Development of a Novel Mass Spectrometric ... - Jacobs University

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545.5053 C 40 H 65 545.5081 5.1 547.5221 C 40 H 67 547.5237 2.9 549.5376 C 40 H 69 549.5394 3.2 551.5529 C 40 H 71 551.555 3.8 553.4754 C 41 H 61 553.4768 2.5 553.5721 C 40 H 73 553.5707 -2.5 555.4922 C 41 H 63 555.4924 0.4 557.5054 C 41 H 65 557.5081 4.8 559.5218 C 41 H 67 559.5237 3.4 561.5376 C 41 H 69 561.5394 3.2 563.553 C 41 H 71 563.555 3.5 565.5717 C 41 H 73 565.5707 -1.7 569.5075 C 42 H 65 569.5081 1 571.5247 C 42 H 67 571.5237 -1.7 573.5371 C 42 H 69 573.5394 4 575.5543 C 42 H 71 575.555 1.2 577.5695 C 42 H 73 577.5707 2 581.511 C 43 H 65 581.5081 -5 583.5244 C 43 H 67 583.5237 -1.2 585.5361 C 43 H 69 585.5394 5.6 587.5523 C 43 H 71 587.555 4.6 589.5701 C 43 H 73 589.5707 1 591.5995 C 43 H 75 591.5863 -2.2 597.5399 C 44 H 69 597.5394 -0.8 599.553 C 44 H 71 599.555 3.3 601.5699 C 44 H 73 601.5707 1.3 603.5848 C 44 H 75 603.5863 2.4 611.5556 C 45 H 71 611.555 -1 613.5693 C 45 H 73 613.5707 2.2 615.5842 C 45 H 75 615.5863 3.4 625.5717 C 46 H 73 625.5707 -1.6 627.5858 C 46 H 75 627.5863 0.8 629.594 C 46 H 77 629.602 1.2 639.585 C 47 H 75 639.5863 2.1 641.599 C 47 H 77 641.602 4.6 647.4623 C 49 H 59 647.4611 -1.8 653.622 C 48 H 77 653.602 -3 655.6155 C 48 H 79 655.6176 3.2 129
Liqui Moly car motor oil Meas. m/z Mol.Formula m/z error [ppm] 183.2109 C 13 H 27 183.2107 -1 197.2269 C 14 H 29 197.2264 -2.5 211.2416 C 15 H 31 211.242 1.9 225.257 C 16 H 33 225.2577 3.1 253.2886 C 18 H 37 253.289 1.5 267.3036 C 19 H 39 267.3046 3.7 281.3199 C 20 H 41 281.3203 1.4 295.3355 C 21 H 43 295.3359 1.3 309.3511 C 22 H 45 309.3516 1.6 323.3666 C 23 H 47 323.3672 1.8 337.3812 C 24 H 49 337.3829 5 351.3971 C 25 H 51 351.3985 4 365.4126 C 26 H 53 365.4142 4.4 379.4283 C 27 H 55 379.4298 4 393.4438 C 28 H 57 393.4455 4.3 407.46 C 29 H 59 407.4611 2.7 421.4765 C 30 H 61 421.4768 0.7 449.5067 C 32 H 62 449.5081 3.1 561.6322 C 40 H 81 561.6333 2 701.791 C 50 H 101 701.7898 -1.7 739.8029 C 53 H 103 739.8054 3.3 841.9416 C 60 H 121 841.9463 5.5 Contaminated-by-usage car motor oil Meas. m/z Mol. Formula m/z err [ppm] 175.1484 C 13 H 19 175.1481 -1.5 177.1645 C 13 H 21 177.1638 -4.3 179.18 C 13 H 23 179.1794 -3.3 181.1944 C 13 H 25 181.1951 3.9 183.2108 C 13 H 27 183.2107 -0.5 185.1318 C 14 H 17 185.1325 3.8 187.1476 C 14 H 19 187.1481 3.1 189.1629 C 14 H 21 189.1638 4.8 191.1786 C 14 H 23 191.1794 4.2 130
Page 1 and 2:
Development of a Novel Mass Spectro
Page 3 and 4:
Declaration of Authorship I ,Nadim
Page 5 and 6:
This work has been carried out unde
Page 7 and 8:
Contents Contents Declaration of Au
Page 9 and 10:
List of Figures List of Figures Fig
Page 11 and 12:
List of Figures Figure 3-39 MS 2 fr
Page 13 and 14:
List of Tables List of Tables Table
Page 15 and 16:
Abbreviations Abbreviations APCI AP
Page 17 and 18:
Abbreviations UV VGOs VOCs VRs ultr
Page 19 and 20:
Introduction Analytical chemistry h
Page 21 and 22:
Introduction 1.2 Presence and Fate
Page 23 and 24:
Introduction aliphatic hydrocarbons
Page 25 and 26:
Introduction Figure 1-1 Examples of
Page 27 and 28:
Introduction Figure 1-2 Range of io
Page 29 and 30:
Introduction fractions. 42 Another
Page 31 and 32:
Introduction 1.3.5 APLI Other crude
Page 33 and 34:
Introduction products). Other molec
Page 35 and 36:
Introduction Other studies performe
Page 37 and 38:
Introduction APLI-FT ICR-MS Crude o
Page 39 and 40:
Introduction spectrometry in as muc
Page 41 and 42:
Introduction catalytic processing t
Page 43 and 44:
Introduction Figure 1-6 Kendrick ma
Page 45 and 46:
Introduction including determinatio
Page 47 and 48:
Introduction 1.5 Scope and Signific
Page 49 and 50:
Experimental e) Other model mixture
Page 51 and 52:
Experimental 2.2.2 Preparation of O
Page 53 and 54:
Experimental 2.4 Graphical Presenta
Page 55 and 56:
Results and Discussion experiment.
Page 57 and 58:
Results and Discussion Intens. [%]
Page 59 and 60:
Results and Discussion common featu
Page 61 and 62:
Results and Discussion 3.2 APCI-TOF
Page 63 and 64:
Results and Discussion These compou
Page 65 and 66:
Page 67 and 68:
Results and Discussion Ions were pr
Page 69 and 70:
Page 71 and 72:
Results and Discussion procedure ba
Page 73 and 74:
Page 75 and 76:
Results and Discussion to produce m
Page 77 and 78:
Results and Discussion 519.5863 519
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Results and Discussion Higher mass
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Page 83 and 84:
Page 85 and 86:
Page 87 and 88:
Results and Discussion isolated fro
Page 89 and 90:
Page 91 and 92:
Page 93 and 94:
Results and Discussion 3.4.5 Tandem
Page 95 and 96: Results and Discussion Intens. [%]
Page 97 and 98: Results and Discussion injected int
Page 101 and 102: Results and Discussion 3.4.8 Quanti
Page 103 and 104: Results and Discussion Int. x 10000
Page 105 and 106: Results and Discussion Table 3.6 Qu
Page 107 and 108: Results and Discussion assessment o
Page 109 and 110: Results and Discussion hydrocarbons
Page 117 and 118: Results and Discussion of n-alkanes
Page 119 and 120: Results and Discussion flow (in I2)
Page 121 and 122: Results and Discussion Other intere
Page 123 and 124: Results and Discussion Figure 3-80
Page 125 and 126: Results and Discussion KMD 2.4 2.2
Page 127 and 128: Results and Discussion KMD 1.1 1 Le
Page 129 and 130: Results and Discussion 3.6.4 Asphal
Page 131 and 132: Conclusions In conclusion we could
Page 133 and 134: References References 1. Fay, R. M.
Page 135 and 136: References 23. Colavecchia, M. V.,
Page 137 and 138: References 47. Dzidic, I., Petersen
Page 139 and 140: References Hydroconversion Processe
Page 141 and 142: References 91. Golovlev, V. V., All
Page 143 and 144: Appendix Light shredder waste Meas.
Page 145: 419.4592 C 30 H 59 419.4611 4.6 421
Page 149 and 150: 345.3511 C 25 H 45 345.3516 1.5 349
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