2012 Final Program - Pittcon

10:15 (410-7) Therapeutic Monitoring of Tranexamic Acid Concentration in Patients
Undergoing Cardiac Surgery with the Use of Cardiopulmonary Bypass BARBARA
BOJKO, University of Waterloo, Marcin Wasowicz, Angela Jerath, Janusz Pawliszyn
10:35 (410-8) Investigation of the Adduct Formation of Mercury Species with Components of
Cell Culture Media by Means of HPLC/ESI-TOF-MS MIRIAM SCHWARZER, University
of Muenster, Imke Pieper, Rasmus Janzen, Michael Sperling, Tanja Schwerdtle, Uwe
Karst
ORAL SESSION Session 420
Liquid Chromatography
Monday Morning, Room 307C
Stephen Gozo, Celgene Corporation, Presiding
8:00 (420-1) Separation of Some Drugs by HPLC Using New Cross Linked Co-Polymer of
(Trietyl Amine Glyceryl Maleate) EMAAD TAHA BAKIR AL-TAKRITY, Tikrit University/
College of Science
8:20 (420-2) Systematic Method Development and Optimization in Reversed-Phase UPLC
APARNA CHAVALI, Waters Corporation, Thomas E Wheat, Patricia R McConville
8:40 (420-3) Transfer and Optimization of HPLC Methods to Superficially Porous UHPLC
WILLIAM J LONG, Agilent Technologies, Anne Mack, Maureen Joseph, Jason Link
9:00 (420-4) High Performance Toolbox Approach for HPLC Method Development LAWRENCE
Y LOO, Phenomenex Inc., Tivadar Farkas, Jason A Anspach, Mike Chitty, Jeff J Layne,
Thuylinh Tran
9:20 Recess
9:35 (420-5) Assessment of HILIC Mode and Stationary Phase for UHPLC/MS ANNE MACK,
Agilent Technologies, William J Long, Maureen Joseph, Jason Link
9:55 (420-6) Comparing Selectivity Rules for Core-Shell UHPLC Columns versus Fully Porous
Wide Pore Columns for Protein and Oligonucleotide Separations MICHAEL DAVID
MCGINLEY, Phenomenex Inc., Jeff J Layne, Daniel Brock
10:15 (420-7) Exploiting the Speed and Performance of Analytical Scale Commercial Silica
Monoliths Through an In Situ Modification Process ARIANNE SOLIVEN, University
of Western Sydney, Gary R Dennis, Georges Guiochon, Emily F Hilder, Ross Andrew
Shalliker
10:35 (420-8) Quality by Design (QbD) Approach to Rapid HPLC Method Development for
Pharmaceuticals Using Automated Screening and Design of Experiments (DOE)
CATHARINE JOHNSON, Boehringer Ingelheim, Shaun D Mendonsa
ORAL SESSION Session 430
Liquid Chromatography: Stationary Phase Architecture
Monday Morning, Room 311C
Richard A Henry, Supelco/Sigma-Aldrich, Presiding
8:00 (430-1) Characterization of Carbon-Modified Silicas for Analytical Liquid
Chromatography STEPHEN R GROSKREUTZ, Gustavus Adolphus College, Tuan Tran,
Dwight Stoll, Doug Fryer, Jon D Thompson
8:20 (430-2) Using Solvent-Particle Interactions to Predict Slurry Packing and Performance
of 1.2 µm Superficially Porous Particles Packed in Capillary Columns for Liquid
Chromatography LAURA BLUE, University of North Carolina, James W Jorgenson
8:40 (430-3) Performance Reproducibility of Chromatographic Columns Packed With Sub-3
Micron Core-Shell Particles FABRICE GRITTI, University of Tennessee - Knoxville
9:00 (430-4) Equivalency of Selectivity Plots for Porous and Superficially-Porous Particles
RICHARD A HENRY, Supelco/Sigma-Aldrich, Carmen T Santasania, David S Bell
9:20 Recess
9:35 (430-5) Comparison of Efficiencies of Diamond-Based Core-Shell Materials for HPLC
Made with Different Sizes of Nanodiamonds and Core Carbon Particles CHUAN-
HSI HUNG, Brigham Young University, Landon A Wiest, James M Christensen, Loryn K
Killpack, Robert C Davis, Michael A Vail, Andrew E Dadson, Matthew R Linford
9:55 (430-6) 1.2 µm Large Pore, Thin Shell, Superficially Porous Particles and Their
Chromatographic Performance in Capillary LC Columns JAMES W TREADWAY,
University of North Carolina at Chapel Hill, Laura Blue, James W Jorgenson
10:15 (430-7) Evaluations of Sub 2μm Nonporous Organosilica Hybrid Particles for LC
AMBER D MOORE, SUNY at Buffalo, Luis A Colon
10:35 (430-8) A High-Performance Specialty Column for Surfactant Analysis XIAODONG LIU,
Thermo Fisher Scientific, Mark Tracy, Christopher A Pohl
PITTCON 2012 TECHNICAL PROGRAM
ORAL SESSION Session 440
Microfluidics/Lab-on-a-Chip I- Bioanalytical
Monday Morning, Room 309A
X Nancy Xu, Old Dominion University, Presiding
8:00 (440-1) Flow-Valve Diagnostics for Label-Free, Point-of-Care Analyte Quantitation
DEBOLINA CHATTERJEE, Brigham Young University, Danielle S Mansfield, Neil
Anderson, Adam T Woolley
8:20 (440-2) Platform for Lock-In Detection Using Droplet Microfluidics as a Sample Chopper
to Achieve Nanomolar Absorbance Detection Limits KENNON DEAL, Auburn
University, Christopher J Easley
8:40 (440-3) Electrophoretic Separations in a Paper-PDMS Device CHRISTOPHER R HARRISON,
San Diego State University, Dylan Mitchell
9:00 (440-4) A Continuous-Flow Microfluidic Device for the Automated Preparation of Fatty
Acid Methyl Esters CINDY T DUONG, Florida State University, Michael G Roper
9:20 Recess
9:35 (440-5) Super-localization of Single Molecules and Nanoparticles in High-Fidelity
Optical Imaging Microfluidic Devices NING FANG, Iowa State University, Yong Luo,
Wei Sun
9:55 (440-6) Micellar Electrokinetic Chromatography of Oxidized Lipids in a Three-
Dimensional Polymeric Micro/Nanofluidic Device LARRY R GIBSON, University of
Notre Dame, Paul Bohn
10:15 (440-7) Rapid Prototyping in Polystyrene: Techniques to Produce High Throughput
Microfluidic Devices for the Monitoring of Cell-Cell Communication
STEPHEN T HALPIN, Michigan State University, Dana Spence
10:35 (440-8) Microfluidic Emulsion-Mediated Generation of Clonal Bead Populations
CHERYL J DEJOURNETTE, Auburn University, Christopher J Easley
ORAL SESSION Session 445
Sampling and Sample Preparation II
Monday Morning, Room 308D
Singh Manocha, The Pittsburgh Conference, Presiding
8:00 (445-1) Quantitative Analysis of Stearic Acid in Rubber Using Reactive Pyrolysis GC/MS
ATSUSHI WATANABE, Frontier Laboratories, Chu Watanabe, Robert Freeman
8:20 (445-2) In-vial Pyrolysis (PyroVial) with Pre- and Post - Sample Treatment Combined
with Different Separation Techniques BART TIENPONT, Research Institute for
Chromatography, Frank David, Pat Sandra
8:40 (445-3) High Efficient and Quantitatively Reproducible Protein Digestion by Trypsin-
Immobilized Magnetic Microspheres LIANGLIANG SUN, University of Notre Dame,
Yihan Li, Ping Yang, Guijie Zhu, Norman J Dovichi
9:00 (445-4) Optimization of Solid Phase Microextraction and Comprehensive Two-
Dimensional Gas Chromatography – Time-of-Flight Mass Spectrometry
Technique for High-Resolution Profiling of Plant Metabolites
SANJA RISTICEVIC, University of Waterloo, Janusz Pawliszyn
9:20 Recess
9:35 (445-5) Investigating Low Potency Assay Values for Film Coated Tablets
SHELLY XUE LI, Pfizer, Inc.
9:55 (445-6) Fully Automated Sample Preparation for Pharmaceuticals in Drinking Water
TOM DOBBS, J2 Scientific, Jessica Netzer, Jeff Wiseman
10:15 (445-7) Enhancing the Sensitivity for Trace-Level Analysis of Genotoxic Impurities Using
Polymeric Ionic Liquid-Based Coatings in Solid-Phase Microextraction
TIEN D HO, The University of Toledo, Mark Silver, Jared L Anderson
10:35 (445-8) Automated Sample Preparation for Tablet Content Uniformity and Assay Testing
MARC FINN, SOTAX Corporation, Robert Houser
Monday Morning
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