2009 Pittcon Final Program - Pittcon Web Archives

Pittcon 2009 Technical Program
(1640-19 P) Characterization of Carbonic Anhydrase Model Complexes
DAVID WILSON, McNeese State University, Joseph Emerson
(1640-20 P) Hyphenated LC-MS/LTQ-Orbitrap Analysis for Cyanotoxin
Chlorination By-products Identification and Monitoring SYLVAIN MEREL,
EHESP/LERES, Barbara Le Bot, Fabrice Monteau, Olivier Thomas, Bruno Le
Bizec, Michel Clement
(1640-21 P) Evaluation of a New Analytical Approach for the Total Organic
Carbon Analysis of Brines STEPHEN LAWSON, Teledyne Tekmar, Tom
Hartlein, Stephen Proffitt, Bryan Gates
(1640-22 P) Fast Gas Chromatographic Analysis of Mineral Oil Using
0.15mm ID Columns COEN DUVEKOT, Varian Inc., Robert Belair, Hans van
den Heuvel, Paul van den Engel
(1640-23 P) A New Approach to Total Nitrogen (TN) and Total Organic
Carbon (TOC) Analysis by High Temperature Combustion (HTC) BRYAN
GATES, Teledyne Tekmar, Stephen Lawson, Tom Hartlein, Stephen Proffitt
POSTER SESSION Session 1650
All posters are to be mounted by 10:00 AM and remain on display until
4:30 PM. You cannot get onto the exposition floor until after 9:00 AM.
Authors must be present from 2:30 PM to 4:30 PM. Location of the
posters is on the center of the Exposition Floor - Aisles 2400-3700.
Pharmaceutical Applications of GC, LC, MS
Tuesday Afternoon
(1650-1 P) Residual Solvent Analysis of Revised USP Methodology in a
Fully Compliant 21 CFR 11 Headspace Analyzer JEFF SHERIFF, EST
Analytical
(1650-2 P) Screening for 430 Pesticide Residues in Traditional Chinese
Medicine Using GC/MS: From Sample Preparation to Report Generation in
One Hour MIKE SZELEWSKI, Agilent Technologies, Wei Luan, Zhi-xiu Xu
(1650-3 P) Application of an Optimized Derivatization Procedure for
Determining Aminomethylphosphonic Acid (AMPA) Impurities by GC/MS
KEN NGIM, Theravance, Zhengtian Gu, Jack Green, Joel Cuzzi
(1650-4 P) Increasing Sensitivity and Throughput of Alkyl Sulfonic Acid
Alkylating Agents and Ester Analysis in Genotoxic Testing PETER G
ALDEN, Waters Corporation, Rob S Plumb, Michael D Jones
(1650-5 P) Analysis of Human Urine with Supported Liquid Extraction and
LC-MS/MS MICHELLE KRANZ, Abbott Laboratories, Jill Polzin, Raymond Xu,
Matthew J Rieser, Tawakol El-Shourbagy
(1650-6 P) Phospholipid Depletion in Bio Analysis using HybridSPE
Technology CRAIG AURAND, Sigma-Aldrich, Hillel Brandes, David S Bell, An
Trinh, Paul R Ross
(1650-7 P) Determination of Non-chromophoric Small Molecule Organic
Acids and Bases Using Corona Charged Aerosol Detector and Mass
Spectrometry Coupled with Various Stationary Phases ZONGYUN
HUANG, Bristol Myer Squibb, Yan Zha
(1650-8 P) Chiral LC-MS Analysis of Drug Substances (Beta-Blockers)
from Plasma Using Macrocyclic Glycopeptide Chiral Stationary Phases
DAVID S BELL, Sigma-Aldirch, Craig Aurand, Jennifer Claus, Jay Jones, Dan
Shollenberger
(1650-9 P) Direct LC/MS Analysis of Basic Drugs in Plasma by On-line
Pretreatment with Weak Cation-Exchange Pretreatment Column
MASATOSHI TAKAHASHI, Shimadzu Scientific Instruments, William Hedgepeth
(1650-10 P) Probing Antibody Purity and Degradation with LC/TOFMS
JULIE KOWALSKI, Restek Corporation, Rick Lake, Becky Wittrig, Frank
Dorman, Amanda J Rigdon
(1650-11 P) A Workflow Approach for the Identification and Structural
Elucidation of Impurities in Quetiapine Fumarate Drug Substance
MICHAEL JONES, Waters Corporation, Marian Twohig
(1650-12 P) A Method Development Approach to Achieve an Impurity
Profile for Impurities Present in A Bulk Drug Substance using Sub 2µm
Porous Particle LC Combined with UV-MS MICHAEL JONES, Waters
Corporation
(1650-13 P) Determination of Boronic Acids using Complexation and HPLC
Separation with Visible Detection JOSEPH CARL HELBLE, Infinity
Pharmaceuticals Inc.
(1650-14 P) Optimization of Gas Chromatographic Parameters and
Screening of Columns from Different Manufacturers that Leads to
Successful Implementation of USP Residual Solvent Methods
MOHAMED NAWAS, Dey L.P., Clint Acheson, Liwen Ye
(1650-15 P) Study of Retention of Norepinephrine with Mixed Mode
Reversed Phase/Liquid Chromatography RATHEESH GUNDA, Western
Illinois University, Tarab J Ahmad
(1650-16 P) The Influence of Organic Modifier on the Adsorption Isotherm
of Ibuprofen on Reversed Phase Liquid Chromatography BAKHEET
ALRESHEEDI, Western Illinois University, Tarab Ahmad
(1650-17 P) Retention of Melamine and Cyanuric Acid on Reversed Phase
Mixed Mode/ Ion Excahnge Liquid Chromatography THOMPSON ALTON ,
Western Illinois University, Tarab J Ahmad
(1650-18 P) Azithromycin in Pharmaceutical Dosage Forms HENDRIK-JAN
BROUWER, Antec Leyden, Lusi van Heerwaarden, Nico Reinhoud, Martin
Eysberg
(1650-19 P) Method Development and Validation for Chemical Purity
Determination of DCGB LIANMEI FENG, deCODE chemistry, Leo Formanski,
Heping Zhang, Jenny Lin
(1650-20 P) Retention Behavior of Dopamine under Overloaded Conditions
on Mixed Mode Reversed Phase/Ion Exchange Liquid Chromatography
KEERTHI GUNDUBOINA, Western Illinois University, Tarab J Ahmad
(1650-21 P) Toward Development of "Generic" Separation Methods for
Achiral Pharmaceutical Analysis Using SFC PAUL M LEFEBVRE, Averica
Discovery Services Inc., Jeffery P Kiplinger, Stephanie K Kavrakis
(1650-22 P) The Use of High Quality Silica Media in Pilot and Process Scale
Chromatography using Custom Designed High Pressure Process LC
Columns and Systems RENO T NGUYEN, Grace Davison Discovery
Sciences, Jochen Saar, Kim Vind, Bart Denoulet
(1650-23 P) Optimizing the Performance of Denali RP Media for Preparative
Purification RENO T NGUYEN, Grace Davison Discovery Sciences, Jochen
Saar, Bart Denoulet
(1650-24 P) Estimation of Rabeprazole Sodium (API) by High-Performance
Liquid Chromatography VIPUL T PRAJAPATI, Faculty of Pharmacy, DDU,
Tushar G Barot
(1650-25 P) A Validated RP-HPLC Method for Simultaneous Estimation of
Impurity Indapamide (Methyl Nitrosoindoline) API VIPUL T PRAJAPATI,
Faculty of Pharmacy, DDU, Tushar G Barot
(1650-26 P) Preliminary Studies on the Characterization of Penicillins via
48 SO + Utilizing cap-HPLC-ICPMS BRITTANY LYN CATRON, University of
Cincinnati, Scott Afton, Joseph A Caruso
(1650-27 P) Method Development for Profiling of Impurities in Synthetic
Oligonucleotides Synthesized by Solid-Phase Phosphoramidite Approach
IRENA NIKCEVIC, University of Cincinnati, Tad Wyrzykiewicz, Patrick A
Limbach
(1650-28 P) Synthesis of 5-(substituted phenyl)-{3-[4-(2-methyl-4-
benzylidene-5-oxo-imidazol-Synthesis of 5-(substituted phenyl)-{3-[4-(2-
methyl-4-benzylidene-5-oxo-imidazol- PIYUSH J VYAS, Sheth M.N. Science
College
POSTER SESSION Session 1660
All posters are to be mounted by 10:00 AM and remain on display until
4:30 PM. You cannot get onto the exposition floor until after 9:00 AM.
Authors must be present from 2:30 PM to 4:30 PM. Location of the
posters is on the center of the Exposition Floor - Aisles 2400-3700.
Physical Measurements
Tuesday Afternoon
(1660-1 P) Simultaneous, Real-Time, Multi-Parameter Analysis of
Nanoparticles in Liquids DUNCAN ALLEN GRIFFITHS, NanoSight, Jeremy
Warren, Andrew Malloy, Bob Carr, Patrick Hole
(1660-2 P) Measuring the Spontaneous Translocation of Phospholipids in
a Supported Bilayer Structure BENJAMIN OBERTS, Michigan State
University, Gary Blanchard
(1660-3 P) Laser Induced Breakdown Detection of Particulate Impurities in
Water Investigation of Dynamics of Optical Breakdown VALERY
BULATOV, Technion-Israel Institute of Technology, Gregory Toker, Jane
Levinson, Tatiana Kovalchuk, Israel Schechter
(1660-4 P) Effect of Higher Concentration of Secondary Ligand on Stability
of Mixed Ligand Complexes RASHMIKANT AMRUTLAL PATEL, Muni. Arts
& U.B. Science College, Dilip S Pabreja
(1660-5 P) An Evaluation of Oxidant Reagents for Total Organic Carbon
Analysis for Low-Level Analysis STEPHEN LAWSON, Teledyne Tekmar,
Tom Hartlein, Stephen Proffitt, Bryan Gates
Tuesday, p.m., March 10
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