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2012 Final Program - Pittcon

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PITTCON <strong>2012</strong> TECHNICAL PROGRAM<br />

Wednesday Afternoon<br />

POSTER SESSION Session 2140<br />

All posters will be on display from 10:00 AM to 4:30 PM with authors present from 1:00 PM to 3:00<br />

PM. Location of the posters is on the Exposition Floor – Red Area, Aisles 1300-1500. The Exposition<br />

Floor opens at 9:00 AM.<br />

LC-MS Applications<br />

Wednesday Afternoon, Red Area on Exposition Floor, Aisles 1300-1500<br />

(2140-1 P) Carbohydrate Analysis Using HPLC with PAD, FLD, CAD and MS Detectors<br />

BRUCE A BAILEY, Thermo Fisher Scientific, Paul Anthony Ullucci, Marc Plante,<br />

Christopher Crafts, Ian Niel Acworth, Rainer Bauder<br />

(2140-2 P) LC/MS/MS Determination of Taurine and Related Metabolites in Urine as<br />

Bladder Cancer Biomarkers SANJEEWA GAMAGEDARA, Missouri University of<br />

Science & Technology, Honglan Shi, Yinfa Ma<br />

(2140-3 P) NonenzymaticGlycation of Deoxy Guanosine Monophosphate (dGMP) by Methyl<br />

Glyoxal and Glucosamine: An In vitro Study of AGE Formation LASKER S LASKER,<br />

University of Rhode Island, Puneet S Gupta, Weixi Liu, Dain Joel<br />

(2140-4 P) Rapid Liquid Chromatography-Multistage Mass Spectrometry Neuropeptide<br />

Analysis Using Large Diameter Particulate Phase ZHOU YING, University of<br />

Michigan<br />

(2140-5 P) Repeatability Evaluation of a Liquid Chromatography (HILIC)-High Resolution<br />

TOF Mass Spectrometry System in Analysis of Biological Samples LI ZHANG, LECO<br />

Corporation, Xue Shi, Xiaoli Wei, Kevin Siek, Joe Binkley, Jeffrey S Patrick, Xiang Zhang<br />

(2140-7 P) Establishment of Chemical Warfare Agent Instrument and Method Detection<br />

Limits for Liquid Chromatography and Mass Spectrometer Instrumentation<br />

DONALD R GUSTAVSON, US Army, Benjamin J Hunt, Richard M Phan<br />

(2140-8 P) A Novel LC-MS Method For Sensitive Detection of Inorganic Azide by Employing<br />

a Strain Promoted Click Chemistry LIFANG WANG, Georgia State University,<br />

Chaofeng Dai, Weixuan Chen, Siming L Wang, Binghe Wang<br />

(2140-9 P) The Determination of Fruit Juice Authenticity Using High Resolution<br />

Chromatography, UV, Time of Flight MS and Multivariate Analysis ANTONIETTA<br />

GLEDHILL, Waters Corporation, Marian Twohig, Jennifer A Burgess, Dana Krueger<br />

(2140-10 P) Noise Removal from Deconvoluted Spectral Data for On-Line 2DLC-MS Top-<br />

Down Proteomics KAITLIN M FAGUE, University of North Carolina at Chapel Hill,<br />

Jordan T Stobaugh, James W Jorgenson, James R Parks<br />

(2140-11 P) Derivatization of Nitroaromatics for Trace Analysis by LCMS WU XINGHUA,<br />

Celgene Corporation, Leon Liang, Shan Shao, Feifei Tian, Dora Visky, Li Zhu, Lisa Fan,<br />

Ruimin Xie, Xiaolin Fu<br />

(2140-12 P) Analysis of Calcitriol in Plasma Using LC-MS/MS LUISA PEREIRA, Thermo Fisher<br />

Scientific, Kim Phipps, Joanna Denbigh, Tim Liddicoat, Stephen Westwood<br />

(2140-13 P) Simultaneous Quantification of 17-β-oestradiol and Oestrone in Human Plasma<br />

by Liquid Chromatography-Tandem Mass Spectrometry LUISA PEREIRA, Thermo<br />

Fisher Scientific, William Faulkner, Kim Phipps, Anthony Edge, Stephen Westwood,<br />

Kevin He<br />

(2140-14 P) A New Active Sampling Device for LC/MS Determination of Vapor Phase and<br />

Particulate Isocyanate Derivatives in Workplace Environments KRISTEN L<br />

SCHULTZ, Supelco/Sigma-Aldrich, Leonard Michael Sidisky, Jamie Brown, Gunner<br />

Skarping, Maryann Dalene, Daniel Karlsson<br />

(2140-15 P) Development of a UHPLC-MS/MS Method for the Measurement of<br />

Chlortetracycline Degradation in Swine Manure WEILIN L SHELVER, USDA, Vincent<br />

H Varel<br />

(2140-16 P) Quantitative Analysis of Drug Analytes in Rat and Human Plasma Using LC/MS<br />

with Online Sample Preparation GUIFENG JIANG, ThermoFisher Scientific, Terry<br />

Zhang, Kayvon Jalali<br />

(2140-17 P) Applying Japanese Pharmacopeia Purity Test Methods to Atrovastatin Calcium<br />

Hydrate Impurity Profiling Using 2D-LCMS-IT-TOF System ICHIRO HIRANO,<br />

Shimadzu Corporation, Tairo Ogura, Yusuke Inohana<br />

POSTER SESSION Session 2150<br />

All posters will be on display from 10:00 AM to 4:30 PM with authors present from 1:00 PM to 3:00<br />

PM. Location of the posters is on the Exposition Floor – Red Area, Aisles 1300-1500. The Exposition<br />

Floor opens at 9:00 AM.<br />

Mass Spectrometry II<br />

Wednesday Afternoon, Red Area on Exposition Floor, Aisles 1300-1500<br />

(2150-1 P) Analysis of Melamine Glycation Endproducts Using Matrix-Assisted Laser<br />

Desorption/Ionization Mass Spectrometry and Electrospray Ionization Mass<br />

Spectrometry WEIXI LIU, University of Rhode Island, Menashi Cohenford, Joel A Dain<br />

(2150-2 P) Atmospheric Pressure Gas Ionizer to Replace Radioactive Sources RICHARD L<br />

FINK, Applied Nanotech, Inc., Thuesen H Leif, Tikhonski Alexei<br />

(2150-3 P) The Development of an Ultra Low Noise Microchannel Plate Ion Detector<br />

SHARON MROTEK, Photonis USA, Bruce Laprade<br />

(2150-4 P) Proton-Transfer-Reaction Mass Spectrometry (PTR-MS) with Real-Time<br />

Nosespace Air Sampling - An Essential Tool for Food and Flavor Analysis LUKAS<br />

MAERK, IONICON Analytik, Christian Lindinger, Eugen Hartungen, Simone Juerschik,<br />

Philipp Sulzer, Alfons Jordan, Tilmann D Maerk<br />

(2150-5 P) Evaluating the Flowing Afterglow for Real Time Identification and<br />

Quantification of Multiple VOCs KATHRYN T MICKO, University of Pittsburgh, Joseph<br />

J Grabowski<br />

(2150-6 P) A New, Intuitive and User Friendly Software Platform with Optimized Analytical<br />

Workflow, Extended Functionality and Comprehensive Peripheral Control for<br />

ICP-Q-MS HOLGER JEGLINSKI, Thermo Fisher Scientific, Lothar Rottmann, Julian Wills,<br />

Meike Hamester<br />

(2150-7 P) Assignment of Molecular Formula in Extractable Testing by Software<br />

Enhancement of Unit Mass Data YIN LIU, Mannkind Corporation, John Cunningham,<br />

Baiba Cabovska, Sam Shum, Arthur Bailey<br />

(2150-8 P) Tetraalkyl Ammonium Bromides for the Standardization and Performance<br />

Evaluation of Thermal Desorption Ion Mobility Spectrometers LEONARD<br />

DEMORANVILLE, National Institute of Standards and Technology, Greg Gillen, Laurent<br />

Houssiau<br />

POSTER SESSION Session 2160<br />

All posters will be on display from 10:00 AM to 4:30 PM with authors present from 1:00 to 3:00 PM.<br />

Location of the posters is on the Exposition Floor – Blue Area, Aisles 3300-3500. The Exposition Floor<br />

opens at 9:00 AM.<br />

Pharmaceutical GC and/or MS II<br />

Wednesday Afternoon, Blue Area on Exposition Floor, Aisles 3300-3500<br />

(2160-1 P) Analysis of 2,4,6-tribromoanisole (TBA) and 2,4,6-tribromophenol (TBP) in<br />

Pharmaceutical Container Closure Systems Using GC-MS ERIC L SPAHLINGER,<br />

Catalent Pharma Solutions, James B Robb, III, James W Mclean, Tom N Feinberg, Alan D<br />

Hendricker<br />

(2160-3 P) Characterization and Identification of Essential Oils by GC-MS VIVEK R DHOLE,<br />

Thermo Fisher Scientific, Balasubramanian Sitharaman, Inderjit Kaur<br />

(2160-4 P) Detection and Quantification of Formaldehyde by Derivatisation with<br />

Pentafluorobenzylhydroxyl Amine in Pharmaceutical Excipients by GC-SHS-Mass<br />

Spectrometry PADMAJA PRABHU, PerkinElmer, Anil Nimkar, William Goodman<br />

(2160-5 P) USP 467: A Dynamic Headspace Approach to Reach Low Concentration Limits<br />

ILARIA FERRANTE, DANI Instruments SpA, Daniele Recenti, Manuela Bergna<br />

(2160-7 P) Residual Solvents USP - Problems and Solutions PETTER TOLLBACK,<br />

Syntagon AB, Magnus Ericsson<br />

(2160-8 P) A Sub-2µm Particle Supercritical Fluid Chromatography Coupled to Mass<br />

Spectrometry Method Development Strategy for Lipid Analysis MICHAEL D<br />

JONES, Waters Corporation, Giorgis M Isaac, Stephen McDonald<br />

88

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