64: Siltek -Deactivated Guard Columns/
Page 65 and 66: Leak Detective II Leak Detector Af
Page 67: Method 8260 8260 Internal Standard
Page 71 and 72: 04.2 & 04.1 SOW CLP 04.1 VOA CAL200
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