CRYSTALSIX - Schoonover, Inc.

CRYSTALSIX - Schoonover, Inc. CRYSTALSIX - Schoonover, Inc.

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CrystalSix Sensor Operating Manual Table 4-1 Troubleshooting (continued) Symptom Cause Remedy Crystal ceases to oscillate during deposition before it reaches its “normal life. Crystal does not oscillate or oscillates intermittently (both in vacuum and in air). Crystal oscillates in vacuum but stops oscillation after open to air. Crystal near the end of its life. Scratches or foreign particles on the crystal holder seating surface. Crystal is being hit by small droplets of molten material from the evaporation source. Damaged crystal. Deposition material built-up on edge of the crystal holder and touching the crystal. Material on crystal holder partially masking full crystal area. Defective or damaged crystal. Existence of electrical short or poor electrical contacts. Crystal was near the end of its life; opening to air causes film oxidation, which increases film stress. Excessive moisture accumulation on the crystal. Replace crystal. Replace the crystal holder (IPN 750-262-G1). Clean, polish the crystal seating surface of the crystal holder. Move the sensor further away from the evaporant source. Change crystal. Clean the crystal holder. Clean crystal holder. Replace crystal. Check for electrical continuity and short in sensor cable, connector, contact springs, feedthroughs. Replace crystal Turn off cooling water to sensor before opening it to air; flow hot water through the sensor when the chamber is open. IPN 074-155G 4 - 10

CrystalSix Sensor Operating Manual Table 4-1 Troubleshooting (continued) IPN 074-155G Symptom Cause Remedy Thermal instability: large changes in thickness reading during source warm-up (usually causes thickness reading to decrease) and after the termination of deposition (usually causes thickness reading to increase) Poor thickness reproducibility Crystal not properly seated. Excessive heat input to the crystal. No cooling water. Poor thermal transfer from water tube to body. Erratic source emission characteristics. Check and clean crystal seating surface of the crystal holder. If heat is due to radiation from the evaporation source, move sensor further away from source and use sputtering crystals for better thermal stablity. Check cooling water flow rate. Flow rate should be minimum of 150-200 c/min @ 30 °C max. Use a new water tube whenever the clamping assembly has been removed from the body. If a new water tube is not available, use a single layer of common aluminum foil between the cooling tube and the sensor body, if your process allows. Move sensor to a different location; check the evaporation source for proper operating conditions; insure relatively constant pool height and avoid tunneling into the melt. 4 - 11

CrystalSix Sensor Operating Manual<br />

Table 4-1 Troubleshooting (continued)<br />

IPN 074-155G<br />

Symptom Cause Remedy<br />

Thermal instability: large<br />

changes in thickness<br />

reading during source<br />

warm-up (usually causes<br />

thickness reading to<br />

decrease) and after the<br />

termination of deposition<br />

(usually causes<br />

thickness reading to<br />

increase)<br />

Poor thickness<br />

reproducibility<br />

Crystal not properly<br />

seated.<br />

Excessive heat input to<br />

the crystal.<br />

No cooling water.<br />

Poor thermal transfer<br />

from water tube to body.<br />

Erratic source emission<br />

characteristics.<br />

Check and clean crystal<br />

seating surface of the<br />

crystal holder.<br />

If heat is due to radiation<br />

from the evaporation<br />

source, move sensor<br />

further away from source<br />

and use sputtering<br />

crystals for better thermal<br />

stablity.<br />

Check cooling water flow<br />

rate. Flow rate should be<br />

minimum of 150-200<br />

c/min @ 30 °C max.<br />

Use a new water tube<br />

whenever the clamping<br />

assembly has been<br />

removed from the body. If<br />

a new water tube is not<br />

available, use a single<br />

layer of common<br />

aluminum foil between<br />

the cooling tube and the<br />

sensor body, if your<br />

process allows.<br />

Move sensor to a<br />

different location; check<br />

the evaporation source<br />

for proper operating<br />

conditions; insure<br />

relatively constant pool<br />

height and avoid<br />

tunneling into the melt.<br />

4 - 11

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