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filters with 4⋅ 10 -6 nm/K thermal drift, and a light weight<br />

carbon fiber frame with a very low coefficient of axial<br />

expansion. The RT1550 is also equipped with a<br />

water-cooled lens mount for additional temperature<br />

stabilization. The total length of each pyrometer is 550 mm,<br />

and they have an integrated electronic module with a<br />

single USB connection to a laptop computer that contains<br />

the control software.<br />

Calibration of pyrometers<br />

Fixed-point BBs at the freezing temperatures of Sn, Zn, Al,<br />

and Ag have been used as reference standard sources of<br />

spectral radiance. In addition, a Au fixed point has been<br />

used to verify the calibration of an RT900. As an example,<br />

the freezing plateau of the Zn is shown in Fig. 4.<br />

The defining equation of ITS-90, which is based on<br />

Planck’s radiation law, has been used with a RT900<br />

pyrometer to compare the calibrations with Al, Ag, and Au<br />

fixed points. The deviations, shown in Table 1 for an<br />

RT900, are calculated relative to the calibration at the Ag<br />

fixed point.<br />

Temperature, ºC<br />

419.5275<br />

419.5270<br />

419.5265<br />

419.5260<br />

419.5255<br />

dedicated to the spectral radiance characterization of IR<br />

radiation sources as well as to the maintenance and<br />

dissemination of the radiance temperature scale below the<br />

silver point.<br />

This new facility will employ two different fixed-point<br />

BB designs with different crucible geometry and furnace<br />

designs: a traditional NIST design 6 as well as more a<br />

recent one 7 . We have performed a first round of<br />

comparisons of these two different BBs, which indicates<br />

the existence of a small but statistically significant<br />

difference in radiance temperatures. A consistent offset is<br />

found even in the case of using the same furnace with<br />

different crucibles.<br />

One possible cause of such a systematic offset in<br />

measurement with two different furnaces is the<br />

out-of-field-scatter (SSE) that is very dependent on the<br />

furnace design. However, the SSE correction cannot be<br />

easily applied because of the partially obscured<br />

observation conditions of many features of the radiation<br />

field. Because of this, we have decided to take an approach<br />

originally suggested by Jones and Tapping 8 and<br />

demonstrated in Fig. 5 below. A fixed-point blackbody is<br />

used in a regular configuration. The only difference is that<br />

in place of the metal filled crucible we use an empty one<br />

that has had the rear half of the cavity removed. In this<br />

case the ideal field of view of the pyrometer is totally filled<br />

with a highly absorbing cone attached to BB rear flange.<br />

419.5250<br />

0:00:00 1:00:00 2:00:00 3:00:00 4:00:00<br />

Time<br />

Figure 4. Freezing plateau of Zn measured with an RT1550.<br />

An RT1550 has been calibrated with Sn, Zn, Al, and Ag<br />

fixed points. Next, the Sakuma-Hattori interpolation<br />

equation 3 has been fitted with the measurement results<br />

using a nonlinear fitting software 4 . The deviations, shown<br />

in Table 1 for the RT1550, demonstrate the difference<br />

between the defined fixed-point temperatures and the<br />

temperatures achieved with the Sakuma-Hattori<br />

interpolation equation.<br />

Table 1. Evaluation Results of Pyrometers<br />

Fixed ITS-90 freezing Deviation from ITS-90, mK<br />

point temperature, C RT900 RT1550<br />

Sn 231.928 n/a 3<br />

Zn 419.527 n/a 23<br />

Al 660.323 -18 -13<br />

Ag 961.780 0 44<br />

Au 1064.18 25 n/a<br />

We do not have sufficient history to fully account for long<br />

term stability, but after round-trip transportation to a<br />

customer in California and one year of use, the RT1500<br />

and RT900 agreed to within 0.1 ºC.<br />

Discussion<br />

Pyrometer development was performed in the framework<br />

of a project to build a customer facility for IR spectral<br />

emissivity calibration 5 . Currently both pyrometer models<br />

are being incorporated into a new NIST facility that will be<br />

Figure 5. Out-of-field scatter experiment schematic<br />

The results of the crucible comparison and out-of-field<br />

scatter contribution for both furnaces should be available<br />

by the time of the conference.<br />

Acknowledgments The authors would like to thank Peter<br />

Saunders (MSL, New Zeeland) for providing the nonlinear fitting<br />

software used for the calculation of Sakuma-Hattori parameters,<br />

and Howard Yoon (NIST) for his advice on lens selection.<br />

References<br />

1. Preston-Thomas, H., The ITS-90,” Metrologia 27, 3-10, 1990.<br />

2. Ohtsuka M., Bedford R.E., Measurement of size-of-source<br />

effects in an optical pyrometer, Measurement 7, 2-6, 1988.<br />

3. Sakuma, F. and Kobayashi, M., Interpolation Equations of<br />

scales of radiation thermometers, in Proc. TEMPMEKO 1997,<br />

305-310, 1997.<br />

4. Saunders, P., White, D. R., Physical basis of interpolation<br />

equations for radiation thermometry, Metrologia, 40, 195–203,<br />

2003.<br />

5. Hanssen, L.M., Mekhontsev, S.N., and Khromchenko, V.B.,<br />

Infrared spectral emissivity characterization facility at NIST,<br />

Proc. SPIE 5405, 1-12, 2004.<br />

6. Mielenz, K.D., Saunders, R.D., and Shumaker, J., Spectroradiometric<br />

Determination of Freezing Temperature of Gold, J.<br />

Res. Natl. Inst. Stand. Techn. 95, 49-67, 1990.<br />

7. Hanssen, L. M., Mekhontsev, S. N., Khromchenko, V. B.,<br />

Prokhorov, A. V. and Zeng, J., Study of infrared emissivity of<br />

a fixed-point blackbody cavity, Proc. NEWRAD 2005.<br />

8. Jones T.P., and Tapping, J., Precision Photoelectric Pyrometer<br />

for the Realization of the IPTS-68 above 1064.43 ° C,<br />

Metrologia 18, 23-31, 1982.<br />

314

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