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Operating Manual - John Morris Scientific

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80<br />

40<br />

0<br />

160<br />

240<br />

320<br />

<strong>Operating</strong> <strong>Manual</strong><br />

Ultra-Low Refrigerated Circulators<br />

air cooled<br />

F81-HL<br />

F83-HL<br />

FP88-HL<br />

T<br />

ESC<br />

Sollwert 165.5°C<br />

ExternIst: 124.7°C<br />

Leistung: 50 %<br />

Regelung: intern<br />

1 2 3 F<br />

4 5 6<br />

7 8 9 0<br />

SL<br />

°C<br />

°C<br />

F95-SL<br />

FP88<br />

water cooled<br />

FW95-SL<br />

Software-version: V4.xx-xxxx<br />

Printed in Germany<br />

Changes without prior notification reserved<br />

1.951.2812 BE3 03/07<br />

Innovative Temperature Technology<br />

JULABO Labortechnik GmbH<br />

77960 Seelbach / Germany<br />

+49 (0) 7823 / 51-0<br />

+49 (0) 7823 / 24 91<br />

info@julabo.de<br />

www.julabo.de<br />

19512812.doc 27.03.07


Content<br />

Page<br />

<strong>Operating</strong> manual 2 ... 13<br />

<strong>Operating</strong> instructions 14 ... 80<br />

Congratulations!<br />

You have made an excellent choice.<br />

JULABO thanks you for the trust you have placed in us.<br />

This operating manual has been designed to help you gain an understanding of the principles of<br />

operating and possibilities of our circulators. For optimum utilization of all functions, we recommend<br />

that you thoroughly study this manual prior to beginning operation.<br />

Quality Management System<br />

ISO 9001<br />

2000<br />

c e<br />

W e<br />

r t<br />

i<br />

a r e<br />

f<br />

i e d<br />

The JULABO Quality Management System:<br />

Development, production and distribution of temperature application<br />

instruments for research and industries conform to the requirements according<br />

to DIN EN ISO 9001:2000.<br />

Certificate Registration No. 01 100044846<br />

Unpacking and checking<br />

Unpack the circulator and accessories and check for damages incurred during transit. These should be<br />

reported to the responsible carrier, railway, or postal authority, and a request for a damage report<br />

should be made. These instructions must be followed fully for us to guarantee our full support of your<br />

claim for protecting against loss from concealed damage. The form required for filing such a claim will<br />

be provided by the carrier.<br />

2


Ultra-Low Refrigerated Circulators<br />

TABLE OF CONTENTS<br />

<strong>Operating</strong> manual ................................................................................................................ 5<br />

Description ........................................................................................................................ 5<br />

Operator responsibility – Safety recommendations............................................................ 6<br />

EC Conformity................................................................................................................... 8<br />

Warranty conditions........................................................................................................... 9<br />

Technical specifications................................................................................................... 10<br />

<strong>Operating</strong> instructions........................................................................................................ 14<br />

1. <strong>Operating</strong> controls and functional elements ................................................................ 14<br />

2. Safety notes for the user............................................................................................. 17<br />

3. Preparations ............................................................................................................... 17<br />

3.1. Installation .............................................................................................................. 17<br />

3.2. Bath fluids .............................................................................................................. 18<br />

3.2.1. Tubing........................................................................................................... 19<br />

3.3. Filling / draining ...................................................................................................... 20<br />

3.4. Temperature application to external systems ......................................................... 22<br />

3.4.1. External control ............................................................................................. 23<br />

4. <strong>Operating</strong> procedures ................................................................................................. 24<br />

4.1. Power connection................................................................................................... 24<br />

4.2. Switching on / Selecting the language .................................................................... 24<br />

5. <strong>Manual</strong> operation ........................................................................................................ 25<br />

5.1. Start - Stop ............................................................................................................. 25<br />

5.2. Setting the temperatures .............................................................................. 26<br />

5.3. Safety installations, warning functions .......................................................... 27<br />

5.3.1. Early warning system, low level protection .................................................... 30<br />

6. Menu functions.................................................................................................. 31<br />

6.1. Configuration.......................................................................................................... 32<br />

6.2. Control ................................................................................................................... 36<br />

6.3. Start of a profile ...................................................................................................... 40<br />

6.3.1. Edit after start................................................................................................ 43<br />

6.3.2. Interrupting a profile ...................................................................................... 44<br />

6.3.3. Interruption after a power failure.................................................................... 44<br />

6.3.4. Termination of a profile.................................................................................. 45<br />

3


6.4. Integrated programmer – Generation II...................................................................46<br />

6.5. Analog inputs/outputs .............................................................................................49<br />

6.6. Limits ......................................................................................................................56<br />

6.7. Serial interface........................................................................................................58<br />

6.8. ATC Absolute Temperature Calibration, 3-point calibration.....................................59<br />

6.9. Setting the pump pressure......................................................................................62<br />

7. Troubleshooting guide / Error messages.....................................................................63<br />

8. Safety recommendations.............................................................................................67<br />

9. Electrical connections..................................................................................................68<br />

10. Remote control............................................................................................................71<br />

10.1. Setup for remote control .........................................................................................71<br />

10.2. Communication with a PC or a superordinated data system ...................................71<br />

10.3. List of commands....................................................................................................73<br />

10.4. Status messages ....................................................................................................76<br />

10.5. Error messages ......................................................................................................76<br />

11. JULABO Service – Online remote diagnosis ...............................................................78<br />

12. Installation of electronic module ..................................................................................79<br />

13. Maintaining the cooling performance...........................................................................79<br />

14. Cleaning / repairing the unit.........................................................................................80<br />

4


Ultra-Low Refrigerated Circulators<br />

<strong>Operating</strong> manual<br />

Description<br />

JULABO circulators have been designed for temperature application to specific fluids in a bath tank.<br />

The units provide pump nozzles for temperature application to an external system (loop circuit).<br />

The circulators are operated via the splash-proof keypad. The implemented<br />

microprocessor technology allows to set and to store different values that can be<br />

indicated on the VFD COMFORT-DISPLAY and LCD DIALOG-DISPLAY. Three<br />

menu keys facilitate adjusting setpoints, warning and safety functions and menu<br />

functions.<br />

The integrated programmer allows storing and running temperature and timedependent<br />

processes.<br />

ICC<br />

TCF<br />

ATC 3<br />

RS232<br />

RS485<br />

Pt100<br />

SMART<br />

PUMP<br />

The control electronics including “ICC - Intelligent Cascade Control“ automatically<br />

adapts the heat supplied to the thermal requirements of the bath.<br />

The TCF - Temperature Control Features allow the user to have access to all<br />

important temperature control parameters. This means: Full control on the control<br />

mode and the chance to manually adjust or adapt control to the specific application.<br />

Absolute Temperature Calibration (ATC3) provides a high temperature stability in<br />

the bath. With the 3-point calibration an offset is adjusted at three temperatures to<br />

ensure an accurate temperature pattern at the selected spot in the bath over the full<br />

temperature range.<br />

Electrical connections:<br />

The serial interface, switchable from RS232 to RS485, allows modern process<br />

technology without additional interface.<br />

Connection for Pt100 external sensor for external temperature measurement and<br />

control.<br />

Alarm output for external alarm message or control of JULABO refrigerating baths<br />

or solenoid valve (cooling water).<br />

The electronic module (option) provides 3 further analog connections (alarm input,<br />

standby input, recorder output, programmer input).<br />

The excess temperature protection conforming to IEC 61010-2-010 is a safety<br />

installation independent from the control circuit. This protection can be indicated<br />

and set on the LCD DIALOG-DISPLAY.<br />

The early warning system for low level signals that bath fluid needs to be refilled<br />

before the low level protection conforming to IEC 61010-2-010 causes a complete<br />

shut-down of the main functional elements.<br />

The pump capacity (electronically adjustable via the motor speed) enables to adapt<br />

to varying conditions for internal and external temperature applications.<br />

JULABO circulators are not conceived for direct temperature application to food and<br />

luxury articles or pharmaceutical and medico-technical products. Direct temperature<br />

application means: Unprotected contact of the object with the bath medium (bath fluid).<br />

5


<strong>Operating</strong> manual<br />

Operator responsibility – Safety recommendations<br />

The products of JULABO Labortechnik GmbH warrant a safe operation if installation, operation and<br />

maintenance is carried out according to common safety regulations. This section informs you about<br />

potential dangers that may arise from operating the circulator and also mentions the most important<br />

safety precautions.<br />

Persons:<br />

The operator is responsible for the qualification of the personnel operating the units.<br />

The operator should be constantly informed about the dangers involved with their job activities as well<br />

as preventive actions.<br />

Make sure all persons expected to carry out operation, installation and maintenance of the unit read<br />

and understand the safety information and operating instructions.<br />

When using hazardous materials, the circulator may only be operated by persons that are absolutely<br />

familiar with these materials and the circulator. These persons must be fully aware of possible risks.<br />

If you have any questions concerning the operation of your unit or the information in this manual,<br />

please contact us!<br />

Contact<br />

JULABO Labortechnik GmbH<br />

Eisenbahnstrasse 45<br />

77960 Seelbach / Germany<br />

+49 7823 51-0<br />

+49 7823 2491<br />

info@julabo.de<br />

www.julabo.de<br />

Handling:<br />

You received a product conceived for industrial use. Nevertheless, avoid strikes to the housing,<br />

vibrations, damages to the keypad foil (keys, display) or contamination.<br />

Make sure the product is regularly checked for proper condition. Regularly check (at least every<br />

2 years) the proper condition of the mandatory, warning, prohibition and safety labels.<br />

Take care that the mains supply features a low impedance to avoid any negative affects on the<br />

instrument being operated in the same mains.<br />

This unit is designed for operation in a controlled electromagnetic environment. This means that<br />

transmitting devices (e.g. cellular phones) should not be used in the immediate vicinity.<br />

Magnetic radiation may influence other units with components susceptible to magnetic fields<br />

(e.g. a monitor). We recommend to keep a minimum distance of 1 m.<br />

Permissible ambient temperature: max. 40 °C, min. 5 °C.<br />

Permissible relative air humidity: 50 % (40 °C).<br />

Do not store in an aggressive atmosphere. Protect from contaminations. Do not expose to sunlight.<br />

Operation:<br />

Only qualified personnel is authorized to perform configuration, installation, maintenance and repairs of<br />

the circulator.<br />

Routine operation can also be carried out by untrained personnel who should however be instructed by<br />

trained personnel. The summarized user guidance (short manual) and the specification table with<br />

information on individual parameters are sufficient for this.<br />

Use:<br />

The bath can be filled with flammable materials. Fire hazard!<br />

There might be chemical dangers depending on the bath medium used.<br />

Observe all warnings for the used materials (bath fluids) and the respective instructions (safety data<br />

6


Ultra-Low Refrigerated Circulators<br />

sheets).<br />

Insufficient ventilation may result in the formation of explosive mixtures. Only use the unit in well<br />

ventilated areas.<br />

Only use recommended materials (bath fluids). Only use non-acid and non corroding bath fluids.<br />

When using hazardous materials, the user must attach the enclosed safety labels to the front of the<br />

unit so they are well visible: The yellow warning label W09 (danger area) and the blue mandatory label<br />

M018 or Semi S1-0701 Table A1-2 #9 (Carefully read the user information prior to beginning<br />

operation).<br />

Warning label W09:<br />

Colors:<br />

yellow, black<br />

Mandatory label M018<br />

Colors: blue, white<br />

Danger area.<br />

Attention! Observe instructions.<br />

(operating manual, safety data sheet)<br />

Carefully read the user information prior to beginning<br />

operation<br />

Scope: EU<br />

Semi S1-0701<br />

Table A1-2 #9<br />

Carefully read the user information prior to beginning<br />

operation<br />

Scope: NAFTA<br />

Particular care and attention is necessary because of the wide operating range.<br />

There are thermal dangers: Burn, scald, hot steam, hot parts and surfaces that can be touched.<br />

Warning label W26:<br />

Colors: yellow, black<br />

Hot surface warning.<br />

(The label is put on by JULABO)<br />

Observe the instructions in the manuals for instruments of a different make that you connect to the<br />

circulator, particularly the respective safety recommendations. Also observe the pin assignment of<br />

plugs and technical specifications of the products.<br />

Disposal:<br />

The circulator contains a so-called back-up battery that supplies voltage to memory chips when the unit<br />

is switched off. Do not dispose of the battery in domestic waste!<br />

Depending on battery regulations in your country, you might be obliged to give back used or defect<br />

batteries to gathering places.<br />

The product may be used with oil as bath fluid. These oils fully or partially consist of mineral oil or<br />

synthetic oil. For disposal, observe the instructions in the safety data sheets.<br />

This unit contains the refrigerants R404A and R23 – at this time considered not to have any negative<br />

effects on the ozone layer. However, during the long operating period of the unit, disposal prescriptions<br />

may change. So only qualified personnel should take care of disposal.<br />

Valid in EU countries<br />

Directive 2002/96/EC of the European Parliament and of the Council of 27 January<br />

2003 on waste electrical and electronic equipment (WEEE).<br />

This directive requires electrical and electronic equipment marked with a crossedout<br />

trash can to be disposed of separately in an environmentally friendly manner.<br />

Contact an authorized waste management company in your country.<br />

Disposal with household waste (unsorted waste) or similar collections of municipal<br />

waste is not permitted!<br />

7


<strong>Operating</strong> manual<br />

EC Conformity<br />

The products described in the operating instructions conform to the requirements of<br />

the following European guidelines:<br />

Low voltage regulations with respect to legal harmonization of the member countries concerning<br />

electric devices for use within certain voltage limits.<br />

EMC guideline with respect to legal harmonization of the member countries concerning<br />

electromagnetic compatibility.<br />

JULABO Labortechnik GmbH<br />

Eisenbahnstr. 45<br />

77960 Seelbach / Germany<br />

8


Ultra-Low Refrigerated Circulators<br />

Warranty conditions<br />

JULABO Labortechnik GmbH warrants its products against defects in material or in workmanship,<br />

when used under appropriate conditions and in accordance with appropriate operating instructions<br />

for a period of ONE YEAR.<br />

Extension of the warranty period – free of charge<br />

With the ‘1PLUS warranty’ the user receives a free of charge extension to the warranty of up to 24<br />

months, limited to a maximum of 10 000 working hours.<br />

To apply for this extended warranty the user must register the unit on the JULABO web site<br />

www.julabo.de, indicating the serial no. The extended warranty will apply from the date of JULABO<br />

Labortechnik GmbH’s original invoice.<br />

JULABO Labortechnik GmbH reserves the right to decide the validity of any warranty claim. In case of<br />

faults arising either due to faulty materials or workmanship, parts will be repaired or replaced free of<br />

charge, or a new replacement unit will be supplied.<br />

Any other compensation claims are excluded from this guarantee.<br />

9


<strong>Operating</strong> manual<br />

Technical specifications<br />

F81-HL<br />

F83-HL<br />

Working temperature range °C -81 ... 100 -83 ... 50<br />

Temperature stability °C ±0,02 ±0,02<br />

Temperature selection<br />

digital<br />

via keypad<br />

indication on LCD DIALOG-DISPLAY (°C/°F)<br />

remote control via personal computer indication on monitor<br />

Temperature indication<br />

VFD COMFORT-DISPLAY (°C/°F)<br />

Resolution °C 0.01<br />

Absolute Temperature Calibration °C ±3<br />

Temperature control<br />

ICC - Intelligent Cascade Control<br />

Heater wattage (at 230 V) kW 1,3 1,3<br />

Cooling capacity °C +20 0 -20 -40 -60 -80 +20 0 -20 -40 -60 -80<br />

Medium ethanol kW 0.45 0.38 0.36 0.32 0.27 0.07 0.9 0.78 0.72 0.6 0.38 0.12<br />

Cooling compressor 2-stage 2-stage<br />

Refrigerant R404A/R23 R404A/R23<br />

Electronically adj. pump capacity stages 1 ... 4 1 ... 4<br />

Flow rate l/min at 0 bar 22 ... 26 22 ... 26<br />

Pressure max. bar at 0 liter 0.7 0.7<br />

Suction max bar at 0 liter 0.4 0.4<br />

Electrical connections:<br />

External alarm device 24-0 V DC / max. 25 mA<br />

Computer interface RS232 or RS485<br />

External Pt100 sensor<br />

Optional for HL and SL<br />

(Order No. 8900100 Electronic module with analog connections)<br />

Programmer input -100 °C to 400 °C = 0 - 10 V or 0 - 20 mA or 4 - 20 mA<br />

Input for the signal of a flow meter or external manipulated variable<br />

Temperature recorder outputs 0 - 10 V (0 V = -100 °C, 10 V = 400 °C)<br />

0 - 20 mA (0 mA = -100 °C, 20 mA = 400 °C)<br />

4 - 20 mA (4 mA = -100 °C, 20 mA = 400 °C)<br />

Standby input<br />

for external emergency switch-off<br />

Alarm output<br />

for external alarm signal<br />

Overall dimensions (WxDxH) cm 50x58x89 55x60x92<br />

Bath opening (WxL) cm 13x15 13x15<br />

Bath depth cm 16 16<br />

Filling volume liters 5 ... 6,5 5,5 ... 8<br />

Weight kg 88 118<br />

Ambient temperature °C 5 ... 40 5 ... 40<br />

Mains power connection V/ Hz 207-253 / 50-60 207-253 / 50<br />

230 V<br />

Current input (at 230 V) A 16 16<br />

Mains power connection V/ Hz<br />

207-253 / 60<br />

230 V/60 Hz<br />

Current input (at 230 V) A 16<br />

All measurements have been carried out at: rated voltage and frequency ambient temperature: 20 °C<br />

Technical changes without prior notification reserved.<br />

10


Ultra-Low Refrigerated Circulators<br />

FP88-HL<br />

Working temperature range °C -88 ... 100<br />

Temperature stability °C ±0.02<br />

Temperature selection<br />

digital<br />

via keypad<br />

indication on LCD DIALOG-DISPLAY (°C/°F)<br />

remote control via personal computer indication on monitor<br />

Temperature indication<br />

VFD COMFORT-DISPLAY (°C/°F)<br />

Resolution °C 0.01<br />

Absolute Temperature Calibration °C ±3<br />

Temperature control<br />

ICC - Intelligent Cascade Control<br />

Heater wattage (at 230 V) kW 1,3<br />

Cooling capacity °C +20 0 -20 -40 -60 -80<br />

Medium ethanol kW 1.1 0.96 0.92 0.73 0.59 0.15<br />

Cooling compressor<br />

2-stage<br />

Refrigerant<br />

R404A/R23<br />

Electronically adj. pump capacity stages 1 ... 4<br />

Flow rate l/min at 0 bar 22 ... 26<br />

Pressure max. bar at 0 liter 0.7<br />

Suction max bar at 0 liter 0.4<br />

Electrical connections:<br />

External alarm device 24-0 V DC / max. 25 mA<br />

Computer interface RS232 or RS485<br />

External Pt100 sensor<br />

Optional for HL and SL<br />

(Order No. 8900100 Electronic module with analog connections)<br />

Programmer input -100 °C to 400 °C = 0 - 10 V or 0 - 20 mA or 4 - 20 mA<br />

Input for the signal of a flow meter or external manipulated variable<br />

Temperature recorder outputs 0 - 10 V (0 V = -100 °C, 10 V = 400 °C)<br />

0 - 20 mA (0 mA = -100 °C, 20 mA = 400 °C)<br />

4 - 20 mA (4 mA = -100 °C, 20 mA = 400 °C)<br />

Standby input<br />

for external emergency switch-off<br />

Alarm output<br />

for external alarm signal<br />

Overall dimensions (WxDxH) cm 55x60x92<br />

Bath opening (WxL) cm 13x15<br />

Bath depth cm 16<br />

Filling volume liters 5,5 ... 8<br />

Weight kg 121<br />

Ambient temperature °C 5 ... 40<br />

Mains power connection V/ Hz 207-253 / 50<br />

230 V/50 Hz<br />

Current input (at 230 V) A 16<br />

Mains power connection V/ Hz 207-253 / 60<br />

230 V/60 Hz<br />

Current input (at 230 V) A 16<br />

All measurements have been carried out at: rated voltage and frequency ambient temperature: 20 °C<br />

Technical changes without prior notification reserved.<br />

11


<strong>Operating</strong> manual<br />

F95-SL<br />

FW95-SL (water cooled)<br />

Working temperature range °C -95 ... 0 -95 ... 0<br />

Temperature stability °C ±0,05 ±0,05<br />

Temperature selection<br />

digital<br />

via keypad<br />

indication on LCD DIALOG-DISPLAY (°C/°F)<br />

remote control via personal computer indication on monitor<br />

Temperature indication<br />

VFD COMFORT-DISPLAY (°C/°F)<br />

Resolution °C 0.01<br />

Absolute Temperature Calibration °C ±3<br />

Temperature control<br />

ICC - Intelligent Cascade Control<br />

Heater wattage (at 230 V) kW 3 3<br />

Cooling capacity °C 0 -20 -40 -60 -80<br />

Medium ethanol kW 2.0 1.9 1.65 1.20 0.36<br />

Cooling compressor 2-stage 2-stage<br />

Refrigerant R404A/R23 R404A/R23<br />

Electronically adj. pump capacity stages 1 ... 4 1 ... 4<br />

Flow rate l/min at 0 bar 22 ... 26 22 ... 26<br />

Pressure max. bar at 0 liter 0.7 0.7<br />

Suction max bar at 0 liter 0.4 0.4<br />

Electrical connections:<br />

External alarm device 24-0 V DC / max. 25 mA<br />

Computer interface RS232 or RS485<br />

External Pt100 sensor<br />

Optional for HL and SL<br />

(Order No. 8900100 Electronic module with analog connections)<br />

Programmer input -100 °C to 400 °C = 0 - 10 V or 0 - 20 mA or 4 - 20 mA<br />

Input for the signal of a flow meter or external manipulated variable<br />

Temperature recorder outputs 0 - 10 V (0 V = -100 °C, 10 V = 400 °C)<br />

0 - 20 mA (0 mA = -100 °C, 20 mA = 400 °C)<br />

4 - 20 mA (4 mA = -100 °C, 20 mA = 400 °C)<br />

Standby input<br />

for external emergency switch-off<br />

Alarm output<br />

for external alarm signal<br />

Overall dimensions (WxDxH) cm 59x76x116 59x76x116<br />

Bath opening cm 7 7<br />

Bath depth cm 20 20<br />

Filling volume liters 22 22<br />

Weight kg 214 214<br />

Ambient temperature °C 5 ... 40 5 ... 40<br />

Mains power connection V/ Hz 360-440/3Phases/ 50 360-440/3Phases / 50<br />

400 V/3P/50 Hz<br />

Current input (at 400 V) A 24 24<br />

Mains power connection V/ Hz 207-253/3Phases / 60 207-253/3Phases / 60<br />

230 V/3P/60 Hz<br />

Current input (at 230 V) A 28 24<br />

All measurements have been carried out at: rated voltage and frequency ambient temperature: 20 °C<br />

Technical changes without prior notification reserved.<br />

12


Ultra-Low Refrigerated Circulators<br />

Only for water-cooled models:<br />

Cooling water pressure (IN / OUT ) max. 6 bar<br />

Difference pressure (IN - OUT )<br />

3.5 to 6 bar<br />

Cooling water temperature


80<br />

40<br />

0<br />

160<br />

240<br />

320<br />

<strong>Operating</strong> instructions<br />

<strong>Operating</strong> instructions<br />

1. <strong>Operating</strong> controls and functional elements<br />

Front view<br />

2<br />

3<br />

4<br />

5<br />

T<br />

ES<br />

C<br />

Sollwert<br />

165.5°C ExternIst:<br />

124.7°C Leistung: 50<br />

%Regelung:<br />

intern<br />

1<br />

4<br />

7<br />

2<br />

5<br />

8<br />

3<br />

6<br />

F<br />

9 0<br />

°C<br />

°C<br />

HL<br />

1a<br />

6<br />

Rear view<br />

17a<br />

16a<br />

7 8 9a10 11 12<br />

ext<br />

Pt10<br />

0<br />

T16A<br />

T16A<br />

SERIA<br />

L<br />

REG<br />

+E-<br />

PROG<br />

ALAR STAND-<br />

M BY<br />

T1.25<br />

13<br />

14<br />

15<br />

21 22<br />

9<br />

1b<br />

19<br />

9b<br />

18<br />

FP88<br />

FPW<br />

24<br />

17b<br />

20<br />

1a<br />

1b<br />

Mains power switch, illuminated<br />

Mains power switch, illuminated<br />

for circulator<br />

for cooling machine<br />

2 VFD-COMFORT-DISPLAY<br />

14<br />

Header: Control indicators see sections 2.1 and 2.2<br />

Line 1: Actual valueinternal or external<br />

The display is depending on the selected control mode in the<br />

menu > Control < (internal or external).<br />

Line 2: Working temp. setpoint, constantly<br />

Line 3: Actual value (E = external or I = internal)<br />

Alternating with the display in line 1<br />

S xxx.xx<br />

Use the keys to indicate further values in line 3. However, the<br />

functions of these keys are different with the programmer started.<br />

PI Capacity in % - with manipulated variable set to >controlserialeprog


Ultra-Low Refrigerated Circulators<br />

H<br />

U<br />

F<br />

Heater capacity in Watts<br />

Mains voltage Volts<br />

Flow rate in liters/minute<br />

(providing EPROG input set to >FlowrateConfiguration> page 32<br />

2.1 Control indicators in the header:<br />

Heating / Cooling / Alarm /<br />

Remote control<br />

2.2 Control indicators in the header:<br />

Temperature indication Internal or External actual value<br />

Temperature indication in °C or °F (see page 36)<br />

2.3<br />

3<br />

Setpoint1: 150.00°C<br />

IntAct : 148.53°C<br />

Power : 80 %<br />

Control : intern<br />

RS232 : 150.00°C<br />

ExtAct : 145.30°C<br />

Power : 80 %<br />

Control : extern<br />

4 Keypad 1<br />

Display for the adjusted pump pressure stage in the -OFF- mode.<br />

Display for the effective pump pressure stage (rotation speed) after start.<br />

Four stages, adjustable via the<br />

LCD DIALOG-DISPLAY<br />

button, in the menu >PUMP


<strong>Operating</strong> controls and functional elements<br />

6 Adjustable excess temperature protection according to IEC 61010-2-010<br />

7<br />

8<br />

ext Pt100<br />

SERIAL<br />

Socket for external measurement and control sensor<br />

or external setpoint programming<br />

Interface RS232 / RS485: remote control via personal computer<br />

9 Socket: control cable of JULABO refrigerated circulator<br />

or output for alarm messages<br />

Option: Electronic module Order No. 8 900 100<br />

The circulator automatically recognizes the connected electronic module.<br />

10<br />

Alarm output (for external alarm signal)<br />

11<br />

12<br />

ALARM<br />

STAND-BY<br />

Standby input (for external emergency switch-off)<br />

Programmer input and temperature recorder output<br />

REG+E-PROG<br />

13 Connector for supplementary pump or solenoid valve<br />

230 V / max. 1.25 A<br />

No control voltage in the -OFF- condition<br />

14 Connector solenoid valve<br />

1. No control voltage in the -OFF- condition<br />

2. Configurable for controlled counter cooling via solenoid valve<br />

(only used with Heating Circulators)<br />

15 Fuses (for connectors 13, 14), T1.25A<br />

16a<br />

16b<br />

17a<br />

17b<br />

Mains fuses for circulator, T16A<br />

Mains fuses for cooling machine, T10A<br />

Mains power cable with plug for circulator<br />

Mains power cable with plug cooling machine<br />

18 F95, FW95 Built-in mains outlet for connection of circulator (230 V / 16 A)<br />

Built-in mains outlet 230 V / 6 A<br />

18 F81, F83, FP88 Built-in mains outlet for connection of circulator (230 V / 10 A)<br />

19 Drain port with drain tap<br />

20 Venting grid, removable<br />

21<br />

22 Pump connectors suction pump pressure pump<br />

OUT IN<br />

24<br />

Only for water cooled models: Cooling water OUTLET and INLET<br />

16


Ultra-Low Refrigerated Circulators<br />

2. Safety notes for the user<br />

In addition to the safety warnings listed above, warnings are posted throughout the<br />

manual. These warnings are designated by an exclamation mark inside an equilateral<br />

triangle. „Warning of a dangerous situation (Attention ! Please follow the documentation).“<br />

The danger is described according to an alarm keyword.<br />

Read and follow these important instructions.<br />

Warning:<br />

Describes a possibly highly dangerous situation.. If this is not avoided, serious injury and<br />

danger to life could result.<br />

Caution:<br />

Describes a possibly dangerous situation. If this is not avoided, slight or minor injuries<br />

could result. A warning of possible damage can also be contained in the text.<br />

Notice:<br />

Describes a possibly harmful situation. If this is not avoided, the product or anything in its<br />

surroundings can be damaged.<br />

3. Preparations<br />

3.1. Installation<br />

<br />

<br />

<br />

<br />

<br />

Place the unit on an even surface on a pad made of non-flammable material.<br />

The place of installation should be large enough and provide sufficient air<br />

ventilation to ensure the room does not warm up excessively because of the<br />

heat the instrument radiates to the environment. (Max. permissible ambient<br />

temperature: 40 °C).<br />

With regard to a disturbance in the cooling loop (leakage), the guideline EN<br />

378 prescribes a certain room space to be available for each kg of refrigerant.<br />

The necessary amount of refrigerant is specified on the type plate.<br />

> For 0.48 kg of refrigerant R404A, a room space of 1 m 3 is required.<br />

> For 0.68 kg of refrigerant R23, a room space of 1 m 3 is required.<br />

Keep at least 20 cm of open space on the front and rear venting grids.<br />

Do not set up the unit in the immediate vicinity of heat sources and do not<br />

expose to sun light<br />

Before operating the unit after transport, wait about one hour after setting it up.<br />

This will allow any oil that has accumulated laterally during transport to flow<br />

back down thus ensuring maximum cooling performance of the compressor.<br />

OUT<br />

IN<br />

G½"<br />

Only for water cooled models:<br />

Ensure circulation of cooling water by connecting the tubing to cooling water inlet<br />

and outlet on the rear of the refrigerated circulator.<br />

Cooling water connectors: G½"<br />

Cooling water see page 13<br />

17


Preparations<br />

3.2. Bath fluids<br />

Caution:<br />

Carefully read the safety data sheet of the bath fluid used, particularly with regard to<br />

the fire point!<br />

If a bath fluid with a fire point of 65 °C is used, only supervised operation is possible.<br />

Water:<br />

The quality of water depends on local conditions.<br />

Ferrous water can cause corrosion - even on stainless steel.<br />

Chloric water can cause pitting corrosion.<br />

Recommended bath fluids:<br />

Bath fluids Temperature range Flash point fire point<br />

water 5 °C ... 80 °C<br />

mixture water/glycol -30 °C bis 50 °C<br />

Thermal M +40 °C ... +170 °C >280 °C >305 °C<br />

Thermal H +20 °C ... +250 °C >270 °C >360 °C<br />

Thermal HY -80 °C ... +55 °C >75 °C >80 °C<br />

Thermal H5S -50 °C ... +105 °C >110 °C >130 °C<br />

Thermal H10S -20 °C ... +180 °C >175 °C >210 °C<br />

Thermal H20S +0 °C ... +220 °C >230 °C >270 °C<br />

Order No. 10 liters Bath fluids Order No. 5 liters<br />

8 940 100 Thermal M 8 940 101<br />

8 940 102 Thermal H 8 940 103<br />

8 940 104 Thermal HY 8 940 105<br />

8 940 106 Thermal H5S 8 940 107<br />

8 940 114 Thermal H10S 8 940 115<br />

8 940 108 ThermalH20S 8 940 109<br />

Notice:<br />

Please contact JULABO before using other than recommended bath fluids.<br />

JULABO takes no responsibility for damages caused by the selection of an unsuitable<br />

bath fluid.<br />

Unsuitable bath fluids are liquids which e.g.<br />

<br />

<br />

<br />

are very highly viscous<br />

(much higher than 70 mm 2 /s at the respective working temperature)<br />

have corrosive characteristics or<br />

tend to cracking.<br />

ATTENTION: The maximum permissible viscosity is 70 mm 2 /s .<br />

18


Caution:<br />

Ultra-Low Refrigerated Circulators<br />

The temperature controlling i.e. of fluids in a reactor constitutes normal circulator<br />

practice.<br />

We do not know which substances are contained within these vessels.<br />

Many substances are:<br />

<br />

<br />

inflammable, easily ignited or explosive<br />

hazardous to health<br />

environmentally unsafe<br />

i.e.: dangerous<br />

The user alone is responsible for the handling of these substances!<br />

The following questions shall help to recognize possible dangers and to reduce the<br />

risks to a minimum.<br />

<br />

<br />

<br />

Are all tubes and electrical cables connected and installed?<br />

Note:<br />

sharp edges, hot surfaces in operation, moving machine parts, etc.<br />

Do dangerous steams or gases arise when heating?<br />

Is an exhaust needed when working?<br />

What to do when a dangerous substance was spilled on or in the unit?<br />

Before starting to work, obtain information concerning the substance and<br />

determine the method of decontamination.<br />

3.2.1. Tubing<br />

Recommended tubing:<br />

Order No. Length Temperature range<br />

8930008 1 m CR ® tubing 8 mm inner dia. -20 °C to 120 °C<br />

8930012 1 m CR ® - tubing 12 mm inner dia. -20 °C bis 120 °C<br />

8930108 1 m Viton tubing 8 mm inner dia. -50 °C to 200 °C<br />

8930112 1 m Viton tubing 12 mm inner dia. -50 °C bis 200 °C<br />

8930410 1 m Insulation for tubing 8 mm inner dia. -50 °C bis 100 °C<br />

8930412 1 m Insulation for tubing 12 mm inner dia. -50 °C bis 100 °C<br />

8 930 209 0.5 m<br />

8 930 210 1.0 m<br />

8 930 211 1.5 m<br />

8 930 214 3.0 m<br />

8 930 220 0.5 m<br />

8 930 221 1.0 m<br />

8 930 222 1.5 m<br />

8 930 223 3.0 m<br />

Metal tubing, triple insulated, M16x1 -100 °C to +350 °C<br />

Metal tubing, insulated, M16x1 -50 °C to +200 °C<br />

19


Preparations<br />

Warning: Tubing:<br />

At high working temperatures the tubing used for temperature application and cooling<br />

water supply represents a danger source.<br />

A damaged tubing line may cause hot bath fluid to be pumped out within a short time.<br />

This may result in:<br />

Burning of skin<br />

Difficulties in breathing due to hot atmosphere<br />

Safety recommendations<br />

Employ suitable connecting tubing.<br />

Make sure that the tubing is securely attached.<br />

Avoid sharp bends in the tubing, and maintain a sufficient distance from<br />

surrounding walls.<br />

Regularly check the tubing for material defects (e.g. for cracks).<br />

Preventive maintenance: Replace the tubing from time to time.<br />

3.3. Filling / draining<br />

Filling<br />

Take care that no liquid enters the interior of the circulator.<br />

<br />

<br />

Recommended maximum filling level with water as bath fluid:<br />

30 mm below the tank rim<br />

Recommended maximum filling level with bath oils:<br />

40 mm below the tank rim<br />

After filling, immerse the samples in the bath or place the lid on the<br />

bath, in case the opening is not to be used.<br />

The circulator provides an early warning system for low level<br />

(description – please refer to page 30) that may be triggered when<br />

changing samples in the bath.<br />

Notice:<br />

Pay attention to the thermal expansion of bath oil during heating to avoid overflowing<br />

of the liquid.<br />

Exercise caution when emptying hot bath fluids!<br />

Check the temperature of the bath fluid prior to draining (by switching the unit on for<br />

a short moment, for example).<br />

Store and dispose the used bath fluid according to the laws for environmental<br />

protection.<br />

20


Ultra-Low Refrigerated Circulators<br />

Draining:<br />

<br />

<br />

<br />

<br />

The drain plug is located behind the venting grid on the front of<br />

the unit, which can be taken off by removing 4 screws.<br />

Slide a short piece of tube onto the drain port and hold it into a<br />

pail.<br />

Unscrew the drain tap and empty the unit completely.<br />

Tighten the drain tap.<br />

Penetration of ice flakes/water into bath oil<br />

At working temperatures below 0 °C humidity from the<br />

atmosphere may penetrate into bath oil through condensation.<br />

This may subsequently result in the formation of ice flakes,<br />

preventing the pump from proper operation.<br />

For this reason, the bottom of the bath tank provides a groove<br />

sloping down towards the drain tap. Thus water having<br />

penetrated into the bath oil gathers in the groove immediately<br />

behind the drain tap.<br />

Shut down the refrigerated circulator at a bath temperature of +10 °C.<br />

<br />

Wait for a while and open the drain tap to drain the water.<br />

21


Preparations<br />

3.4. Temperature application to external systems<br />

Temperature application to external, closed systems<br />

ext<br />

Pt100<br />

SERIAL ALARM STAND-BY REG+<br />

E-PROG<br />

The circulator is used for temperature application to external,<br />

closed systems (loop circuit) with simultaneous temperature<br />

application in the circulator bath.<br />

T16A<br />

T16A<br />

21 22<br />

T1.25A<br />

<br />

<br />

<br />

Unscrew the M16x1 collar nuts on the pump connectors with a<br />

19 mm (3/4“) wrench and remove the sealing disks. Using the<br />

collar nuts, screw on the tubing connection fittings (for tubing<br />

8 mm or 12 mm in diameter) delivered with the unit and tighten<br />

firmly. (Pressure pump: 22, suction pump: 21)<br />

Push on the tubings, and secure with tube clamps.<br />

Attach the tubing to the connectors of the external closed<br />

system, e.g., an instrument with a pressure-resistant<br />

temperature jacket or a temperature coil, and fasten with tube<br />

clamps to prevent slipping.<br />

Tubing see page 19<br />

Temperature application to external, open systems<br />

The circulator is equipped with both a pressure and suction pump<br />

for external temperature application in open systems.<br />

Differing flow rates of the pressure and suction pumps should be<br />

compensated. To maintain a constant liquid level, the JULABO<br />

„D+S“ Level Adapter is recommended for the external bath tank.<br />

The flow rate of the pressure pump will be then regulated by a<br />

built-in float device. The liquid level may be changed by a height<br />

adjustment on the „D+S“ Level Adapter.<br />

Accessory: „D+S“ Level Adapter Order No. 8 970 410<br />

S = Suction pump connection<br />

D = Pressure pump connection<br />

K = Float<br />

H = Height adjustment<br />

Important:<br />

The liquid level should be equal in the internal and external<br />

baths (absolute height).<br />

If you take out samples (for example Erlenmeyer flasks) from<br />

the external bath, turn the circulator off with the Start/Stop key.<br />

When working at temperatures below 0 °C and using the "D+S"<br />

Level Adapter do not use oil as the bath liquid. Condensing air<br />

will result in the formation of ice and thus affects the function of<br />

the float.<br />

Caution:<br />

Securely attach all tubing to prevent slipping.<br />

If the circulator is operated without external system, close the pump connector (22)<br />

with the cap nut.<br />

22


Ultra-Low Refrigerated Circulators<br />

Return flow safety device<br />

ext SERIAL ALARM STAND-BY REG+<br />

Pt100<br />

E-PROG<br />

T16A<br />

T16A<br />

T1.25A<br />

13<br />

14<br />

Inputs/Outputs<br />

>SV-Out : Backflow<br />

Chan.1 : xxxxxxx<br />

Chan.2 : xxxxxxx<br />

(see page 50)<br />

If the liquid levels in the circulator bath and the external<br />

system are at different heights, overflowing must be<br />

prevented after the power has been turned off.<br />

Flood hazard!<br />

For this reason, solenoid valves for loop circuit or shut-off<br />

valves can be integrated in the loop circuit.<br />

Connect the valve to the connector (13).<br />

If socket (14) is used:<br />

In menu >Inputs/Outputs< set the<br />

menu item >SV-Out< to >BackflowControl< (see page 36).<br />

IMPORTANT: Measures for external control<br />

For external control and temperature measurement an external<br />

Pt100 sensor must be connected to the socket (17) on the rear of the<br />

circulator.<br />

Order No. Description Material cable<br />

8 981 003 200 x 6 mm dia., stainless steel 1.5 m<br />

8 981 005 200 x 6 mm dia., glass 1.5 m<br />

8 981 006 20 x 2 mm dia., stainless steel 1.5 m<br />

8 981 010 300 x 6 mm dia., stainless steel 1.5 m<br />

8 981 013 600 x 6 mm dia., stainless steel/Teflon 3 m<br />

8 981 014 1200 x 6 mm dia., stainless steel/Teflon 3 m<br />

8981103 Extension cable for Pt100 sensor 3.5 m<br />

8 981 020 M+R in-line Pt100 sensor<br />

The M+R in-line Pt100 sensor is a flow sensor and can be installed in<br />

the loop circuit.<br />

Pt100<br />

M+R<br />

23


<strong>Operating</strong> procedures<br />

4. <strong>Operating</strong> procedures<br />

4.1. Power connection<br />

Caution:<br />

Only connect the unit to a power socket with earthing contact (PE – protective earth)!<br />

We disclaim all liability for damage caused by incorrect line voltages!<br />

Check to make sure that the line voltage matches the supply voltage<br />

specified on the identification plate. Deviations of ±10 % are permissible.<br />

<br />

<br />

<br />

Connect the circulator with mains power cable (17a) to the mains<br />

outlet (18).<br />

Connect the control cable (9) between the connectors (9a, 9b).<br />

Connect the refrigerated circulator with mains power cable (17b) to<br />

the mains socket.<br />

4.2. Switching on / Selecting the language<br />

1a<br />

1b<br />

Switching on:<br />

<br />

Circulator and cooling machine may be turned on and off with<br />

separate mains switches. The integrated control light will illuminate to<br />

indicate that power has been applied.<br />

**** JULABO ****<br />

*** HighTech ***<br />

** Circulator **<br />

* V4.xx-xxx *<br />

The unit performs a self-test.<br />

Then the software version (example: V 4.xx-xxxx) appears. The<br />

display „OFF“ or „R OFF“ indicates the unit is ready to operate.<br />

The circulator enters the operating mode activated before switching<br />

the circulator off:<br />

keypad control mode (manual operation) or<br />

remote control mode (operation via personal computer).<br />

-OFF-<br />

S 150.00<br />

I 24.60<br />

Configuration<br />

Off-Mode : pump off<br />

>Language : english<br />

Reset : no<br />

Selecting the language:<br />

There are two options for the language of the LCD DIALOG-DISPLAY:<br />

German or English. Select the desired language in the menu<br />

>Configuration< under the submenu >Language/SpracheLanguage/Sprache


Ultra-Low Refrigerated Circulators<br />

5. <strong>Manual</strong> operation<br />

5.1. Start - Stop<br />

24.60<br />

S 150.00<br />

E -----<br />

Setpoint1: 150.00°C<br />

IntAct : 24.60°C<br />

Power : 80 %<br />

Control : intern<br />

Start: Press the start/stop key .<br />

The actual bath temperature is displayed on the VFD COMFORT-<br />

DISPLAY.<br />

The LCD DIALOG-DISPLAY informs about adjustments and<br />

conditions on the circulator (see example on the left).<br />

Stop: Press the start/stop key .<br />

The VFD COMFORT-DISPLAY indicates the message „OFF“.<br />

Autostart: see chapter 6.1. Configuration<br />

The Autostart function enables the start of the circulator directly by<br />

pressing the mains switch or using a timer.<br />

Control of the cooling machine:<br />

With the mains switch (1b) turned on, the circulator automatically<br />

switches the cooling machine off and on.<br />

<br />

<br />

It is switched off, if:<br />

- the actual working temperature is increased by >30 °C (cooling is<br />

not required).<br />

- the heater operates at full power (>800 W) for longer than 5<br />

minutes.<br />

It is switched on, if:<br />

- cooling is necessary for maintaining the bath temperature.<br />

After switch-off, the cooling machine automatically switches on only<br />

after a delay of 5 minutes for protecting the cooling compressor.<br />

To save energy, turn off the cooling machine with the mains switch<br />

(1b) whenever cooling is not required.<br />

25


<strong>Manual</strong> operation<br />

5.2. Setting the temperatures<br />

Factory setting:<br />

Setpoints<br />

>Setpoint1: 20.00°C<br />

Setpoint2: 37.00°C<br />

Sezpoint3: 70.00°C<br />

Press the<br />

key to call up the menu for temperature selection.<br />

3 different working temperatures are adjustable. Their values are freely<br />

selectable within the operating temperature range.<br />

This setting may be carried out with the circulator being in the Start or<br />

Stop condition!<br />

Example: Setting working temperature „Setpoint 3“<br />

Setpoints<br />

Setpoint1: 20.00°C<br />

Setpoint2: 37.00°C<br />

>Setpoint3: 70.00°C<br />

Setpoints<br />

Setpoint1: 20.00°C<br />

Setpoint2: 37.00°C<br />

>Setpoint3: 85.00°C<br />

25.83<br />

S 85.00<br />

E -----<br />

1. Press the key.<br />

The LCD DIALOG-DISPLAY indicates the valid settings.<br />

2. Use the keys to select Setpoint 3.<br />

(One segment of the line blinks)<br />

Change the value to 85 °C.<br />

3. Use the numeral keypad to enter 8 and 5.<br />

Then press enter to store the value.<br />

The value remains visible on the LCD DIALOG-DISPLAY for about 10<br />

seconds, or press to update the display immediately.<br />

In the >Start< condition this value is immediately used for controlling the<br />

working temperature.<br />

The indication on the VFD COMFORT-DISPLAY is updated.<br />

The heater control indicator blinks.<br />

<br />

Notice: See SetMax: and SetMin:<br />

in chapter 6.6.Limits on page 56<br />

Example: Selecting the working temperature<br />

Press the key. Use the keys to select setpoint 1, 2 or 3<br />

and press enter .<br />

The circulator uses the new working temperature value for temperature<br />

control.<br />

26


Ultra-Low Refrigerated Circulators<br />

5.3. Safety installations, warning functions<br />

Settings for the excess temperature protection according to IEC 61010-2-010<br />

and for the high and low temperature warning functions are made<br />

in a menu that is called up with the key .<br />

ESC<br />

Safety-Values<br />

>Warn-Type: Warning /Alarm<br />

OverTemp: 85.00°C<br />

SubTemp : -99.99°C<br />

SafeTemp : 100.00°C<br />

SafeSens : xx.xx°C<br />

1<br />

80<br />

40<br />

0<br />

160<br />

240<br />

320<br />

°C°C<br />

Legend:<br />

1<br />

Setting via keypad<br />

Select parameter<br />

Select menu item<br />

Change menu level<br />

scroll down / scroll up<br />

1. Press the key<br />

The LCD DIALOG-DISPLAY shows the valid settings (see example above).<br />

2. Use the keys to select the menu item.<br />

3. Settings:<br />

Warn-Type: Select the parameter with the key<br />

enter<br />

(warning or alarm).<br />

and press<br />

Example:<br />

OverTemp and SubTemp: Use the numeral keypad to enter the value and<br />

press enter .<br />

SafeTemp: Set the new cut-out value using a screwdriver via the LCD<br />

DIALOG-DISPLAY. (Example: 50 °C)<br />

The value remains visible on the LCD DIALOG-DISPLAY for about 10<br />

seconds, or press<br />

to update the display immediately.<br />

27


<strong>Manual</strong> operation<br />

Recommendation:<br />

Set the excess temperature protection >SafeTemp< at 5 to 10 °C above the<br />

working temperature setpoint.<br />

Warning:<br />

The excess temperature protection >SafeTemp< should be set at least 25 °C below<br />

the fire point of the bath fluid used.<br />

In the event of wrong setting there is a fire hazard!<br />

We disclaim all liability for damage caused by wrong settings!<br />

Warn-Type: >Warning< or >Alarm<<br />

For the two menu items >OverTemp< and >SubTemp< choose between a<br />

warning message being signaled or a complete shutdown of the main<br />

functional elements such as heater and circulating pump being effected.<br />

OverTemperature: SubTemperature:<br />

If for a sensitive temperature application task adherence to a working<br />

temperature value >Setpoint< is to be supervised, then set high and low<br />

temperature warning values.<br />

In the example below, the >Setpoint< of 85 °C is surrounded by the values<br />

>OverTemp< 87 °C and >SubTemp< 83 °C. The electronics immediately<br />

registers when the actual temperature attains a temperature out of the<br />

limits and it follows a reaction according to what is set in the menu item<br />

>Warn-TypeWarning<<br />

An audible warning (interval tone)<br />

sounds and a meassage appears on<br />

the VFD COMFORT-DISPLAY.<br />

OverTemp SubTemp<br />

XXXXX<br />

WARNING<br />

CODE 03<br />

XXXXX<br />

WARNING<br />

CODE 04<br />

Warn-Type: >Alarm<<br />

A complete shutdown of heater and<br />

circulating pump is effected.<br />

An audible alarm (continuous tone)<br />

sounds and a message appears on the<br />

VFD COMFORT-DISPLAY.<br />

OverTemp SubTemp<br />

XXXXX<br />

ALARM<br />

CODE 03<br />

XXXXX<br />

ALARM<br />

CODE 04<br />

Press for help on the LCD.<br />

Actual temperature<br />

above high temperature<br />

value.<br />

Actual temperature<br />

below low temperature<br />

value.<br />

28


Ultra-Low Refrigerated Circulators<br />

Setpoint3 85.0°C<br />

OverTemp 87.0°C<br />

SubTemp 83.0°C<br />

The warning functions are only triggered when the actual bath temperature,<br />

after start from the „OFF“ or „rOFF“ mode, lies within the set limits for 3<br />

seconds.<br />

Setting range:<br />

20 °C ... 320 °C<br />

SafeTemperature: Indicated is the cut-out value set with a screwdriver on the<br />

excess temperature protection device.<br />

This safety installation is independent of the control circuit. When the<br />

temperature of the bath fluid has reached the safety temperature, a complete<br />

shutdown of the heater and pump is effected.<br />

The alarm is indicated by optical and audible signals (continuous tone).<br />

The following error message appears on the VFD COMFORT-DISPLAY:<br />

XXXXX<br />

ALARM<br />

CODE 14<br />

A L A R M !<br />

IntAct: 24.60°C<br />

Safety circuit alarm<br />

Press<br />

for help on the LCD<br />

Working temperature<br />

exceeds the adjusted<br />

safety temperature.<br />

<br />

SafeSens: Indicated is the temperature value of the safety sensor.<br />

29


<strong>Manual</strong> operation<br />

5.3.1. Early warning system, low level protection<br />

(patented)<br />

This low level protection is independent of the control circuit and is<br />

divided in two sections.<br />

1. Switch in stage 1 recognizes a critical fluid level .<br />

An audible warning (interval tone) sounds and a message<br />

appears on the VFD COMFORT-DISPLAY.<br />

Setpoint1: 150.00°C<br />

XXXXX<br />

WARNING<br />

CODE 40<br />

IntAct : 124.70°C<br />

Power : xx %<br />

Please Refill !!!<br />

Refill bath fluid!<br />

2. Switch in stage 2 recognizes a low fluid level .<br />

If stage 2 of the low level protection device (according to IEC<br />

61010-2-010) is triggered, a complete shutdown of the heater<br />

and circulating pump is effected.<br />

A continuous alarm tone sounds and a message >ALARM<<br />

>CODE 01< appears on the VFD COMFORT-DISPLAY.<br />

XXXXX<br />

ALARM<br />

CODE 01<br />

<br />

Insufficient liquid<br />

level or float is<br />

defective.<br />

Press<br />

Turn off the unit with the mains switch, refill bath fluid and turn<br />

the unit on again!<br />

3. Float<br />

4. Circulating pump<br />

5. Heater<br />

Warning:<br />

Important: Check the safety installations from time to time.<br />

See page 67.<br />

For refill always use the same bath fluid type that is already in the bath.<br />

Bath oils must not contain any water contaminants and should be pre-heated to the<br />

actual bath temperature! Explosion hazard at higher temperatures!<br />

30


Ultra-Low Refrigerated Circulators<br />

6. Menu functions<br />

The term „menu functions“ refers to adjustments such as<br />

<br />

<br />

<br />

<br />

<br />

<br />

<br />

<br />

<br />

Configuration of the circulator<br />

Internal and external control with adjustable control parameters<br />

Start menu for the integrated programmer<br />

Integrated programmer; 6 profiles with 60 sections each<br />

Configurable inputs and outputs; analog recorder outputs, input for external<br />

programmer or manipulated variable or flow rate<br />

Determination of limits for all important setting ranges and capacity<br />

variables<br />

Online communication, with adjustable interface parameters<br />

Absolute temperature calibration; sensor calibration<br />

Electronically adjustable pump capacity<br />

>Configuration<br />

Control<br />

Profile Start<br />

Int.Programmer<br />

Inputs/Outputs<br />

Limits<br />

Interface serial<br />

ATCalibration<br />

Pump<br />

ESC<br />

Legend<br />

1<br />

Setting via keypad<br />

Select parameter<br />

Select menu item<br />

Change menu level<br />

scroll down / scroll up<br />

1. If you press , use the keys to move in menu level 1.<br />

2. If the desired menu item is highlighted on the LCD DIALOG-DISPLAY (>),<br />

press enter to change to menu level 2.<br />

31


Menu functions<br />

6.1. Configuration<br />

>Configuration<br />

Control<br />

Profile Start<br />

Int.Programmer<br />

ESC<br />

ESC<br />

Configuration<br />

>Setpoint : keypad /RS232/ext.Pt100/eprog<br />

Autostart: off /on<br />

OFF-Mode : pump off /pump on<br />

Language : German /Englisch<br />

Reset : no /yes<br />

Variable : control /serial/eprog<br />

Unit : °C /°F<br />

1. Use the up/down keys to select the desired menu item.<br />

2. Use the left/right keys to select the parameter (parameter blinks).<br />

3. Press enter to store the new parameter.<br />

Setpoint<br />

The circulator provides four possibilities for setpoint setting. The selected mode<br />

is indicated in line 1 on the LCD DIALOG-DISPLAY.<br />

Setpoint1: 150.00°C<br />

IntAct : 148.53°C<br />

Power : 80 %<br />

Control : intern<br />

RS232 : 150.00°C<br />

ExtAct : 145.30°C<br />

Power : 80 %<br />

Control : extern<br />

R<br />

-OFF-<br />

S xxxx<br />

I xxxx<br />

Possible parameters:<br />

Keypad – Setpoint setting via keypad or via the integrated programmer.<br />

(factory setting)<br />

RS232 or RS485 - Setpoint setting via the serial RS232/RS485 interface (20)<br />

through a PC or superordinated data system.<br />

In the header of the VFD COMFORT-DISPLAY an „R“ illuminates. It<br />

indicates that remote control mode is set.<br />

Important:<br />

Connect the circulator to a PC using an interface cable.<br />

Check the interface parameters of both interfaces (on circulator and PC)<br />

and make sure they match.<br />

(see 10.1. Setup for remote control on page 71 )<br />

Pt100 : 150.00°C<br />

ExtAct : 145.30°C<br />

Power : 80 %<br />

Control : extern<br />

ext.Pt100 – Setpoint setting via the analog socket „ext. Pt100“ using an<br />

external temperature sensor or an appropriate voltage/current source.<br />

32


Ultra-Low Refrigerated Circulators<br />

eprog : 50.0°C<br />

IntAct : 24.7°C<br />

Power : 80 %<br />

Control : intern<br />

eprog – Can only be adjusted when an electronic module with analog<br />

connections is used (option).<br />

Setpoint setting via the analog interface REG+E-PROG through an external<br />

programmer.<br />

Important:<br />

Connect the external programmer to the circulator via the socket REG+E-<br />

PROG.<br />

In the menu >Inputs/Outputs< set the parameter >EPROG< and the input<br />

variables (see page 52).<br />

The E-Prog input can only be used either under menu item >Setpoint< or<br />

under menu item > Variable < (page 34).<br />

Autostart<br />

Possible parameters:<br />

on - AUTOSTART on<br />

off - AUTOSTART off (Factory setting)<br />

Note:<br />

The temperature system has been configured and supplied by JULABO<br />

according to N.A.M.U.R. recommendations. This means for the start mode, that<br />

the unit must enter a safe operating state after a power failure (non-automatic<br />

start mode). This safe operating state is indicated by „ OFF „, resp. R OFF on<br />

the VFD-COMFORT-DISPLAY. A complete shutdown of the main functional<br />

elements such as heater and circulating pump is effected simultaneously.<br />

The values set on the circulator remain stored, and the unit is returned to<br />

operation by pressing the start/stop key (in manual control mode).<br />

In remote control mode, the values need to be resent by the PC via the<br />

interface.<br />

Should such a safety standard not be required, the AUTOSTART function<br />

(automatic start mode) may be activated, thus allowing the start of the<br />

instrument directly by pressing the mains power switch or using a timer.<br />

The AUTOSTART function can only be used, if set point setting is carried<br />

out via >keyboard< or >eprog< or >ext. Pt100


Menu functions<br />

OFF-Mode<br />

Normally the circulating pump is switched via the start/stop signal. However, if<br />

circulation should be maintained also for the -OFF- condition, the parameter<br />

>pump on< needs to be set.<br />

Possible parameters:<br />

pump off (factory setting)<br />

pump on<br />

Language<br />

There are two options for the language of the LCD DIALOG-DISPLAY: German<br />

or English.<br />

Possible parameters:<br />

deutsch / englisch German / English<br />

Reset<br />

Use this to reset all values to factory setting (except date and time).<br />

Possible parameters:<br />

yes<br />

no (factory setting)<br />

Variable - actuating variable<br />

The variable corresponds to the extent to which the heater or cooling machine<br />

of the circulator is controlled. Heat or cold is applied to the bath according to<br />

this variable. If this happens with the control electronics of the circulator, called<br />

>control< in this particular case, the bath temperature is exactly heated and<br />

maintained constant at the adjusted set point.<br />

Programming of variables for the parameters > serial < or > eprog < is only<br />

accepted, if the unit is in Start mode.<br />

Possible parameters:<br />

control – The internal control electronics of the circulator controls the heater<br />

and cooling machine. Self-tuning is possible.<br />

serial – The heater or cooling machine receives the control signal via the serial<br />

interface. Self-tuning is not possible.<br />

eprog - The heater or cooling machine receives the control signal via the E-<br />

Prog input. Self-tuning is not possible. (option).<br />

ImportantImportant:<br />

Set the parameter >EPROG< and the input variables also in the menu<br />

>Inputs/Outputs< (see page 52).<br />

Note:<br />

The E-Prog input can only be used either under menu item >Setpoint<<br />

(page 32) or under menu item > Variable


Ultra-Low Refrigerated Circulators<br />

Warning:<br />

The working temperature range of the refrigerated circulator is determined during<br />

configuration. If set to >Control seriel < and > eprog serial< and >eprog<<br />

Start conditions:<br />

The external variable lies within the range –1 % to –100 %.<br />

<br />

<br />

Time limit:<br />

A 1-stage cooling machine produces cooling capacity after 5 minutes, a 2-stage<br />

cooling machine after 10 minutes.<br />

The indicator light illuminates only after this delay.<br />

This time delay after switch-off and switch-on of the cooling unit ensures protection<br />

of the cooling compressor.<br />

Temperature limit<br />

The bath temperature must be within the configured range (working temperature<br />

range) of the refrigerated circulator. If the temperature exceeds the maximum<br />

temperature, the compressor remains switched-off if cooling is requested. If the<br />

bath temperature falls below the configured temperature range, the compressor<br />

switches on and cold is applied to the bath after the time delay indicated above.<br />

Stop conditions:<br />

<br />

<br />

If the external variable is above 95 % (heating capacity) for more than 5 minutes,<br />

the cooling machine is switched off.<br />

Refrigerated circulators are configured to the effect that the compressor can only<br />

operate within a certain, limited temperature range. The compressor is switched off<br />

if the temperature exceeds the configured maximum temperature.<br />

Special conditions on FP88-HL<br />

If cooling is requested, the FP88 cooling machine changes the variable to the effective<br />

value within 100 seconds starting at 0 % (at –100 % this means –1 % per second).<br />

Only after this time is elapsed, cooling capacity is produced and the indicator light<br />

illuminates.<br />

If the variable is changed to the heating range (between 1 % to 100 %) within these<br />

100 seconds, then the time is set to 0 if cooling is requested again.<br />

35


Menu functions<br />

Example:<br />

Setpoints<br />

>Setpoint1: 20.00°C<br />

Setpoint2: 37.00°C<br />

Sezpoint3: 70.00°C<br />

°C °F <br />

Setpoints<br />

>Setpoint1: 68.00°F<br />

Setpoint2: 98.60°F<br />

Setpoint3: 158.00°F<br />

Unit<br />

Temperature values can be displayed in the unit °C or °F.<br />

With this change all adjusted temperature values are converted and displayed<br />

into the new unit.<br />

-OFF-<br />

S xxxx<br />

I xxxx<br />

°F Possible parameters:<br />

°C (factory setting)<br />

°F<br />

6.2. Control<br />

The circulator is conceived for internal and external temperature control.<br />

Switching is carried out in this submenu. Depending on what is set, only the<br />

respective set of parameters is indicated.<br />

Configuration<br />

>Control<br />

Profile Start<br />

Int. Programmer<br />

ESC<br />

ESC<br />

Control<br />

>ControlType: intern<br />

: Selftuning : once /always/off<br />

Dynamic : aperio /normal<br />

Xp : 1.0K<br />

Tn : 100s<br />

1<br />

Tv : 5s<br />

internal<br />

Control<br />

>ControlType: extern<br />

Selftuning: once /always/off<br />

CoSpeed : 0.0<br />

Xp : 0.7K<br />

Tn : 720s<br />

Tv : 55s<br />

Xpu : 5.0K<br />

external<br />

Example: 0.8<br />

1. Use the keys to select the menu item.<br />

2. With the keys select the parameter (parameter blinks)<br />

or<br />

use the numeral keypad to enter the numbers (number segment blinks).<br />

3. Press enter to store the new parameter or value.<br />

36


Ultra-Low Refrigerated Circulators<br />

-OFF-<br />

S xx.xx<br />

E xx.xx<br />

ControlType: Can only be adjusted in the -OFF- condition<br />

Possible parameters:<br />

intern internal temperature control<br />

extern external temperature control with external Pt100 sensor<br />

ext.<br />

Pt100<br />

IMPORTANT:<br />

Additional measures for external temperature control.<br />

Connect a Pt100 sensor to the socket on the rear of the circulator.<br />

Sensor calibration of the external Pt100 sensor is carried out in the menu<br />

>ATCalibration Status< set to >no< (see page 59).<br />

Suggested adjustments for external temperature control:<br />

AreaUp/ AreaDown and IntMax / IntMin<br />

see chapter >Limits< on page 56.<br />

External temperature control does not allow for setpoint setting via the<br />

socket „ext. Pt100“ (see page 32).<br />

Notice:<br />

Place the external sensor into the bath medium and securely fix the sensor.<br />

Selftuning:<br />

When performing an selftuning for the controlled system (temperature<br />

application system), the control parameters Xp, Tn and Tv are automatically<br />

determined and stored.<br />

Possible parameters:<br />

off - no selftuning.<br />

The control parameters ascertained during the last identification are used<br />

for control purposes.<br />

once – single selftuning (factory setting)<br />

The instrument performs a single selftuning of the controlled system after<br />

each start with the start/stop key or after receiving a start command<br />

via the interface.<br />

always – continual selftuning<br />

The instrument performs a selftuning of the controlled system whenever<br />

a new setpoint is to be reached.<br />

Use this setting only when the temperature application system changes<br />

permanently.<br />

37


Menu functions<br />

Dynamic:<br />

°C<br />

normal<br />

temp. stability<br />

This parameter affects the temperature pattern only in case<br />

of internal control.<br />

aperiodic<br />

Possible parameters:<br />

setpoint<br />

normal –Allows for reaching the setpoint faster, but<br />

overshooting of up to 5 % is possible.<br />

°C<br />

normal<br />

t<br />

Aperiodic – (factory setting)<br />

Target temperature is attained without overshooting.<br />

temp. stability<br />

aperiodic<br />

With both adjustments an adequate temperature<br />

stability is reached after approximately the same time.<br />

temperature ramp<br />

t<br />

CoSpeed:<br />

This parameter affects the temperature pattern only in case<br />

of external control.<br />

Possible parameters: 0 ... 5<br />

°C<br />

Int. temperature<br />

Ext. temperature<br />

5<br />

3<br />

0<br />

Setpoint<br />

t<br />

During selftuning, the control parameters Xp, Tn<br />

and Tv of a controlled system are automatically<br />

determined and stored. Depending on the<br />

controlled system, time for tuning can be<br />

unequally longer. This controller layout allows<br />

protection of sensitive objects requiring<br />

temperature application.<br />

As soon as a co-speed factor is set, it is<br />

considered for calculating the control parameters.<br />

As shown in the diagram, tuning times become<br />

shorter the higher the co-speed factor is, but<br />

overshooting can happen in the internal system.<br />

Control parameters – intern / extern<br />

The control parameters preset in factory are in most cases adequate for<br />

achieving an optimum temperature pattern for the samples requiring<br />

temperature application.<br />

Each parameter may be manually set via the keypad if necessary, to allow<br />

optimum control performance.<br />

Setting range:<br />

internal / external<br />

0.1 ... 99.9 K<br />

Proportional range >Xp<<br />

The proportional range is the range below the selected temperature value in<br />

which the control circuit reduces the heating power from 100 % to 0 %.<br />

38


Ultra-Low Refrigerated Circulators<br />

Setting range:<br />

internal / external<br />

3 ...9999 s<br />

Resetting time >Tn< (Integral component)<br />

Compensation of the remaining control deviation due to proportional<br />

regulation. An insufficient resetting time may cause instabilities to occur.<br />

Excessive resetting time will unnecessarily prolong compensation of the<br />

control difference.<br />

Setting range:<br />

internal / external<br />

0 ... 999 s<br />

Lead time >Tv< (Differential component)<br />

The differential component reduces the control settling time. An insufficient<br />

lead time will prolong the time required to compensate for disturbance effects<br />

and cause high overshooting during run-up. An excessive lead time could<br />

cause instabilities (oscillations) to occur.<br />

Setting range:<br />

0.1 ... 99.9 K<br />

Proportional range >Xpu<<br />

The proportional range Xpu of the cascaded controller is only needed for<br />

external control.<br />

Optimization instructions for the PID control parameters:<br />

°C<br />

optimum setting<br />

The heat-up curve reveals inappropriate control<br />

settings.<br />

°C<br />

t<br />

Inappropriate settings may produce the following heat-up curves:<br />

Xp too low<br />

Tv/Tn too low<br />

°C<br />

t<br />

t<br />

°C<br />

Xp too high or Tv too high<br />

°C<br />

Tv/Tn too high or Xp too high<br />

t<br />

t<br />

39


Menu functions<br />

6.3. Start of a profile<br />

The start menu of the integrated programmer allows calling up and defined<br />

starting of one of six previously stored temperature profiles. The profiles are<br />

started manually or via the integrated timer.<br />

Configuration<br />

Control<br />

>Profile Start<br />

Int.Programmer<br />

ESC<br />

ESC<br />

>Start Profile 0<br />

at Step 0 1<br />

Runs 1<br />

Profile End Stdby /SetpPG/Setp 1/Setp 2/Setp 3<br />

Start no /yes/time<br />

>hour.min 11:15<br />

Day.Mon 11.12 1<br />

Year 2004<br />

Start no /yes<br />

Example: 11:15<br />

1. Use the keys to select the menu item.<br />

2. With the keys select the parameter (parameter blinks)<br />

or<br />

use the numeral keypad to enter the numbers (number segment blinks).<br />

3. Press enter to store the new parameter or value.<br />

If the parameter time is selected, a further submenu opens for setting the<br />

start time.<br />

Possible parameters:<br />

Start Profile 0 to 5<br />

Select the profile that should be started.<br />

at Step 0 to 60.<br />

Select the section with which the profile should be started.<br />

Runs 0 to 99<br />

Select the number of profile repetitions.<br />

Start<br />

no / yes (manual start)<br />

or<br />

time (via integrated timer)<br />

40


Ultra-Low Refrigerated Circulators<br />

Profile End Stdby / SetpPG / Setp 1 / Setp 2 / Setp 3<br />

This parameter is used to determine if the unit switches to the -OFFcondition<br />

at the end of a profile, or if temperature control is continued<br />

and the working temperature setpoint that is be used in such case.<br />

Examples:<br />

-OFF-<br />

S 25.00<br />

E -----<br />

Setpoint3: 80.00°C<br />

IntAct : 80.00°C<br />

Power : 2%<br />

Control : intern<br />

Setpoint<br />

Setpoint1: 25.00°C<br />

>Setpoint2: 58.00°C<br />

Setpoint3: 85.00°C<br />

Setpoint2: 58.00°C<br />

IntAct : 60.00°C<br />

Power : 0%<br />

Control : intern<br />

60.00<br />

S 58.00<br />

E -----<br />

Start<br />

Stdby – If the end of the profile is reached, the circulator switches to<br />

the -OFF- condition. The VFD display indicates the working<br />

temperature setpoint, that was displayed in line 2 already before the<br />

program was started (example: S 25.00 °C ).<br />

SetpPG – (Setpoint of the ProGrammer) At the end of the profile, the<br />

setpoint of the last program section is written to the position of<br />

setpoint 3 (example: 80.00 °C) and indicated in line 1 of the LCD<br />

display. The circulator operates and controls this temperature until<br />

the Start/Stop key<br />

is pressed or a new profile is started.<br />

Setp 1, Setp 2, Setp 3 – („Setp“ short for Setpoint)<br />

Before starting the programmer, a temperature value is set for one of<br />

the three setpoints in the menu.<br />

(example: Setpoint 2 58.00 °C)<br />

The circulator operates and controls this temperature at the end of<br />

the profile until the Start/Stop key<br />

is started.<br />

no / yes (manual start)<br />

or<br />

time (via integrated timer)<br />

is pressed or a new profile<br />

When selecting the parameter time, a new submenu is called up for entry of<br />

the start time.<br />

A flashing segment indicates that a start time needs to be entered.<br />

hour.min<br />

Start time<br />

Day.Mon<br />

day and month<br />

Year<br />

year<br />

Set each entry with enter .<br />

Start no / yes<br />

A flashing line indicates that the parameter „yes“ needs to be entered.<br />

Press the key to select the parameter and press enter .<br />

Starttime: 06:00<br />

Date : 15:12<br />

*** wait ***<br />

Acttime 02:34:45<br />

The temperature system switches to waiting mode and a flashing line<br />

„wait“ appears on the LCD DIALOG-DISPLAY. The start time and actual<br />

time are permanently indicated on the display.<br />

41


Menu functions<br />

Examples:<br />

Setp. : 125.8°C<br />

IntAct: 124.7°C<br />

Prof. : 4 Step: 12<br />

Remain: 00:03:45<br />

Setp. : 125.8°C<br />

IntAct: 124.7°C<br />

Prof. : 4 Step: 12<br />

All : 00:03:45<br />

Setpoint : 125.8°C<br />

IntAct : 124.7°C<br />

Prof : 4 Step:12<br />

S12:150:00 h:m 01:10<br />

>Edit Profile: 4<br />

Step: 12<br />

Setp: 150.00°C<br />

Time [hh:mm] 01:10<br />

Indication after successful start:<br />

The started programmer displays the actually calculated setpoint in line<br />

1. The value changes until the final temperature of the section is reached<br />

(temperature ramp).<br />

1 st line: Setpoint of the programmer<br />

2 nd line: Actual temperature value<br />

at internal control = IntAct:<br />

at external control = ExtAct:<br />

xxx.xx<br />

xxx.xx<br />

3 rd line: Selected profile and the actual section (step).<br />

4 th line: With the keys the following information can be<br />

displayed in line 4.<br />

<br />

<br />

Remaining time of the actual section (standard display)<br />

Remaining total time: Profile x number of repetitions<br />

(All: Days/hours:minutes:seconds)<br />

Particularitys:<br />

1. If a total time of more than 999 days is calculated, only the hours<br />

are displayed on the unit.<br />

(All: hours:minutes:seconds)<br />

2. If the time period of a section is edited after start, then the<br />

remaining total time can no longer be displayed.<br />

<br />

The data of a section as stored under „Edit Profile“.<br />

Use the keys to successively indicate the sections of a<br />

profile. Unused sections or incorrect data are skipped.<br />

42


Ultra-Low Refrigerated Circulators<br />

6.3.1. Edit after start<br />

A JULABO programmer of generation II allows editing of a running<br />

profile. A programmer of the previous generation requested the profile to<br />

be interrupted, edited and then started again.<br />

>Edit Profile: 1<br />

Step: 6<br />

Setp: 100.00°C<br />

Time [hh:mm] 01:05<br />

Start and quit the edit mode:<br />

After start, press the key to enter the submenu „Edit Profile“.<br />

Press to quit the edit mode.<br />

Deleting a complete section:<br />

Use the keys to move to line 2.<br />

Use the keys to choose the desired section.<br />

Press the key to delete the complete section.<br />

>Edit Profile: 1<br />

**Step is deleted **<br />

Setp: °C<br />

Time [hh:mm]<br />

>Edit Profile: 1<br />

** Step is active **<br />

Setp: 100.00°C<br />

Time [hh:mm] 01:05<br />

If the desired section is already chosen, the section is deleted even if<br />

the cursor > is in line 1, 3 or 4.<br />

Deletion is indicated in the respective line of the LCD display:<br />

** Step is deleted **<br />

The section that is currently processed cannot be deleted. If you still<br />

try it, the message ** Step is active ** appears on the<br />

LCD display.<br />

Changing a section:<br />

The values in lines 3 and 4 can be changed, even on the section that<br />

is currently processed.<br />

In the input window, select the menu item with the keys .<br />

Use the numeral keypad to enter the numbers and press enter .<br />

Edit Profile: 1<br />

Step: 6<br />

>Setp: 83.00°C<br />

time [hh:mm] 01:25<br />

Examples:<br />

Setpoint: target temperature 83 °C<br />

Time time period 1 hour:25 minutes<br />

Particularity for changes in a section that is currently in process.<br />

If the target temperature is changed, the slope of the ramp is<br />

automatically calculated on basis of the remaining time of the<br />

section.<br />

If the time period is changed, the slope of the ramp is automatically<br />

calculated on basis of the new total time of the section.<br />

The „remaining total time“ (Profile x number of repetitions) as<br />

described on page 42 can no longer be displayed.<br />

43


Menu functions<br />

6.3.2. Interrupting a profile<br />

Setp. : 125.80°C<br />

IntAct: 124.70°C<br />

Prof. : 4 Step:12<br />

*** pause ***<br />

Press the start/stop key to interrupt or continue a profile.<br />

The setpoint and time period set for the corresponding section are<br />

thus stopped at the values presently achieved.<br />

The instrument is put on hold and the message „pause“ flashes on<br />

the LCD DIALOG DISPLAY.<br />

STAND-BY<br />

Setp. : xxx.xx°C<br />

IntAct: xxx.xx°C<br />

Prof. : 4 Step:12<br />

*** STAND-BY ***<br />

A profile can be interrupted or restarted by an external emergency<br />

shut-off.<br />

Important:<br />

For this, in the menu >Inputs/Outputs< the menu item >Ext. StBy <<br />

must be set to >activ< (see page 54)<br />

and in the menu >Configuration< >Autostart< needs to be set (see<br />

page 33).<br />

Setpoint control and timer are interrupted by breaking the contact<br />

„AK”.<br />

The instrument is put on hold and the message „Stand-By“ flashes on<br />

the LCD DIALOG-DISPLAY.<br />

Notice: This is not an actual emergency switch-off.<br />

Warning:<br />

Following a power interruption, it would be possible in this condition for the instrument<br />

to restart automatically. The safety and warning functions of the instrument should<br />

always be used to their fullest capacity.<br />

See Warning page 33.<br />

6.3.3. Interruption after a power failure<br />

There is every possibility to operate the programmer safe to power<br />

failures.<br />

Important:<br />

For this in the menu >Configuration< >Autostart< needs to be set (see<br />

page 33).<br />

Starttime: 06:00<br />

Date : 15:12<br />

*** wait ***<br />

Acttime 02:34:45<br />

If the AUTOSTART function is activated, the programmer starts again<br />

at a point approx. 20 seconds before the interruption took place.<br />

However, an uncontrolled change of the bath temperature happened.<br />

Power failure when the instrument is on hold if start is effected via the<br />

built-in timer:<br />

If the starting time is not yet reached, the programmer is put on hold<br />

again.<br />

If the starting time is exceeded, the programmer starts immediately.<br />

44


Ultra-Low Refrigerated Circulators<br />

6.3.4. Termination of a profile<br />

Setp : 125.80°C<br />

IntAct: 124.70°C<br />

Prof. : 4 Step:12<br />

Remain: 00:03:45<br />

<br />

>Start Profile x<br />

at Step<br />

x<br />

Runs 1<br />

Start<br />

no<br />

A profile can be terminated by pressing<br />

switches back to the Start menu.<br />

Press again to quit the menu<br />

or<br />

use the keys to remain in the Start menu.<br />

. The programmer<br />

The start of another temperature profile can now be prepared if<br />

necessary.<br />

Examples:<br />

Setpoint1: 150.00°C<br />

IntAct : 83.24°C<br />

Power : 0 %<br />

Control : intern<br />

-OFF-<br />

S 150.00<br />

E -----<br />

Interruption after a power failure<br />

In case of a power failure, the reaction of the circulator is the same as<br />

when switched off and on again with the mains switch.<br />

The LCD DIALOG-DISPLAY gives information on the adjustments and<br />

conditions of the circulator.<br />

The VFD COMFORT-DISPLAY indicates "OFF".<br />

45


Menu functions<br />

6.4. Integrated programmer – Generation II<br />

The integrated programmer allows any desired temperature program<br />

sequences to be realized. Such a temperature sequence is called profile. A<br />

profile consists of individual sections defined by duration (t:) and target<br />

temperature. Target temperature is the setpoint (T:), that is achieved at the end<br />

of a section. The programmer uses time and temperature difference values<br />

within a section to calculate a temperature ramp.<br />

Profile Start<br />

>Int. Programmer<br />

Inputs/Outputs<br />

Limits<br />

ESC<br />

ESC<br />

Int. Programmer<br />

>Edit<br />

Delete<br />

Print<br />

Set Clock<br />

>Edit Profile: 0<br />

Step: 0<br />

Setp: °C<br />

Time [hh:mm]<br />

1<br />

ESC<br />

>Delete Prof. 0<br />

from Step 0 1<br />

to Step 60<br />

delete no /yes<br />

>Print Profile 0<br />

Print<br />

yes /no<br />

1<br />

>hour.min 14:24<br />

Day.Mon 07.12<br />

Year 2003<br />

09:27:36<br />

1<br />

1. Use the keys to select the desired menu item in menu level 2<br />

on the LCD DIALOG-DISPLAY (>) and press enter to change to menu<br />

level 3. An input window opens for each menu item.<br />

2. In the input window, select the menu item with the keys .<br />

3. Use the keys to select the parameter (parameter blinks)<br />

or<br />

use the numeral keypad to enter the numbers (number segment blinks).<br />

4. Press enter to store the new parameter or value.<br />

46


Int. Programmer<br />

>Edit<br />

Delete<br />

Print<br />

Set Clock<br />

Edit<br />

Important:<br />

Delete<br />

Print<br />

Set clock<br />

Compile profiles<br />

Display sections<br />

Also a running profile can be changed.<br />

See „Edit after start“ page 43<br />

Delete sections<br />

Print a programmed profile<br />

Ultra-Low Refrigerated Circulators<br />

Set the real time on the instrument<br />

Compile profiles:<br />

A flashing segment indicates that a number needs to be entered.<br />

Under submenu „Edit Profile“ enter a profile number.<br />

Six profiles may be stored (nos. 0 to 5).<br />

Example:<br />

>Edit Profile: 1<br />

Step: 6<br />

Setp: 100.00°C<br />

Time [hh:mm] 01:05<br />

Edit Profil:<br />

Profile No.1<br />

Then programme the desired values for each section.<br />

Use the keypad to set section number, target temperature and time<br />

period. Set each entry with enter .<br />

Step: Section No. 6<br />

Setpoint: target temperature - 100 °C<br />

Time<br />

time period - 1 h:05 minutes<br />

When the program is running, only sections having complete information<br />

for target temperature and time period are considered.<br />

It makes sense, to leave out section numbers in the profile, in order to<br />

use them later for corrections in the profile<br />

Important:<br />

If a time of 00:00 is set for a profile, the profile is continued with the next<br />

section only after the setpoint temperature (±0.2 °C) is reached.<br />

Example:<br />

Step (No.) 1 3 5 6 9 11 14<br />

Setpoint (°C) 50 50 100 100 80 80 20<br />

Time (h.m) 00:08 00.02 00:10 01:05 00:10 00:05 00:30<br />

47


Menu functions<br />

>Edit Profile: 1<br />

Step: 3<br />

Setp: 50.00°C<br />

Time [hh:mm] 00:02<br />

Example:<br />

>Delete Prof. 4<br />

from Step<br />

to Step<br />

8<br />

34<br />

delete<br />

yes<br />

<br />

>Delete Prof.<br />

from Step<br />

4<br />

8<br />

to Step 34<br />

****** delete ******<br />

Display sections (Step):<br />

1 Use the keys to select the submenu „Step“, enter the<br />

desired number<br />

and press enter<br />

or<br />

2 If the submenu „Step“ is selected, section by section can be shown<br />

in ascending order by the key .<br />

Each previously set value is displayed.<br />

Delete:<br />

A flashing segment indicates that the respective profile number<br />

needs to be entered in which one or more consecutive sections are<br />

to be deleted.<br />

Example:<br />

Delete step 8 to step 34 in profile 4.<br />

Line 4 indicates the deletion.<br />

yes<br />

Example:<br />

>Print Profile 2<br />

Print<br />

yes<br />

<br />

>Print Profile 2<br />

****** print *******<br />

Print:<br />

Each profile may be printed via the serial interface for control or<br />

documentation.<br />

A flashing segment indicates that the number of the profile to be<br />

printed needs to be entered.<br />

Example: Print profile 2<br />

yes<br />

Printing is indicated in line 2.<br />

>hour.min 14:24<br />

Day.Mon 07.12<br />

Year 2003<br />

14:24:36<br />

Setting clock<br />

The integrated clock allows starting a profile at any date and time.<br />

The clock is preset in the factory.<br />

Lines 1 to 3:<br />

Check for correctness of the preset date and time and correct if<br />

necessary.<br />

The time is diplayed permanently in line 4.<br />

48


Ultra-Low Refrigerated Circulators<br />

6.5. Analog inputs/outputs<br />

ALARM STAND-BY<br />

REG+<br />

E-PROG<br />

In order to use the analog inputs and outputs, the circulator must be<br />

equipped with the electronics module available as option.<br />

Order No. 8 900 100 Electronic module<br />

This submenu enables setting of the input and output values for the<br />

programmer input and the temperature recorder outputs of socket<br />

REG+E-PROG.<br />

The >STAND-BY< input and the >ALARM< output are configurable.<br />

If the electronic module is not fitted, this menu can only be used to<br />

switch control of the solenoid valve.<br />

Int. Programmer<br />

>Input/Output<br />

Limits<br />

Interface serial<br />

ESC<br />

Indication without electronic module<br />

Inputs/Outputs<br />

>SV-Out. : Backflow /C-Puls<br />

ESC<br />

Inputs/Outputs<br />

>SV-Out. : Backflow /C-Puls<br />

Chan.1 : ActInt<br />

Chan.2 : Power<br />

Chan.3 : Setpoint<br />

EPROG : Setpoint<br />

Ext.StBy : inactive /active<br />

AlarmOut : StdBy<br />

>Chan.1 : ActInt /<br />

0V = -99.9°C<br />

10V = 400.0°C<br />

ActExt/Power/Setpoint<br />

1<br />

>Chan.2 : Power /<br />

0V = 0.00%<br />

10V = 100%<br />

ActInt/ActExt/Setpoint<br />

1<br />

ESC<br />

>Chan.3 : Setpoint / ActExt/ACtInt/Power<br />

0mA = -99.9°C<br />

20mA = 400.0°C 1<br />

Region: 0-20mA /4-20mA<br />

>EPROG : Setpoint / ActVar (%)/Flowrate(l/min)<br />

Signal : Voltage /Current<br />

L Value -99.9°C REM: % / l/Min<br />

H Value 400.0°C REM: % / l/Min<br />

Setpoint : xx.xx°C REM: % / l/Min 1<br />

AlarmOut<br />

>Function: StdBy /Alarm/Al+StBy<br />

Type : normal /invers<br />

NOTE: Channel 2 is pre-configured for connecting a HST<br />

Booster heater.<br />

49


Menu functions<br />

Menu level 2<br />

Inputs/Outputs<br />

>SV-Out : Backflow /C-Puls<br />

Chan.1 : ActInt<br />

Chan.2 : ActInt<br />

Chan.3 : Setpoint<br />

EPROG : Setpoint<br />

Ext.StBy : inactiv /activ<br />

AlarmOut : StdBy<br />

1. Use the keys to select the desired (>) menu item in<br />

menu level 2 on the LCD DIALOG-DISPLAY.<br />

2. Use the keys and to store the desired parameter or<br />

press enter to enter menu level 3. An input window<br />

opens for each menu item.<br />

3. In the input window in menu level 3 select the menu item with<br />

the keys .<br />

4. Use the keys to select the parameter (parameter blinks)<br />

or<br />

use the numeral keypad to enter the numbers (number<br />

segment blinks).<br />

5. Press enter to store the new parameter or value.<br />

Menu level 2<br />

SV-Output<br />

Control connector (14) 230 V max. 1.25 A<br />

Channel 1 voltage output for recorder (V)<br />

Channel 2 voltage output for recorder (V))<br />

Channel 3 current output for recorder (mA)<br />

EPROG<br />

External standby<br />

Alarm output<br />

external programmer input<br />

Standby input<br />

(for external emergency switch-off)<br />

Output for external alarm signal<br />

Control connector (14):<br />

SV-Out >Backflow< or >C-Puls<<br />

The control output (14) can be matched to solenoid valves for<br />

different tasks.<br />

>Backflow< In the OFF condition, the control output (14) is not<br />

powered.<br />

See – Return flow safety device- on page 23<br />

>C-Puls< The control output (14) can be used for emitting a cooling<br />

pulse. For the pulsing period, the output is powered.<br />

(only used with Heating Circulators)<br />

50


Ultra-Low Refrigerated Circulators<br />

REG+E-PROG (12):<br />

Outputs of the connector<br />

1. First define the desired output value for channels 1 to 3:<br />

ActInt internal actual temperature value (bath temperature)<br />

ActExt ernal actual temperature value (external sensor)<br />

Power periodic or intermittent heating or cooling<br />

Setpoint active setpoint temperature<br />

(Setpoint1, 2, 3,/ integr. programmer /external programmer)<br />

2. Then select the display size for channels 1 to 3:<br />

Voltage outputs channels 1 and 2<br />

Assign the voltage values of 0 V to the lowest and 10 V to the highest<br />

necessary temperature or power rating required as an output value<br />

(°C / %).<br />

Current output channel 3<br />

Assign the current values 0 mA or 4 mA to the lowest and 20 mA to<br />

the highest temperature or power rating required as an output value<br />

(°C / %).<br />

3. The current output (chanell 3) offers 2 ranges for selection:<br />

0 to 20 mA or 4 to 20 mA<br />

0 V<br />

10 °C 210 °C<br />

200 K<br />

197 °C 202 °C<br />

5 K<br />

0 mA 20 mA<br />

4 mA<br />

Examples:<br />

>Chan.1 : ActInt<br />

0V = 10°C<br />

10V = 210°C<br />

lowest temperature value: 10 °C<br />

highest temperature value 210 °C<br />

Fig. shows 200 C scaled to paper width<br />

rise: 50 mV/°C<br />

lowest temperature value: 197 °C<br />

highest temperature value: 202 °C<br />

Fig. shows 5 C scaled to paper width<br />

rise: 2000 mV/°C<br />

51


Menu functions<br />

Menu >Configuration<<br />

Configuration<br />

>Setpoint :<br />

Autostart: off<br />

Standby : pump off<br />

Language : english<br />

Reset : no<br />

Variable : Control /serial/eprog<br />

eprog Keypad/RS232/extPt100<br />

E-PROG - Input<br />

Setting needs to be carried out, if<br />

1. setpoint programming is to be made via an<br />

external programmer.<br />

For this, in the menu >Configuration< first set<br />

the menu item >Setpoint< to >eprogInputs/Outputs<<br />

>EPROG : Flowrate<br />

Signal : Voltage<br />

L Value 0.0L<br />

H Value 50.0L<br />

Flowrate: xx.xL<br />

Setpoint/Variable<br />

(Liters/Minute)<br />

2. the heater variable should be controlled via an<br />

external control pulse.<br />

For this, in the menu >Configuration< set the<br />

menu item > Variable.< to >eprogSetpoint< or under menu item > Variable Setpoint< or > Variable ConfigurationInputs/OutputsEPROG : Setpoint<br />

Signal : Current<br />

L Value 0.0°C<br />

H Value 300.0°C<br />

Setpoint : 50.0°C<br />

<br />

Connect the external programmer to socket (12) REG+E-PROG of<br />

the circulator.<br />

Selecting the signal:<br />

The programmer (E-PROG) input of the circulator can be matched to<br />

the output signal of the external programmer.<br />

Voltage voltage input<br />

Current current input<br />

„L Value“ - Setting the LOW value: (See below )<br />

Adjust and set the lowest desired working temperature on the<br />

programmer (e.g. 0 C).<br />

Enter the same value on the circulator by pressing the appropriate<br />

buttons on the keypad and press enter<br />

to set.<br />

„H Value“ - Setting the HIGH value: (See below )<br />

Adjust and set the highest desired working temperature on the<br />

programmer (e.g. 300 C).<br />

Enter the same value on the circulator by pressing the appropriate<br />

buttons on the keypad and press enter<br />

to set.<br />

Example:<br />

Set a temperature of 50 C on the external programmer!<br />

The value adjusted and set on the external programmer is displayed<br />

in line 4 of the LCD DIALOG-DISPLAY for control purposes.<br />

52


Ultra-Low Refrigerated Circulators<br />

Eprog : 50.0°C<br />

IntAct : 24.7°C<br />

Power : 80 %<br />

Control : intern<br />

After returning the LCD display to standard display by pressing<br />

this value is displayed in line 1<br />

(Example: Eprog 50.00 C).<br />

This EPROG input enables the use of different voltage and current<br />

values as program parameters.<br />

°C<br />

300<br />

250<br />

200<br />

150<br />

B<br />

A<br />

„L Value“ - Setting the LOW value: (See below )<br />

1) Adjust and set the lowest desired value on the voltage or<br />

current source resp. (Example A: 1 V).<br />

2) Assign a lower temperature threshold value to this adjusted<br />

voltage/current value by pressing the appropriate buttons on the<br />

keypad of the instrument (Example A: 20 C ) and set by<br />

pressing enter .<br />

100<br />

80<br />

60<br />

40<br />

20<br />

1 2 3 4 5 6 7 8 9 10 V<br />

2 4 6 8 10 14 18 20 mA<br />

„H Value“ - Setting the HIGH value: (See below )<br />

1) Adjust and set the highest desired value on the voltage or<br />

current source resp. (Example A: 10 V).<br />

2) Assign an upper temperature threshold value to this adjusted<br />

voltage/current value by pressing the appropriate buttons on the<br />

keypad of the instrument<br />

(Example A: 200 C) and set by pressing enter .<br />

Return to the standard display by pressing .<br />

Example B in the diagram serves to illustrate that the end point<br />

values are freely selectable.<br />

>EPROG : Setpoint<br />

Signal : Voltage<br />

L Value<br />

H Value<br />

20.0°C<br />

200.0°C<br />

Setpoint : 152.0°C<br />

<br />

Eprog : 152.00°C<br />

IntAct : 50.76°C<br />

Power : 100 %<br />

Control : intern<br />

Example out of diagram A:<br />

Adjusting the voltage source for an output of 7.6 V!<br />

Line 5 of the LCD DIALOG-DISPLAY shows the externally set setpoint<br />

value. The instrument calculates this value from the rise angle of the two<br />

pre-decided end points (in example A: 7.6 V correspond to an external<br />

setpoint temperature of 152.0 C ).<br />

After returning the LCD display to standard display by pressing ,<br />

this value is displayed in line 1<br />

(Example: EPROG 152.00 C).<br />

Notice:<br />

If this adjustment is not correctly performed at two different points, the setpoint<br />

setting will be incorrect.<br />

<br />

Important:<br />

The usable temperature range between > L Value < and > H Value < is limited to the<br />

configured working temperature range of the circulator resp. of the unit combination<br />

(working temperature range see technical specifications on page 10)<br />

53


Menu functions<br />

Ext. StBy (External STANDBY input)<br />

(for external emergency switch-off)<br />

(Connector see page 70)<br />

Possible parameters:<br />

inactiv - standby input is ignored<br />

activ<br />

- standby input is active<br />

AK<br />

2<br />

1<br />

STAND-BY<br />

3<br />

Activate the standby input:<br />

1. Under menu item >Ext. StByactiv


Alarm output (10)<br />

(for external alarm signal)<br />

Ultra-Low Refrigerated Circulators<br />

This socket is a potential-free change-over contact. With the<br />

adjustments in the menu >Inputs/Outputs< all operating conditions<br />

can be signaled without having to change the pin assignments.<br />

Menu >Inputs/Outputs<<br />

AlarmOut<br />

>Function: StdBy /Alarm/Al+StBy<br />

Type : normal /invers<br />

ALARM<br />

Signification of the terms under menu item >Function< :<br />

The circulator is in condition<br />

>StandBy< or >Alarm<<br />

-OFF-<br />

S xx.xx<br />

E -----<br />

XXXXX<br />

ALARM<br />

CODE xx<br />

For >Type: normal< pins 2 and 3 are connected in any case<br />

according to the selected >FunctionType: invers< pins 2 and 1 are connected in any case<br />

according to the selected >Function


Menu functions<br />

6.6. Limits<br />

The menu >Limits< allows for setting the minimum and maximum values for all<br />

important setting ranges and capacity variables.<br />

Inputs/Outputs<br />

>Limits<br />

Interface serial<br />

ATCalibration<br />

ESC<br />

ESC<br />

Limits<br />

>SetMax :300.00°C<br />

SetMin :-94.99°C<br />

HeatingMax: 100%<br />

CoolingMax: 0%<br />

IntMax :300.00°C<br />

IntMin :-94.99°C<br />

Upper band: 200K<br />

Lower band: 200K<br />

1<br />

In case of external control<br />

these menu items are<br />

additionally indicated<br />

SetMax: and SetMin:<br />

Maximum and minimum setpoint<br />

Restriction for the adjustable temperature range.<br />

Setting range: see working temperature range<br />

The limitation of the operating temperature range effects the temperature<br />

setting under the menu called up with the key - Setpoint 1, 2, 3.<br />

It is possible to adjust only working temperatures that lie within the limit range<br />

set here.<br />

Existing settings for Setpoint 1, 2, 3 and also for >OverTemp< and >SubTemp<<br />

(see page 28) are automatically defered within the limit range.<br />

HeatingMax:<br />

and CoolingMax:<br />

Adjusted maximum heating / cooling.<br />

Setting range: 0 to 100 % in steps of 1 %<br />

Heating and cooling powers of the circulator are adjustable. 100 %<br />

corresponds to the values in the technical specifications of the equipment.<br />

Factory setting: CoolingMax<br />

Refrigorated/heating circulator Fxx = 0 % eg. F81<br />

Refrigorated/heating circulator FPxx = 100 % eg. FP88<br />

56


Ultra-Low Refrigerated Circulators<br />

>SafeTemp:<<br />

IntMax: and IntMin: Limit setting<br />

Setting range: see working temperature range<br />

The limits IntMax and IntMin are only valid for external control. IntMax and<br />

IntMin are used to limit the expected internal bath temperatures to any upper<br />

and lower values. The temperature controller cannot exceed these limits even if<br />

it would be required for reaching the temperature in the external system.<br />

Consequently the external setpoint may thus not be reached.<br />

Sense of a limit setting:<br />

Protects the bath fluid from overheating.<br />

Prevents an undesired alarm shut-down by the excess temperature<br />

protection - >ALARM CODE 14IntMax:< to a value at least 5 °C below the >SafeTemp:< value.<br />

Protects the pump motor from high viscosity of the bath fluid at low<br />

temperatures.<br />

For refrigerated circulators: Freezing protection when using water as bath<br />

fluid.<br />

°C<br />

200<br />

150<br />

Upper band: and Lower band: Band limit<br />

The band limit is active for external control.<br />

internal bath<br />

external system<br />

For the heat-up and cool-down phases<br />

different settings to conform to the<br />

requirements of the particular application<br />

are possible.<br />

Setting range: 0 ... 200 °C<br />

100<br />

75<br />

50<br />

25<br />

AreaUp<br />

AreaDown<br />

10 20 30 40 50 60 10 20 30 40 50 60 10 [min]<br />

During the heat-up phase the difference value always adds to the actual<br />

external temperature. During the cool-down phase, the difference value is<br />

subtracted.<br />

t<br />

Using Upper band and Lower band, the<br />

difference between the temperatures in<br />

the internal bath and the external system<br />

can be limited to any maximum value for<br />

the heat-up or the cool-down phase.<br />

Sense of a band limit:<br />

Ensures gentle heating for the objects requiring temperature application.<br />

Protects glass reactors, for example, from thermal shock.<br />

The IntMax: and IntMin: values are superordinated to this band limit.<br />

57


Menu functions<br />

6.7. Serial interface<br />

For communication between circulator and a PC or a superordinated<br />

process system the interface parameters of bath units must be identical. The<br />

adjustment is usually carried out one time only in the menu >Interface<br />

serialInterface serial<br />

ATCalibration<br />

ESC<br />

Interface<br />

>Type<br />

RS232 /RS485/PROFI<br />

Baudrate 4800 /9600/19200/38400<br />

Parity<br />

Handshake<br />

even /no/odd<br />

hardw / softw<br />

Interface<br />

>Type<br />

RS485 /PROFI/RS232<br />

Baudrate 4800 /9600/19200/38400<br />

Parity<br />

even /no/odd<br />

Address 0<br />

RS232<br />

RS485<br />

1<br />

Type<br />

RS232 / RS485<br />

Baud rate 4800/9600/19200/38400<br />

Parity<br />

none/even/odd<br />

Handshake software handshake/hardware handshake<br />

Address 0 to 127<br />

Factory settings:<br />

4800 Bauds<br />

even<br />

hardware handshake<br />

58


Ultra-Low Refrigerated Circulators<br />

6.8. ATC Absolute Temperature Calibration, 3-point calibration<br />

ATC serves to compensate a temperature difference that might occur between<br />

circulator and a defined measuring point in the bath tank because of physical<br />

properties.<br />

Limits<br />

Interface serial<br />

>ATCalibration<br />

Pump<br />

ESC<br />

ESC<br />

ATCalibration<br />

>Sensor : intern<br />

Status : no /yes<br />

Type : 3-point /1-point/2-point<br />

TmpValue1: xx.xx°C<br />

CalValue1: xx.xx°C<br />

TmpValue2: xx.xx°C<br />

CalValue2: xx.xx°C<br />

TmpValue3: xx.xx°C<br />

1<br />

CalValue3: xx.xx°C<br />

internal<br />

ESC<br />

ATCalibration<br />

>Sensor : extern<br />

Status : no /yes<br />

Type : 3-point /1-point/2-point<br />

TmpValue1: xx.xx°C<br />

CalValue1: xx.xx°C<br />

TmpValue2: xx.xx°C<br />

CalValue2: xx.xx°C<br />

external<br />

1<br />

TmpValue3: xx.xx°C<br />

CalValue3: xx.xx°C<br />

Sensor: >internextern<<br />

Calibration can be carried out for the internal temperature sensor and<br />

for the external temperature sensor connected to the socket „ext.<br />

Pt100“.<br />

The circulator is able to store both parameter sets. However, only the<br />

one set under this menu item is indicated.<br />

Status:<br />

>no< The controller of the circulator uses the original curve of<br />

the temperature sensor.<br />

Important: During the calibration process >no< needs to be set.<br />

>yes<<br />

curve.<br />

The controller of the circulator uses the new calibration<br />

59


Menu functions<br />

Type:<br />

A >1-point2-point < or >3-point < calibration can be carried<br />

out.<br />

First geometrically define the location for calibration (measuring point<br />

T M ), then determine the temperature values of of the calibration<br />

points.<br />

The calibration type also determines the number of pairs of values<br />

indicated on the LCD DIALOG-DISPLAY.<br />

TmpValue: 1 or 2 or 3<br />

Defined temperature value of the calibration point. This value is<br />

automatically stored with >CalValue< and can be indicated for control<br />

purposes.<br />

CalValue: 1 or 2 or 3<br />

The „Calibration value“ is determined with a temperature measuring<br />

device and stored under menu item >CalValueATCalibration< under menu item >Calwert X


Ultra-Low Refrigerated Circulators<br />

1. Use the keys to select the menu item.<br />

2. With the keys select the parameter (parameter blinks)<br />

or<br />

use the numeral keypad to enter the numbers (number segment<br />

blinks).<br />

3. Press enter to store the new parameter or value.<br />

Examples:<br />

T T = 80.00 °C<br />

T M = 79.73 °C<br />

T T = 120.00 °C<br />

T M = 119.51 °C<br />

T T = 160.00 °C<br />

T M = 159.34 °C<br />

Control<br />

>ControlType: intern<br />

Selftuning: once<br />

nein Dynamic : aperio<br />

Example:<br />

3-point calibration for internal control.<br />

In the temperature range of 80 °C to 160 °C the calibration curve of the<br />

temperature sensor (T T ) should be assimilated to the actual temperatures<br />

on the measuring point (T M ).<br />

Press the button. Under the menu >Control< set >ControlType<<br />

to >intern< and press enter .<br />

(ControlType: Can only be adjusted in the –OFF– condition)<br />

Press start/stop .<br />

Calibration procedure:<br />

Setpoints<br />

>Setpoint1: 80.00°C<br />

Setpoint2: 37.00°C<br />

Setpoint3: 70.00°C<br />

1. Press and set the first temperature value under<br />

>Setpoint1< for example (example 1 st value = 80 °C).<br />

2. Wait until this temperature is maintained constant in the bath for<br />

about 5 minutes.<br />

3. Press the button and open the menu >ATCalibrationSensor : intern<br />

Status : no<br />

Type : 3.point<br />

TmpValue1: 80.00°C<br />

CalValue1: 79.73°C<br />

TmpValue2: xx.xx°C<br />

CalValue2: xx.xx°C<br />

TmpValue3: xx.xx°C<br />

CalValue3: xx.xx°C<br />

4. Set the following:<br />

Menu item >Sensor< to >intern< ,<br />

Menu item >Status< to >no< ,<br />

Menu item >Type< to >3-pointCalValue 1< (79.73 °C) using the<br />

numeral keypad.<br />

Press enter and the circulator also stores the value of T T as<br />

value for >TmpValue 1< (80.00 °C) .<br />

The first of the 3 points is now calibrated.<br />

6. Repeat the calibration procedure for 120 °C and 160 °C.<br />

61


Menu functions<br />

6.9. Setting the pump pressure<br />

Examples:<br />

Adjusted<br />

Effective<br />

The pressure of the circulating pump is adjustable in four grades. After<br />

setting, the VFD-Info-Display indicates the corresponding value.<br />

Adjustable pump capacity stage 1 ... 4<br />

Illuminated display:<br />

for pump pressure<br />

Display for the adjusted pump pressure stage in the –OFF- mode.<br />

Display for the effective pump pressure stage (rotation speed) after start.<br />

For protecting the pump motor, the rotation speed changes with the load<br />

applied, for example depending on the viscosity of the bath fluid at different<br />

working temperatures.<br />

Flow rate:<br />

22 ... 26 l/min<br />

Pump capacity stage 1 2 3 4<br />

Pump pressure: [bar] 0,4 0,5 0,6 0,7<br />

Suction pump [bar] 0,2 0,26 0,33 0,4<br />

Total capacity [bar] 0,6 0,76 0,93 1,1<br />

in a loop circuit<br />

Limits<br />

Interface serial<br />

ATCalibration<br />

>Pump<br />

ESC<br />

ESC<br />

Pump<br />

>Pump level: 1 /2/3/4<br />

1. Use the keys to select the menu item.<br />

2. With the keys select the parameter (parameter blinks).<br />

3. Press enter to store the new parameter or value.<br />

62


Ultra-Low Refrigerated Circulators<br />

7. Troubleshooting guide / Error messages<br />

XXXXX<br />

ALARM<br />

CODE 01<br />

+<br />

XXXXX<br />

WARNING<br />

CODE 40<br />

Alarm with a complete shutdown of the unit<br />

Whenever the microprocessor electronics registers a failure, a complete<br />

shutdown of the heater and circulating pump is performed. The alarm<br />

light „ “ illuminates and a continuous signal tone sounds.<br />

The VFD-COMFORT-DISPLAY indicates the cause for the alarm in form<br />

of a code.<br />

Warning without a complete shutdown of the unit<br />

The VFD-COMFORT-DISPLAY indicates the cause for the warning in<br />

form of a code and an acoustic signal sounds in regular intervals.<br />

These messages appear every 10 seconds.<br />

Press enter<br />

to quit the audible signal.<br />

ALARM<br />

CODE 01<br />

Insufficient liquid<br />

level or float is<br />

defective.<br />

Press to indicate the help text in the LCD DIALOG-DISPLAY when<br />

alarm messages appear.<br />

<br />

<br />

<br />

The circulator is operated without bath fluid, or the liquid level is<br />

insufficient. Replenish the bath tank with the bath fluid.<br />

Tube breakage has occured (insufficient filling level due to excessive<br />

bath fluid pumped out). Replace the tubing and replenish the bath<br />

tank with the bath fluid.<br />

The float is defect (e. g., because damaged in transit). Repair by<br />

authorized JULABO service personnel.<br />

ALARM<br />

CODE 02<br />

Control cable of<br />

cooling machine<br />

interrupted during<br />

Operation.<br />

<br />

During the self-test after switch-on a short-circuit is registered<br />

between pin 2 and pin 4 of the control cable or the control cable is<br />

interrupted during operation.<br />

Reconnect the cable or eliminate the short-circuit.<br />

WARNING<br />

CODE 03<br />

WARNING<br />

CODE 04<br />

ALARM<br />

CODE 03<br />

Actual temperature<br />

above high temperature<br />

value.<br />

ALARM<br />

CODE 04<br />

Actual temperature<br />

below low temperature<br />

value.<br />

<br />

Excess temperature warning<br />

or<br />

Excess temperature alarm<br />

Warn-Type: Set to<br />

>Warning< or >Alarm<<br />

<br />

Low temperature warning<br />

or<br />

Low temperature alarm.<br />

Warn-Type: Set to<br />

>Warning< or >Alarm<<br />

63


Troubleshooting guide / Error messages<br />

ALARM<br />

CODE 05<br />

Internal working<br />

sensor shurtcircuited<br />

or<br />

interrupted.<br />

<br />

Cable of the working temperature sensor interrupted or shortcircuited.<br />

ALARM<br />

CODE 06<br />

Difference between<br />

working- and safetytemp.<br />

Bigger than<br />

permissable value.<br />

<br />

Defect of the working or excess temperature sensor.<br />

Working temperature and excess temperature sensors report a<br />

temperature difference of more than 25 °C.<br />

ALARM<br />

CODE 07<br />

The internal I2C<br />

bus-system shows<br />

a failure.<br />

<br />

Other errors (I 2 C-BUS errors)<br />

ALARM<br />

CODE 12<br />

Error in A/Dconverter<br />

of the<br />

internal measuring<br />

system.<br />

<br />

Error in A/D converter<br />

ALARM<br />

CODE 14<br />

Working temperature<br />

exceeds the adjusted<br />

safety temperature.<br />

<br />

<br />

Excess temperature sensors defect.<br />

The excess temperature value lies below the working temperature<br />

setpoint. Set the excess temperature to a higher value.<br />

ALARM<br />

CODE 15<br />

External control<br />

selected, but ext.<br />

sensor not connected<br />

or defective.<br />

<br />

External control selected, but external Pt100 sensor not connected or<br />

defect.<br />

WARNING<br />

CODE 20<br />

<br />

Cooling of the condenser is affected. Clean air-cooled condenser.<br />

Check the flow rate and cooling water temperature on water-cooled<br />

condenser.<br />

64


WARNING<br />

CODE 21<br />

WARNING<br />

CODE 22<br />

WARNING<br />

CODE 23<br />

WARNING<br />

CODE 24<br />

WARNING<br />

CODE 25<br />

ALARM<br />

CODE 33<br />

Internal safetytemperature<br />

sensor<br />

short-circuited or<br />

interrupted.<br />

<br />

<br />

<br />

<br />

<br />

<br />

<br />

<br />

Ultra-Low Refrigerated Circulators<br />

Compressor stage 1 does not work.<br />

After a short cooling interval, the compressor motor will be<br />

automatically reconnected and the message "CODE 21" no longer<br />

appears.<br />

Compressor stage 2 does not work.<br />

Cooling compressor overload protection<br />

The motor of the cooling compressor is equipped with an overload<br />

protector, which will be activated by excessive temperature in the<br />

capsule or by excessive current consumption.<br />

Causes for motor disconnection:<br />

- poor air circulation<br />

- small distance to walls<br />

- dirt accumulated on condenser<br />

- high ambient temperature<br />

- switch-off and on for short intervals<br />

Excess temperature in stage 1 of the compressor.<br />

Excess temperature in stage 2 of the compressor.<br />

Short-circuit in the control cable for the refrigerating machine during<br />

self-test.<br />

Cable of the excess temperature sensor interrupted or short-circuited.<br />

ALARM<br />

CODE 38<br />

Ext. Sensor input<br />

without signal but<br />

setpoint programming<br />

set to ext. Pt100.<br />

<br />

Ext. Pt100 sensor input without signal, but setpoint programming set<br />

to external Pt100.<br />

WARNING<br />

CODE 40<br />

<br />

The early warning system for low level signals a critical fluid level.<br />

Replenish the bath tank with the bath fluid.<br />

After eliminating the malfunction, press the mains power switch off and<br />

on again to cancel the alarm state.<br />

If the unit cannot be returned to operation, contact an authorized<br />

JULABO service station.<br />

65


Troubleshooting guide / Error messages<br />

CONFIGURATION<br />

ERROR<br />

CONFIRM BY<br />

PRESSING : <br />

Special message „CONFIGURATION ERROR“<br />

The configuration of the circulator does not conform to its present use.<br />

Press enter to automatically perform a single modification of the<br />

configuration.<br />

Then contact an authorized JULABO service station.<br />

Disturbances that are not indicated.<br />

The electronic pump motor is overload-protected by an electronic current<br />

limiter. If viscosity of the bath fluid is or becomes too high, the motor<br />

stops running.<br />

Fuses:<br />

The mains fuses on the rear of the unit may easily be exchanged as<br />

shown on the left.<br />

Circulator: Fine fuses (15)– T 1.25 A, 250 V~ , D 5 x 20 mm<br />

Circulator: Fine fuses (16a)– T 16 A, 250 V~ , D5 x 20 mm<br />

Warning:<br />

Before exchanging the fuses, turn off the mains power switch and disconnect the<br />

power plug from the mains socket!<br />

Only use fine fuses with a nominal value as specified.<br />

Example:<br />

Manufacturer Supplier Type Order No.<br />

Schurter Schurter G-fuse insert SPT<br />

No. 0001.2516<br />

T16A 5x20mm<br />

Wickmann Wickmann G-fuse insert<br />

T1.25A 5x20 mm<br />

No. 19195<br />

66


Ultra-Low Refrigerated Circulators<br />

8. Safety recommendations<br />

Follow the safety recommendations to prevent damage to persons or property.<br />

Further, the valid safety instructions for working places must be followed.<br />

<br />

<br />

<br />

<br />

<br />

<br />

<br />

<br />

<br />

<br />

<br />

<br />

<br />

<br />

<br />

Only connect the unit to a power socket with earthing contact (PE – protective<br />

earth)!<br />

Place the instrument on an even surface on a pad made of non-inflammable<br />

material.<br />

Do not stay in the area below the unit.<br />

Make sure you read and understand all instructions and safety precautions listed<br />

in this manual before installing or operating your unit.<br />

Observe the fire point of the bath medium used.<br />

The excess temperature protection should be set at least 25 °C below the fire<br />

point.<br />

Never operate the unit without bath fluid in the bath.<br />

Pay attention to the thermal expansion of bath oil during heating to avoid<br />

overflowing of the fluid.<br />

Prevent water from penetrating into the hot bath oil.<br />

Exercise caution when emptying hot bath fluids!<br />

Check the temperature of the bath fluid prior to draining (by switching the unit on<br />

for a short moment for example).<br />

Observe the limited working temperature range when using plastic bath tanks.<br />

Employ suitable connecting tubing.<br />

Make sure that the tubes are securely attached.<br />

Never operate damaged or leaking equipment.<br />

Always turn off the unit and disconnect the mains cable from the power source<br />

before performing any service or maintenance procedures, or before moving the<br />

unit.<br />

Always empty the bath before moving the unit.<br />

Never operate equipment with damaged mains power cables.<br />

<br />

Some parts of the bath cover and the pump connections may become extremely<br />

warm during continuous operation. Therefore, exercise particular caution when<br />

touching these parts.<br />

Notice:<br />

Check the safety installations at least twice a year!<br />

Excess temperature protection according to IEC 61010-2-010<br />

With a screwdriver turn back the adjustable excess temperature protection until<br />

the shut-down point (actual temperature).<br />

Low level protection according to IEC 61010-2-010<br />

To check the function of the float, it can be manually lowered with a screwdriver<br />

for example.<br />

67


Electrical connections<br />

9. Electrical connections<br />

Notice:<br />

Use shielded cables only.<br />

The shield of the connecting cable is electrically connected to the plug housing.<br />

The unit ensures safe operation if connecting cables with a maximum length of 3 m are<br />

used. The use of longer cables does not affect proper performance of the unit, however<br />

external interferences may have a negative impact on safe operation.<br />

Pt100<br />

Shield<br />

ext. Pt100<br />

2<br />

3<br />

Plug<br />

1<br />

4<br />

Look on<br />

soldering side.<br />

Socket for external Pt100 sensor<br />

Pin assignment:<br />

Pin Signal<br />

1 I+<br />

2 U+<br />

3 U-<br />

4 I-<br />

The shield of the connecting cable is electrically connected to the plug<br />

housing and the sensor tube.<br />

SERIAL<br />

RS232/RS485 serial interface<br />

This port can be used to connect a computer with an RS232 or RS485<br />

cable for remote control of the circulator.<br />

Pin assignments RS232:<br />

Pin 2 RxD Receive Data<br />

Pin 3 TxD Transmit Data<br />

Pin 4 DTR Data terminal ready<br />

Pin 5 0 V Signal GND<br />

Pin 7 RTS Request to send<br />

Pin 8 CTS Clear to send<br />

Pin 1; 6; 9<br />

Reserved - do not use!<br />

Pin assignments RS485:<br />

Pin 3 B<br />

Pin 5 0 V Signal GND<br />

Pin 6 +5 V (50 mA max. load current)<br />

Pin 8 A<br />

Pins 1; 2; 7; 9 are reserved - do not use!<br />

Notice: RS485 serial interface<br />

The max. load current between Pin 5 and Pin 6 is 50 mA.<br />

68


Ultra-Low Refrigerated Circulators<br />

RS232 interface cable 9-pin / 9-pin, 2.5 m - Order No.: 8 980 073<br />

Interface correspondence: RS232<br />

Circulator (9-pole)<br />

PC (9-pole)<br />

Pin 2 RxD Pin 3 TxD<br />

Pin 3 TxD Pin 2 RxD<br />

Pin 4 DTR Pin 6 DSR<br />

Pin 5 GND Pin 5 GND<br />

Pin 7 RTS Pin 8 CTS<br />

Pin 8 CTS Pin 7 RTS<br />

/ Control output<br />

The connector may be used for control of JULABO refrigerated<br />

circulators or as output for alarm messages.<br />

2<br />

4 5<br />

1 3<br />

Circuit: Operation = relay powered<br />

Alarm = relay not powered<br />

Pin assignment:<br />

Pin Signal<br />

1 +24 V (I max. current 25 mA)<br />

2 0 V<br />

3 Alarm relay<br />

4 Reserved - do not use!<br />

5 Cooling pulse<br />

Alarm output<br />

(for external alarm signal)<br />

This potential-free change-over contact is activated in case of an alarm<br />

when pins 2 and 3 are connected.<br />

Switching capacity max. 30 W / 40 VA<br />

Switching voltage max. 125 V/<br />

Switching current max. 1 A<br />

ALARM<br />

Functional description see page 55<br />

69


Electrical connections<br />

STAND-BY input<br />

(for external emergency switch-off)<br />

Pin assignment: Pin Signal<br />

1 not connected<br />

2 5 V / DC<br />

3 0 V<br />

Functional description see page 54<br />

STAND-BY<br />

Programmer input / temperature recorder output<br />

REG+E-PROG<br />

Pin<br />

Signal<br />

1 Voltage output Channel 1 0 ... 10 V<br />

2 Voltage output Channel 2 0 ... 10 V<br />

3 GND for outputs 0 V<br />

4 Programmer input EPROG 0 to 10 V / 0 to 20 mA<br />

5 Current output Channel 3 0 to 20 mA / 4 to 20 mA<br />

6 GND for Programmer 0 V<br />

Functional description see page 51<br />

Control connectors (13, 14)<br />

The control output (14) can be matched to solenoid valves for different<br />

tasks.<br />

See menu settings on page 50<br />

See return flow safety device on page 23<br />

The control output (13) is not powered in the OFF condition.<br />

An external pump motor can be connected.<br />

Output voltage: 230 V / max. 1.25 A<br />

The fuse M 1.25 A is assigned to the control outputs.<br />

70


Ultra-Low Refrigerated Circulators<br />

10. Remote control<br />

10.1. Setup for remote control<br />

SERIAL<br />

R<br />

-OFF-<br />

S xxxx<br />

I xxxx<br />

1. Check the interface parameters for both interfaces (on circulator and PC)<br />

and make sure they match.<br />

In the menu >Interface< set the menu item >Type< to >RS232< or<br />

>RS485Configuration< set the menu item >Setpoint< to >RS232<<br />

or >RS485Configuration< see page 32)<br />

3. Connect both units with an interface cable..<br />

<br />

Like all parameters which can be entered through the keypad, interface<br />

parameters are stored in memory even after the circulator is turned off.<br />

10.2. Communication with a PC or a superordinated data system<br />

If the circulator is put into remote control mode via the configuration level, the<br />

VFD COMFORT-DISPLAY will read „R -OFF-„ = REMOTE STOP. The<br />

circulator is now operated via the computer.<br />

In general, the computer (master) sends commands to the circulator (slave).<br />

The circulator sends data (including error messages) only when the<br />

computer sends a query.<br />

<br />

In remote control mode: After a power interruption the order to start and all<br />

values which have to be adjusted must be resent from the personal computer<br />

via the interface.<br />

AUTOSTART is not possible.<br />

A transfer sequence consists of:<br />

address (RS485 interface only)<br />

command<br />

space (; Hex: 20)<br />

parameter (the character separating decimals in a group is the period)<br />

end of file (; Hex: 0D)<br />

<br />

The response (data string) after an in command is always followed by a<br />

line feed (LF, Hex: 0A).<br />

71


Remote control<br />

The commands are divided into in or out commands.<br />

in commands: asking for parameters to be displayed<br />

out commands: setting parameters<br />

<br />

Important times for a command transmission:<br />

To ensure a safe data transfer, the time gap between two commands should<br />

be at least 250 ms.<br />

The circulator automatically responds to an in command with a data string<br />

followed by a LF (Line Feed). The next command should only be sent after<br />

10 ms.<br />

<br />

The out commands are valid only in remote control mode.<br />

Examples:<br />

When the RS485 interface is used, the three-digit instrument address stands<br />

in front of each command.<br />

(example: address Ad32 = A032 )<br />

Command to set the working temperature >Setpoint1< to 55.5 °C<br />

out_sp_00 55.5<br />

A032_out_sp_00 55.5<br />

Command to ask for the working temperature >Setpoint1<<br />

in_sp_00<br />

A032_in_sp_00<br />

Response from the circulator:<br />

55.5 LF<br />

A032_55.5 LF<br />

Notice:<br />

out-commands<br />

Temperature values can be displayed on the circulator in the unit °C or °F.<br />

According to this setting the instructions via the interface also have to be made in the<br />

set unit.<br />

72


Ultra-Low Refrigerated Circulators<br />

10.3. List of commands<br />

out commands: Setting parameters or temperature values.<br />

Command Parameter Response of circulator<br />

out_mode_01 0 Use working temperature >Setpoint1<<br />

out_mode_01 1 Use working temperature >Setpoint2<<br />

out_mode_01 2 Use working temperature >Setpoint3<<br />

out_mode_02 0 Selftuning „off“.<br />

Temperature control by using the stored parameters.<br />

out_mode_02 1 Selftuning „once“<br />

Single selftuning of controlled system after the next start.<br />

out_mode_02 2 Selftuning „always“<br />

Continual selftuning of controlled system whenever a new<br />

setpoint is to be reached.<br />

out_mode_03 0 Set external programmer input to voltage.<br />

Voltage<br />

0 V ... 10 V<br />

out_mode_03 1 Set external programmer input to current.<br />

Current<br />

0 mA ... 20 mA<br />

out_mode_04 0 Temperature control of internal bath.<br />

out_mode_04 1 External control with Pt100 sensor.<br />

out_mode_05 0 Stop the unit = R –OFF-.<br />

out_mode_05 1 Start the unit.<br />

out_mode_08 0 Set the control dynamics - aperiodic<br />

out_mode_08 1 Set the control dynamics - standard<br />

out_sp_00 xxx.xx Set working temperature. „Setpoint 1“<br />

out_sp_01 xxx.xx Set working temperature. „Setpoint 2“<br />

out_sp_02 xxx.xx Set working temperature. „Setpoint 3“<br />

out_sp_03 xxx.xx Set high temperature warning limit „OverTemp“<br />

out_sp_04 xxx.xx Set low temperature warning limit „SubTemp“<br />

out_sp_06 xxx.xx Set manipulated variable for the heater via serial interface<br />

-100 ... +100 [%]<br />

out_sp_07 x Set the pump pressure stage. (1 ... 4)<br />

out_par_04 x.x CoSpeed for external control 0 ... 5.0.<br />

73


Remote control<br />

Command Parameter Response of circulator<br />

out_par_06 xxx Xp control parameter of the internal controller. 0.1 ... 99.9<br />

out_par_07 xxx Tn control parameter of the internal controller. 3 ... 9999<br />

out_par_08 xxx Tv control parameter of the internal controller. 0 ... 999<br />

out_par_09 xxx Xp control parameter of the cascade controller. 0.1 ... 99.9<br />

out_par_10 xxx Proportional portion of the cascade controller. 1 ... 99.9<br />

out_par_11 xxx Tn control parameter of the cascade controller. 3 ... 9999<br />

out_par_12 xxx Tv control parameter of the cascade controller. 0 ... 999<br />

out_par_13 xxx Maximum internal temperature of the cascade controller.<br />

out_par_14 xxx Minimum internal temperature of the cascade controller.<br />

out_par_15 xxx Band limit (upper) 0 ... 200 °C<br />

out_par_16 xxx Band limit (lower) 0 ... 200 °C<br />

out_hil_00 -xxx Set the desired maximum cooling power (0 % to 100 %).<br />

Note: Enter the value with a preceding negative sign!<br />

This adjustment only makes sense if FP refrigerating units<br />

are used.<br />

out_hil_01 xxx Set the desired maximum heating power (10 % to 100 %).<br />

in commands: Asking for parameters or temperature values to be displayed.<br />

Command Parameter Response of circulator<br />

version None Number of software version (V X.xx)<br />

status none Status message, error message (see page 76)<br />

in_pv_00 none Actual bath temperature.<br />

in_pv_01 none Heating power being used (%).<br />

in_pv_02 none Temperature value registered by the external Pt100 sensor.<br />

in_pv_03 none Temperature value registered by the safety sensor.<br />

in_pv_04 none Setpoint temperature („SafeTemp“) of the excess<br />

temperature protection<br />

in_sp_00 none Working temperature „Setpoint 1“<br />

in_sp_01 none Working temperature „Setpoint 2“<br />

in_sp_02 none Working temperature „Setpoint 3“<br />

in_sp_03 none High temperature warning limit „OverTemp“<br />

in_sp_04 none Low temperature warning limit „SubTemp“<br />

74


Ultra-Low Refrigerated Circulators<br />

Command Parameter Response of circulator<br />

in_sp_05 none Setpoint temperature of the external programmer<br />

(REG+E-PROG) .<br />

in_sp_06 none Temperature indication in °C or °F<br />

in_sp_07 none 1. Adjusted pump stage in the -OFF- condition.<br />

2. Pump stage corresponding to the effective rotation speed<br />

after start.<br />

in_sp_08 none Value of a flowrate sensor connected to the E-Prog input<br />

in_par_00 none Temperature difference between working sensor and safety<br />

sensor<br />

in_par_01 none Te - Time constant of the external bath.<br />

in_par_02 none Si - Internal slope<br />

in_par_03 none Ti - Time constant of the internal bath.<br />

in_par_04 none CoSpeed - Band limit (max. difference between the<br />

temperatures in the internal bath and external system).<br />

in_par_05 none Factor pk/ph0:<br />

Ratio of max. cooling capacity versus max. heating capacity<br />

in_par_06 none Xp control parameter of the internal controller.<br />

in_par_07 none Tn control parameter of the internal controller.<br />

in_par_08 none Tv control parameter of the internal controller.<br />

in_par_09 none Xp control parameter of the cascade controller.<br />

in_par_10 none Proportional portion of the cascade controller.<br />

in_par_11 none Tn control parameter of the cascade controller.<br />

in_par_12 none Tv control parameter of the cascade controller.<br />

in_par_13 none Adjusted maximum internal temperature of the cascade<br />

controller.<br />

in_par_14 none Adjusted minimum internal temperature of the cascade<br />

controller.<br />

in_par_15 none Band limit (upper)<br />

in_par_16 none Band limit (lower)<br />

in_mode_01 none Selected setpoint:<br />

0 = Setpoint 1<br />

1 = Setpoint 2<br />

2 = Setpoint 3<br />

in_mode_02 none Selftuning type:<br />

0 = Selftuning „off“<br />

1 = Selftuning „once“<br />

2 = Selftuning „alway“<br />

75


Remote control<br />

Command Parameter Response of circulator<br />

in_mode_03 none Type of the external programmer input:<br />

0 = Voltage 0 V to 10 V<br />

1 = Current 0 mA to 20 mA<br />

in_mode_04 none Internal/external temperature control:<br />

0 = Temperature control with internal sensor.<br />

1 = Temperature control with external Pt100 sensor.<br />

in_mode_05 none Circulator in Stop/Start condition:<br />

0 = Stop<br />

1 = Start<br />

in_mode_08 none Adjusted control dynamics<br />

0 = aperiodic<br />

1 = standard<br />

in_hil_00 none Max. cooling power (%).<br />

in_hil_01 none Max. heating power (%).<br />

10.4. Status messages<br />

Status messages<br />

Description<br />

00 MANUAL STOP Circulator in „OFF“ state.<br />

01 MANUAL START Circulator in keypad control mode.<br />

02 REMOTE STOP Circulator in „r OFF“ state.<br />

03 REMOTE START Circulator in remote control mode.<br />

10.5. Error messages<br />

Error messages<br />

Description<br />

-01 LOW LEVEL ALARM Low liquid level alarm<br />

-02 REFRIGERATOR ALARM Control cable of the refrigerated circulator or MVS<br />

solenoid valve controller short-circuited or interrupted.<br />

-03 EXCESS TEMPERATURE<br />

WARNING<br />

High temperature warning<br />

-04 LOW TEMPERATURE WARNING Low temperature warning.<br />

-05 WORKING SENSOR ALARM Working temperature sensor short-circuited or interrupted.<br />

-06 SENSOR DIFFERENCE ALARM Sensor difference alarm.<br />

Working temperature and safety sensors report a<br />

temperature difference of more than 25 °C.<br />

-07 I 2 C-BUS ERROR Internal error when reading or writing the I 2 C bus.<br />

76


Error messages<br />

Description<br />

-08 INVALID COMMAND Invalid command.<br />

-09 COMMAND NOT ALLOWED IN<br />

CURRENT OPERATING MODE<br />

Ultra-Low Refrigerated Circulators<br />

Invalid command in current operating mode.<br />

-10 VALUE TOO SMALL Entered value too small.<br />

-11 VALUE TOO LARGE Entered value too large.<br />

-12 TEMPERATURE MEASUREMENT<br />

ALARM<br />

-13 WARNING : VALUE EXCEEDS<br />

TEMPERATURE LIMITS<br />

-14 EXCESS TEMPERATURE<br />

PROTECTOR ALARM<br />

Error in A/D converter.<br />

Value lies outside the adjusted range for the high and low<br />

temperature warning limits. But value is stored.<br />

Excess temperature protector alarm<br />

-15 EXTERNAL SENSOR ALARM External control selected, but external Pt100 sensor not<br />

connected.<br />

-20 WARNING: CLEAN CONDENSOR<br />

OR CHECK COOLING WATER<br />

CIRCUIT OF REFRIGERATOR<br />

-21 WARNING: COMPRESSOR STAGE<br />

1 DOES NOT WORK<br />

-22 WARNING: COMPRESSOR STAGE<br />

2 DOES NOT WORK<br />

-23 WARNING: HIGH TEMPERATURE<br />

ON COMPRESSOR STAGE 1<br />

-24 WARNING: HIGH TEMPERATURE<br />

ON COMPRESSOR STAGE 2<br />

Cooling of the condenser is affected.<br />

Clean air-cooled condenser.<br />

Check the flow rate and cooling water temperature on<br />

water-cooled condenser.<br />

Compressor stage 1 does not work.<br />

Compressor stage 2 does not work.<br />

Excess temperature on compressor stage 1.<br />

Excess temperature on compressor stage 2.<br />

-25 REFRIGERATOR WARNING Error in the cooling machine.<br />

-26 WARNING: STAND-BY PLUG IS<br />

MISSING<br />

-30 CONFIGURATION ERROR:<br />

CONFIRM BY PRESSING <br />

ON CIRCULATOR<br />

External standby contact is open.<br />

(see page 54 and 70)<br />

The configuration of the circulator does not conform to its<br />

present use.<br />

Press enter to automatically perform a single<br />

modification of the configuration.<br />

-33 SAFETY SENSOR ALARM Excess temperature sensor short-circuited or interrupted.<br />

-38 EXTERNAL SENSOR SETPOINT<br />

PROGRAMMING ALARM<br />

Ext. Pt100 sensor input without signal and setpoint<br />

programming set to external Pt100.<br />

-40 NIVEAU LEVEL WARNUNG Low liquid level warning in the internal reservoir.<br />

77


JULABO Service – Online remote diagnosis<br />

11. JULABO Service – Online remote diagnosis<br />

JULABO circulators of the HighTech series are equipped with a so-called<br />

black box. This box is implemented in the controller and records all significant<br />

data for the last 30 minutes.<br />

In case of a failure, this data can be read out from the unit by using special<br />

software. The respective program is available for free download from<br />

www.julabo.de \ EasyBlackBox.<br />

<br />

Installation is easy and carried out step by step.<br />

Please observe the instructions.<br />

<br />

<br />

<br />

Data read-out is possible in the conditions<br />

„OFF“, „R OFF“ or „ALARM“.<br />

Connect the circulator to the computer using an interface<br />

cable.<br />

Start the EasyBlackBox program.<br />

The program asks for the used port (COM1, ......) and the baud<br />

rate of the unit.<br />

You do not have this information on hand? Simply try it out!<br />

The program keeps on sending this request until the actually<br />

used port and correct baud rate are entered.<br />

<br />

Data is read out and shown on the monitor<br />

divided in the sections<br />

>Einstellungen/SettingsAlarmspeicher/Alarms storedBlackbox<<br />

see example<br />

<br />

<br />

After pressing >Speichern/Save< a text file is<br />

compiled. The program proposes a filename -<br />

>C:\model description and barcode no.


Ultra-Low Refrigerated Circulators<br />

12. Installation of electronic module<br />

ALARM STAND-BY<br />

Caution:<br />

Always turn off the unit and disconnect the mains cable from the power source before<br />

performing any service or maintenance procedures, or before moving the unit.<br />

Configuration, installation, maintenance and repairs on the circulator may only be<br />

carried out by qualified personnel.<br />

B Turn off the unit with the mains switch and disconnect the<br />

power plug.<br />

A<br />

REG+<br />

E-PROG<br />

<br />

<br />

<br />

<br />

Open the screws (A) and remove the dummy plate.<br />

Carefully insert the upper edge (B) into the rear panel from<br />

below, align the electronic module at top and bottom and<br />

applying light pressure connect the 15-pole connector.<br />

Attach the electronic module using the screws (A).<br />

The circulator is ready for use. It automatically recognizes the<br />

installed electronic module.<br />

13. Maintaining the cooling performance<br />

In dusty environments, the refrigerating machine’s condenser<br />

should be cleaned by vacuuming every 1 to 2 months. The<br />

condenser is located behind the venting grid on the front of the unit,<br />

which can be taken off by removing the screws.<br />

<br />

<br />

<br />

<br />

<br />

Switch off the unit, disconnect mains power cable.<br />

Remove the venting grid.<br />

Clean the ribbed condenser with a vacuum cleaner.<br />

Replace the venting grid.<br />

Switch on the unit.<br />

79


Cleaning / repairing the unit<br />

14. Cleaning / repairing the unit<br />

Caution:<br />

Always turn off the unit and disconnect the mains cable from the power source before<br />

cleaning the unit. Prevent humidity from entering into the circulator.<br />

Electrical connections and any other work must be performed by qualified personnel<br />

only.<br />

Cleaning:<br />

For cleaning the bath tank and the immersed parts of the circulator, use low surface<br />

tension water (e.g., soap suds).<br />

Clean the outside of the unit using a wet cloth and low surface tension water.<br />

The circulator is designed for continuous operation under normal conditions. Periodic<br />

maintenance is not required.<br />

The tank should be filled only with a bath fluid recommended by JULABO. To avoid<br />

contamination, it is essential to change the bath fluid from time to time.<br />

Repairs<br />

Before asking for a service technician or returning a JULABO instrument for<br />

repair, please contact an authorized JULABO service station.<br />

When returning the unit:<br />

Clean the unit in order to avoid any harm to the service personnel.<br />

Attach a short fault description.<br />

If you intend to return your JULABO unit to us, you will find a Service Return Form<br />

on our website www.julabo.de (Sales & Service/Technical Support/Service Forms).<br />

Please use this as a delivery note and include it to the unit or send it in advance<br />

either by Fax or E-Mail.<br />

During transport the unit has to stand upright. Mark the packing correspondingly.<br />

When returning a unit, take care of careful and adequate packing.<br />

JULABO is not responsible for damages that might occur from insufficient packing.<br />

JULABO reserves the right to carry out technical modifications with repairs for<br />

providing improved performance of a unit.<br />

80

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