Here - PMOD/WRC
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filters with 4⋅ 10 -6 nm/K thermal drift, and a light weight<br />
carbon fiber frame with a very low coefficient of axial<br />
expansion. The RT1550 is also equipped with a<br />
water-cooled lens mount for additional temperature<br />
stabilization. The total length of each pyrometer is 550 mm,<br />
and they have an integrated electronic module with a<br />
single USB connection to a laptop computer that contains<br />
the control software.<br />
Calibration of pyrometers<br />
Fixed-point BBs at the freezing temperatures of Sn, Zn, Al,<br />
and Ag have been used as reference standard sources of<br />
spectral radiance. In addition, a Au fixed point has been<br />
used to verify the calibration of an RT900. As an example,<br />
the freezing plateau of the Zn is shown in Fig. 4.<br />
The defining equation of ITS-90, which is based on<br />
Planck’s radiation law, has been used with a RT900<br />
pyrometer to compare the calibrations with Al, Ag, and Au<br />
fixed points. The deviations, shown in Table 1 for an<br />
RT900, are calculated relative to the calibration at the Ag<br />
fixed point.<br />
Temperature, ºC<br />
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dedicated to the spectral radiance characterization of IR<br />
radiation sources as well as to the maintenance and<br />
dissemination of the radiance temperature scale below the<br />
silver point.<br />
This new facility will employ two different fixed-point<br />
BB designs with different crucible geometry and furnace<br />
designs: a traditional NIST design 6 as well as more a<br />
recent one 7 . We have performed a first round of<br />
comparisons of these two different BBs, which indicates<br />
the existence of a small but statistically significant<br />
difference in radiance temperatures. A consistent offset is<br />
found even in the case of using the same furnace with<br />
different crucibles.<br />
One possible cause of such a systematic offset in<br />
measurement with two different furnaces is the<br />
out-of-field-scatter (SSE) that is very dependent on the<br />
furnace design. However, the SSE correction cannot be<br />
easily applied because of the partially obscured<br />
observation conditions of many features of the radiation<br />
field. Because of this, we have decided to take an approach<br />
originally suggested by Jones and Tapping 8 and<br />
demonstrated in Fig. 5 below. A fixed-point blackbody is<br />
used in a regular configuration. The only difference is that<br />
in place of the metal filled crucible we use an empty one<br />
that has had the rear half of the cavity removed. In this<br />
case the ideal field of view of the pyrometer is totally filled<br />
with a highly absorbing cone attached to BB rear flange.<br />
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0:00:00 1:00:00 2:00:00 3:00:00 4:00:00<br />
Time<br />
Figure 4. Freezing plateau of Zn measured with an RT1550.<br />
An RT1550 has been calibrated with Sn, Zn, Al, and Ag<br />
fixed points. Next, the Sakuma-Hattori interpolation<br />
equation 3 has been fitted with the measurement results<br />
using a nonlinear fitting software 4 . The deviations, shown<br />
in Table 1 for the RT1550, demonstrate the difference<br />
between the defined fixed-point temperatures and the<br />
temperatures achieved with the Sakuma-Hattori<br />
interpolation equation.<br />
Table 1. Evaluation Results of Pyrometers<br />
Fixed ITS-90 freezing Deviation from ITS-90, mK<br />
point temperature, C RT900 RT1550<br />
Sn 231.928 n/a 3<br />
Zn 419.527 n/a 23<br />
Al 660.323 -18 -13<br />
Ag 961.780 0 44<br />
Au 1064.18 25 n/a<br />
We do not have sufficient history to fully account for long<br />
term stability, but after round-trip transportation to a<br />
customer in California and one year of use, the RT1500<br />
and RT900 agreed to within 0.1 ºC.<br />
Discussion<br />
Pyrometer development was performed in the framework<br />
of a project to build a customer facility for IR spectral<br />
emissivity calibration 5 . Currently both pyrometer models<br />
are being incorporated into a new NIST facility that will be<br />
Figure 5. Out-of-field scatter experiment schematic<br />
The results of the crucible comparison and out-of-field<br />
scatter contribution for both furnaces should be available<br />
by the time of the conference.<br />
Acknowledgments The authors would like to thank Peter<br />
Saunders (MSL, New Zeeland) for providing the nonlinear fitting<br />
software used for the calculation of Sakuma-Hattori parameters,<br />
and Howard Yoon (NIST) for his advice on lens selection.<br />
References<br />
1. Preston-Thomas, H., The ITS-90,” Metrologia 27, 3-10, 1990.<br />
2. Ohtsuka M., Bedford R.E., Measurement of size-of-source<br />
effects in an optical pyrometer, Measurement 7, 2-6, 1988.<br />
3. Sakuma, F. and Kobayashi, M., Interpolation Equations of<br />
scales of radiation thermometers, in Proc. TEMPMEKO 1997,<br />
305-310, 1997.<br />
4. Saunders, P., White, D. R., Physical basis of interpolation<br />
equations for radiation thermometry, Metrologia, 40, 195–203,<br />
2003.<br />
5. Hanssen, L.M., Mekhontsev, S.N., and Khromchenko, V.B.,<br />
Infrared spectral emissivity characterization facility at NIST,<br />
Proc. SPIE 5405, 1-12, 2004.<br />
6. Mielenz, K.D., Saunders, R.D., and Shumaker, J., Spectroradiometric<br />
Determination of Freezing Temperature of Gold, J.<br />
Res. Natl. Inst. Stand. Techn. 95, 49-67, 1990.<br />
7. Hanssen, L. M., Mekhontsev, S. N., Khromchenko, V. B.,<br />
Prokhorov, A. V. and Zeng, J., Study of infrared emissivity of<br />
a fixed-point blackbody cavity, Proc. NEWRAD 2005.<br />
8. Jones T.P., and Tapping, J., Precision Photoelectric Pyrometer<br />
for the Realization of the IPTS-68 above 1064.43 ° C,<br />
Metrologia 18, 23-31, 1982.<br />
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