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2012 Final Program - Pittcon

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POSTER SESSION Session 2165<br />

All posters will be on display from 10:00 AM to 4:30 PM with authors present from 1:00 PM to 3:00<br />

PM. Location of the posters is on the Exposition Floor – Red Area, Aisles 1300-1500. The Exposition<br />

Floor opens at 9:00 AM.<br />

Pharmaceutical LC Methodology<br />

Wednesday Afternoon, Red Area on Exposition Floor, Aisles 1300-1500<br />

(2165-1 P) Assessment of a New Generation of Evaporative Light-Scattering Detectors for<br />

Liquid Chromatography: Sensitivity, Linearity, Dynamic Range, Analyte<br />

Dispersion and Response Variation with Eluent Composition ERIC VERETTE, Sedere<br />

(2165-2 P) Applications of Type-C Silica based HPLC Columns in Pharmaceutical Analyses<br />

JOSH YOUNG, MicroSolv Technology Corporation, Maria Matyska, Joseph Pesek,<br />

William Ciccone<br />

(2165-3 P) Application of a Unique HPLC Phase When Exploring HPLC Method Development<br />

Challenges for a Pharmaceutical Combination Therapy Containing Five Active<br />

Ingredients ALAN P MCKEOWN, Advanced Chromatography Technologies<br />

(2165-4 P) Exploring and Leveraging Mixed Mode Interactions to Maximize<br />

Chromatographic Selectivity with Uniquely Designed HPLC/UHPLC Stationary<br />

Phases ALAN P MCKEOWN, Advanced Chromatography Technologies<br />

(2165-5 P) Using a Quality-by-Design Approach for Development and Validation of a<br />

Stability Indicating UPLC Method for Ebastine ALEXANDER H SCHMIDT, Steiner<br />

Pharmaceuticals, Mijo Stanic<br />

(2165-6 P) Using UPLC/MS/MS for Forced Degradation Studies and Impurity Profiling of<br />

Pharmaceuticals MIJO STANIC, Steiner Pharmaceuticals, Alexander H Schmidt<br />

(2165-7 P) Detection of Protein Heterogeneity by HPLC FUMIYA NAKATA, TOSOH Corporation,<br />

Toshito Kamichika, Atis Chakrabarti<br />

POSTER SESSION Session 2170<br />

All posters will be on display from 10:00 AM to 4:30 PM with authors present from 1:00 to 3:00 PM.<br />

Location of the posters is on the Exposition Floor – Blue Area, Aisles 3300-3500. The Exposition Floor<br />

opens at 9:00 AM.<br />

Pharmaceutical LC Techniques<br />

Wednesday Afternoon, Blue Area on Exposition Floor, Aisles 3300-3500<br />

(2170-1 P) The Use of Methyl-Cyclodextrin as a Mobile Phase Additive for the Reversed-<br />

Phase Chromatography of Pharmaceutically-Relevant Compounds JASON W<br />

COYM, University of South Alabama, Ariel S Armstrong, Shauna A Charlton<br />

(2170-2 P) Monitoring of Anions and Cations in Early Stage Product Formulation<br />

CHRISTOPHER CRAFTS, Thermo Fisher Scientific, Bruce A Bailey, Marc Plante, Ian Niel<br />

Acworth<br />

(2170-3 P) Synthesis and Characterization of Wider Bore Methacrylate-Based Polymeric<br />

Monolithic HPLC Columns NEIL D DANIELSON, Miami University, Fotouh R Mansour<br />

(2170-4 P) Eliminating Tedious Fraction Transfer of Natural Product in Low Concentration<br />

by Implementing Automated Fraction Pooling in a Semi-Preparative<br />

Environment of Lycopene in Various Tea Extracts via Flash Chromatography<br />

Using a Manual Purification System TONI R HOFHINE, Gilson, Inc., Seth Hanson<br />

(2170-5 P) HPTLC Method Development and Validation VIDHYA K BHUSARI, Poona College of<br />

Pharmacy, Sunil R Dhaneshwar<br />

(2170-6 P) Sensitive Quantitation of Genotoxic Impurities in Active Pharmaceutical<br />

Ingredients by LC-ICP-MS with Iodo Derivertization HARIGAYA KOKI, Mitsubishi<br />

Tanabe Pharma Corporation, Katsumata Tsunenobu<br />

(2170-7 P) HPLC Quantification of Aphidicolin in Different Extracts of the Endophytic<br />

Fungus Nigrospora Sphaerica ADRIANA A LOPES, FCFRP-USP, Keyller B Borges,<br />

Monica T Pupo<br />

(2170-8 P) Transfer of Methods in LC and UHPLC, What Calculations Do I Need? KEN<br />

BUTCHART, Fortis Technologies Ltd, Mark Woodruff<br />

(2170-9 P) Development of Chemically Modified Carbohydrate Based Chiral Stationary<br />

Phases to Improve Chiral Separations MATTHEW PRZYBYCIEL, ES Industries<br />

(2170-10 P) The Development and Application of Unique Stationary Phases for Sub 2 Micron<br />

HPLC Columns MATTHEW PRZYBYCIEL, ES Industries<br />

(2170-11 P) Development of Ion-Pairing HPLC Methods to Determine EDTA and DTPA in Two<br />

Pharmaceutical Formulations GEORGE WANG, Bristol-Myers Squibb, Frank<br />

Tomasella<br />

(2170-12 P) Development of a New HPLC Method for Characterization of Carbonyl<br />

Reductases in Biotransformation of Tobacco Specific Carcinogen NNK VLADIMIR<br />

WSOL, Charles University, Lucie Skarydova, Michaela Zverinova, Petr Solich<br />

PITTCON <strong>2012</strong> TECHNICAL PROGRAM<br />

(2170-13 P) Improving LC/MS Performance with UHPLC Columns ANNE MACK, Agilent<br />

Technologies, William J Long, Maureen Joseph, Jason Link<br />

(2170-14 P) Characterization of New Reversed Phase Columns Designed for Protein<br />

Separation Based on Wide Pore Silica Gel with C4 Phase YASUTOSHI KAWAI, Tosoh<br />

Corporation, Hiroyuki Yamasaki, Hiroyuki Moriyama<br />

(2170-15 P) Investigation of the Effect of 1-butyl -3-methyl Imidazolium Terafluoroborate<br />

Ionic Liquid on the Separation and Retention Behavior of Amitriptyline and<br />

Nortriptyline on Reversed Phase Liquid Chromatography TARIQ Z AHMAD,<br />

Western Illinois University, Sahar Salam, Tarab Ahmad, Azhar Alhejji<br />

(2170-16 P) The Effect of the Concentration of 1-butyl- 2, 3 Dimethylimadzolium<br />

Tetrafluoroborate Ionic Liquid as a Mobile Phase Additive on the Retention and<br />

Adsorption Behavior of Tryptophan KISHORE KUMAR R ALUGUVELLI, Western<br />

Illinois University, Tariq Z Ahmad, Azhar Alhejji, Tarab Ahmad<br />

(2170-17 P) The Effect of Counter Ions of 1-methy, 3-butyl Imidazolium Ionic Liquid as a<br />

Mobile Phase Additive on the Adsorption Behavior of Tryptophan on Reversed<br />

Phase Liquid Chromatography TARAB AHMAD, Western Illinois University, Azhar<br />

Alhejji, Tariq Z Ahmad, Kishore Kumar R Aluguvelli<br />

POSTER SESSION Session 2175<br />

All posters will be on display from 10:00 AM to 4:30 PM with authors present from 1:00 to 3:00 PM.<br />

Location of the posters is on the Exposition Floor – Blue Area, Aisles 3300-3500. The Exposition Floor<br />

opens at 9:00 AM.<br />

Samples and Sampling IV<br />

Wednesday Afternoon, Blue Area on Exposition Floor, Aisles 3300-3500<br />

(2175-1 P) Improving Standard N-Glycan Sample Preparation with Manual Automation<br />

Using Microchromatography to Improve Efficiency, Accuracy, and<br />

Reproducibility TONI R HOFHINE, Gilson, Inc.<br />

(2175-2 P) Automating Sample Preparation to Reduce Running Costs and Environmental<br />

Impact GAVIN J JONES, Biotage, Tobias Nordin<br />

(2175-3 P) Optimized Sample Preparation Using a Novel SPE Solution LUISA PEREIRA,<br />

Thermo Fisher Scientific, Ken Meadows, Tim Liddicoat, Mike Oliver<br />

(2175-4 P) Evaluation of a Biocide Release from a Paint Film – Application of Sorptive<br />

Stirring Bar Technique/HPLC for Marine Antifouling Paints BORIS POLANUYER,<br />

Dow Chemical, John Ashmore, David Laganella, Peter Y Eastman<br />

(2175-5 P) Automatic Sample Measurement in Karl Fischer Titration GEORGE PORTER,<br />

Metrohm USA, Birgit Faas, Andreas Trinkle, Michael Margreth<br />

(2175-6 P) A New QuECheRS Dispersive SPE Material and Method for Analysis of Veterinary<br />

Drug Residue by LC-MS-MS OLGA SHIMELIS, Supelco/Sigma-Aldrich, Michael Ye,<br />

Emily Barrey, Daniel Vitkuske<br />

CONFEREE NETWORKING<br />

Wednesday, March 14, <strong>2012</strong><br />

1:30 PM - 3:30 PM<br />

Analysis and Control of Genotoxic Impurities in Drug Development<br />

Facilitated by: Jane Li, Genentech and Shelly Li, Pfizer, Inc.<br />

Room 311E<br />

Application and Submission Process for SBIR and STTR NIH Grants<br />

Facilitated by: Erica Guice, Western Slope Laboratory and Yu (Woody) Lin, National Institute of Health<br />

Room 311G<br />

Chromatography Applications and Marketing in China<br />

Facilitated by: Perry Wang, US FDA<br />

Room 312B<br />

FDA Food Safety Modernization ACT - Product Testing and Preventive Controls<br />

Facilitated by: Carol Schneider, Alpha MOS, Inc.<br />

Room 311H<br />

Making the Most Out of Graduate School<br />

Facilitated by: Helen Boylan, Westminster College<br />

Room 312A<br />

Techniques and Methodologies for Direct Speciation<br />

Facilitated by: Manuel Valiente, Universitat Autonoma de Barcelona<br />

Room 311F<br />

Wednesday Afternoon<br />

89

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