Development of a Novel Mass Spectrometric ... - Jacobs University

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Results and Discussion Intens. [%] 100 80 60 40 20 0 113.0 169.0 141.0 154.9 211.0 239.1 267.1 281.2 295.2 309.3 333.3 351.3 +MS 2 (351) 100 150 200 250 300 350 400 450 m/z Figure 3-32 APCI-MS 2 of pentacosane with precursor ion at m/z 351corresponding to (M-1) + Intens. [%] 100 80 154.9 168.9 182.9 197.0 225.0 239.1 295.2 281.1 309.3 323.3 +MS 2 (407) 60 40 20 127.0 337.3 351.3 365.3 389.4 405.2 0 100 150 200 250 300 350 400 m/z Figure 3-33 APCI-MS 2 of nonacosane with precursor ion at m/z 407 corresponding to (M-1) + Intens. [%] 100 80 60 40 20 0 132.9 144.8 186.9 172.9 198.8 269.0 283.1 297.1 325.2 311.1 337.2 351.2 365.2 379.3 393.3 407.3 421.2 433.2 449.3 +MS 2 (449) 150 200 250 300 350 400 450 500 m/z Figure 3-34 APCI-MS 2 of dotriacontane with precursor ion at m/z 449 corresponding to (M-1) + 67
Results and Discussion Intens. [%] 100 562.6 +MS 2 (562) 80 60 295.3 351.4 379.4 407.4 197.1 225.1 253.1 323.3 449.5 463.5 183.0 477.5 40 169.0 491.5 20 0 505.5 150 200 250 300 350 400 450 500 550 600 m/z 519.5 Figure 3-35 APCI-MS 2 of molecular ion of tetracontane (C40) at m/z 562 Intens. [%] 100 80 60 40 20 0 155.0 211.0 197.0 182.9 168.9 295.2 281.2 239.1 267.1 309.3 407.4 435.4 421.4 323.3 449.4 351.4 463.5 477.5 491.5 505.5 529.6 548.7 +MS 2 (548) 150 200 250 300 350 400 450 500 550 m/z Figure 3-36 APCI-MS 2 of molecular ion of nonatriacontane (C39) at m/z 548 Intens. [%] 100 80 60 295.2 225.0 267.1 211.0 253.1 337.3 365.3 351.3 421.4 379.4 407.4 435.4 449.5 +MS 2 (534) 40 20 0 168.9 463.5 515.5 155.0 534.6 491.4 150 200 250 300 350 400 450 500 550 m/z Figure 3-37 APCI-MS 2 of molecular ion of octatriacontane (C38) at m/z 534 68
Page 1 and 2:
Development of a Novel Mass Spectro
Page 3 and 4:
Declaration of Authorship I ,Nadim
Page 5 and 6:
This work has been carried out unde
Page 7 and 8:
Contents Contents Declaration of Au
Page 9 and 10:
List of Figures List of Figures Fig
Page 11 and 12:
List of Figures Figure 3-39 MS 2 fr
Page 13 and 14:
List of Tables List of Tables Table
Page 15 and 16:
Abbreviations Abbreviations APCI AP
Page 17 and 18:
Abbreviations UV VGOs VOCs VRs ultr
Page 19 and 20:
Introduction Analytical chemistry h
Page 21 and 22:
Introduction 1.2 Presence and Fate
Page 23 and 24:
Introduction aliphatic hydrocarbons
Page 25 and 26:
Introduction Figure 1-1 Examples of
Page 27 and 28:
Introduction Figure 1-2 Range of io
Page 29 and 30:
Introduction fractions. 42 Another
Page 31 and 32:
Introduction 1.3.5 APLI Other crude
Page 33 and 34: Introduction products). Other molec
Page 35 and 36: Introduction Other studies performe
Page 37 and 38: Introduction APLI-FT ICR-MS Crude o
Page 39 and 40: Introduction spectrometry in as muc
Page 41 and 42: Introduction catalytic processing t
Page 43 and 44: Introduction Figure 1-6 Kendrick ma
Page 45 and 46: Introduction including determinatio
Page 47 and 48: Introduction 1.5 Scope and Signific
Page 49 and 50: Experimental e) Other model mixture
Page 51 and 52: Experimental 2.2.2 Preparation of O
Page 53 and 54: Experimental 2.4 Graphical Presenta
Page 55 and 56: Results and Discussion experiment.
Page 57 and 58: Results and Discussion Intens. [%]
Page 59 and 60: Results and Discussion common featu
Page 61 and 62: Results and Discussion 3.2 APCI-TOF
Page 63 and 64: Results and Discussion These compou
Page 67 and 68: Results and Discussion Ions were pr
Page 71 and 72: Results and Discussion procedure ba
Page 75 and 76: Results and Discussion to produce m
Page 77 and 78: Results and Discussion 519.5863 519
Page 79 and 80: Results and Discussion Higher mass
Page 83: Results and Discussion Intens. [%]
Page 87 and 88: Results and Discussion isolated fro
Page 93 and 94: Results and Discussion 3.4.5 Tandem
Page 97 and 98: Results and Discussion injected int
Page 101 and 102: Results and Discussion 3.4.8 Quanti
Page 103 and 104: Results and Discussion Int. x 10000
Page 105 and 106: Results and Discussion Table 3.6 Qu
Page 107 and 108: Results and Discussion assessment o
Page 109 and 110: Results and Discussion hydrocarbons
Page 117 and 118: Results and Discussion of n-alkanes
Page 119 and 120: Results and Discussion flow (in I2)
Page 121 and 122: Results and Discussion Other intere
Page 123 and 124: Results and Discussion Figure 3-80
Page 125 and 126: Results and Discussion KMD 2.4 2.2
Page 127 and 128: Results and Discussion KMD 1.1 1 Le
Page 129 and 130: Results and Discussion 3.6.4 Asphal
Page 131 and 132: Conclusions In conclusion we could
Page 133 and 134: References References 1. Fay, R. M.
Page 135 and 136:
References 23. Colavecchia, M. V.,
Page 137 and 138:
References 47. Dzidic, I., Petersen
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References Hydroconversion Processe
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References 91. Golovlev, V. V., All
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Appendix Light shredder waste Meas.
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419.4592 C 30 H 59 419.4611 4.6 421
Page 147 and 148:
Liqui Moly car motor oil Meas. m/z
Page 149 and 150:
345.3511 C 25 H 45 345.3516 1.5 349
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