terms of the illuminance responsivity is less than 0.5 %, which is declared in our calibration and measurement capability (CMC) of the luminous intensity. ITS-90 - RTM( o C) 2 0 -2 -4 -6 -8 1500 2000 2500 3000 Temperature( o C) Figure 2. Temperature difference between the ITS-90 and the radiometric temperature measurement (RTM) at different temperatures. Table 1. Uncertainty budget of comparison of the ITS-90 and the radiometric temperature measurement at 2700 °C. Uncertainty Sources Components ( o C; k=2) the ITS-90 Temperature scale 0.68 Radiometric temperature measurement Spectral responsivity 1.07 Infrared leakage 0.17 Distance 0.35 Blackbody aperture 0.05 Radiometer aperture 0.04 Signal measurement 0.02 Comparison Stability 0.1 using blackbody Uniformity 0.15 Combined uncertainty (k=2) 2.1 To understand the difference and draw out ideas to improve the consistency, the comparison uncertainty at 2700 °C is evaluated as shown in Table 1, where the uncertainty from the ITS-90 realization, the radiometric temperature measurement, and the comparison process using the blackbody are considered. The uncertainty of the ITS-90 is estimated by the local realization of the ITS-90 and the measurement deviation of the two spectral bands of the pyrometer. Taking the uncertainty components such as the cooper fixed point blackbody, and the spectral characteristics, non-linearity of the pyrometer into account according to the standard method described in the reference [7], we estimated the ITS-90 realization uncertainty. The expanded uncertainty (k=1) increases from 0.1 °C at the copper fixed point to 0.7 °C at 3000 °C. The uncertainty of the ITS-90 is smaller than that of the radiometric temperature measurement, in which the spectral responsivity uncertainty is the dominant uncertainty component. Although the temperature differences shown in Fig. 2 are within the error bars, the uncertainty evaluation seems to be somehow optimistic. A systematic error might be mainly related to our lower assignment in scaling the spectral responsivity and the illuminance responsivity, which is observed also in the key comparisons such as CCPR-K.2.b [8] and CCPR-K3.b.2 [9]. Additionally, since the silicon-based photometer can response up to 1100 nm and the spectral emission of the blackbody is more dominant in the infrared, the calibration range of the radiometer spectral responsivity needs to be extended. The uncertainty of the infrared leakage in Table 1 is estimated by assuming a uniform leakage in the order of 10 -6 from 825 nm to 1100 nm. The infrared leakage uncertainty become more significant as the temperature deceases, resulting in 0.5 °C at 1700 °C. We expect that an improvement in the spectral responsivity measurement of the radiometer can resolve the systematic error below 2600 °C. Above 2600 °C, however, we address the pyrometer linearity as an important correction factor to be considered, which has been only measured below the irradiance level corresponding to 2600 °C. IV. Conclusion Consistency of radiometric temperature measurements with the local realization of the ITS-90 at KRISS is confirmed by comparing the blackbody temperatures measured with a reference pyrometer and a filter radiometer in a range from 1700 °C to 2900 °C. The differences are within 2 °C, which is less than the measurement uncertainty as well as our calibration and measurement capability of luminous intensity that is 0.5 %. More accurate calibration of the spectral responsivity of the radiometer in the IR range up to 1100 nm is expected to resolve the systematic error below 2600 °C. Above 2600 °C, it is necessary to check nonlinearity of the pyrometer. Acknowledgement. We are grateful to Dr. Howard Yoon and Dr. Robert D. Saunders at NIST for their continuous encouragement and valuable discussions. References [1] Khlevnoy B. B., Harrison N. J., Rogers L. J., Pollard D. F., Fox N. P., Sperfeld P., Fischer J.,Friedrich R., Metzdorf J., Seidel J., Samoylov M. L., Stolyarevskaya R. I., Khromchenko V. B.,Ogarev S. A., and Sapritsky V. I., Metrologia, 40, S39-S44, 2003. [2] Yoon H. W., Sperfeld P., Galal Yousef S., and Metzdorf J., Metrologia, 37, 377-380, 2000. [3] Sperfeld, P., Raatz, K.-H., Nawo, B., Moller, W., and Metzdorf, J. Metrologia, 32, 435-439, 1995/6. [4] Yoon H. W., Gibson C. E., and Barnes P. Y., Appl. Opt., 41, 5879-5890, 2002. [5] Lassila, A., Toivanen, P., and Ikonen, E., Measure. Sci. Technology, 8, 973-977, 1997. [6] Hahn, J. W., Park, S. N., Lee, E. S., and Rhee, C., Temperature: Its Measurement and Control in Science and Industry 6, 227-235, 1992. [7] Fisher, J., Battuello, M., Sadli, M., Ballico, M., Park, S. N., Saunders, P., Zundong, Y., Carol Johnson, B., Van der Ham, E., Sakuma, F., Machin, G., Fox, N., Li, W., Ugur, S. and Matveyev, M. Temperature: Its Measurement and Control in Science and Industry, 7, 631-638, 2003. [8] Goebel, R., and Stock, M., Metrologia, 41/1A, 2004. [9] Ikonen, E., and Holvila, J., Metrologia, 41/1A, 2004. 52
Project of absolute measuring instrument of power on the basis of high-temperature superconducting thermometer for soft X-ray radiation. A.D. Nikolenko 1 , V. F. Pindyurin. Budker Institute of Nuclear Physics, 630090 Novosibirsk, Russian Federation Khrebtov I.A, Malyarov V.G., Khokhlov D.A., Ivanov K.V. S.I.Vavilov State Optical Institute, 199034, St.Petersburg, Russian Federation The present report considers the design and main attainable parameters of an absolute radiometer with electrical substitution of power on the base of high- temperature superconducting film bolometer cooled by the liquid nitrogen. This radiometer will be created in the framework of the ISTC project #2920 in the Vavilov State Optical Institute (St. Petersburg, Russia). As is planned, this instrument will be used as the reference detector on the "Soft X-ray metrology" station at the VEPP-3 storage ringin of the Siberian Synchrotron Radiation Center (Budker Institute of Nuclear Physics, Novosibirsk, Russia) for measurements of the soft X-ray photon flux with power circa 1mkW with an accuracy of 1%. 1 A.D.Nikolenko@inp.nsk.su Proceedings NEWRAD, 17-19 October 2005, Davos, Switzerland 53
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