Development of a Novel Mass Spectrometric ... - Jacobs University

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References 102. Rodgers, R. P., White, F. M., Hendrickson, C. L., Marshall, A. G., Andersen, K. V., Resolution, elemental composition, and simultaneous monitoring by Fourier transform ion cyclotron resonance mass spectrometry of organosulfur species before and after diesel fuel processing. Analytical Chemistry 1998, 70, 4743-4750. 103. Panda, S. K., Schrader, W., al-Hajji, A., Andersson, J. T., Distribution of polycyclic aromatic sulfur heterocycles in three Saudi Arabian crude oils as determined by Fourier transform ion cyclotron resonance mass spectrometry. Energy & Fuels 2007, 21, 1071-1077. 104. Wu, Z. G., Rodgers, R. P., Marshall, A. G., ESI FT-ICR mass spectral analysis of coal liquefaction products. Fuel 2005, 84, 1790-1797. 105. Hughey, C. A., Hendrickson, C. L., Rodgers, R. P., Marshall, A. G., Qian, K. N., Kendrick mass defect spectrum: A compact visual analysis for ultrahighresolution broadband mass spectra. Analytical Chemistry 2001, 73, 4676-4681. 106. Kendrick, E., A mass scale based on CH 2 =14.0000 for high resolution mass spectrometry of organic compounds. Analytical Chemistry 1963, 35, 2146. 107. Nourreddine, M., Recycling of auto shredder residue. Journal of Hazardous Materials 2007, 139, 481-490. 108. LAGA (2004): Bestimmung des Gehaltes an Kohlenwasserstoffen in Abfällen - Untersuchungs-und Analysenstrategie-Kurzb- ezeichnung: KW/04. Metteilung der Länderarbeitsgemeinschaft Abfall (LAGA) 35, Stand 16.11.2004, 36 S. 109. Carroll, D. I.; Dzidic, I.; Horning, E. C.; Stillwell, R. N., Atmospheric-pressure ionization mass-spectrometry. Applied Spectroscopy Reviews 1981, 17, 337-406. 110. DIN EN 14039 : 12-2000, Charakterisierung von Abfällen -Bestimmung des Gehalts an Kohlenwasserstoffen von C10 bis C40 mittels Gaschromatographie. Deutsches Institute für Normung, 20 S. 111. Luosujarvi, L., Karikko, M. M., Haapala, M., Saarela, V., Huhtala, S., Franssila, S., Kostiainen, R., Kotiaho, T., Kauppila, T. J., Gas chromatography/mass spectrometry of polychlorinated biphenyls using atmospheric pressure chemical ionization and atmospheric pressure photoionization microchips. Rapid Communications in Mass Spectrometry 2008, 22 (4), 425-431. 112. Yamada, M.; Suga, M.; Waki, I.; Sakamoto, M.; Morita, M., Continuous monitoring of polychlorinated biphenyls in air using direct sampling APCI/ITMS. International Journal of Mass Spectrometry 2005, 244 (1), 65-71. 113. Field, F. H., Chemical ionization mass spectrometry. Accounts of Chemical Research 1968, 1, 42. 125
Appendix Light shredder waste Meas. m/z Mol.Formula m/z error [ppm] 189.163 C 14 H 21 189.1638 4.2 191.1789 C 14 H 23 191.1794 2.6 193.1941 C 14 H 25 193.1947 3.1 195.2105 C 14 H 27 195.2107 1 197.2259 C 14 H 29 197.2264 2.5 199.1477 C 15 H 19 199.1481 2 201.164 C 15 H 21 201.1638 -1 203.1796 C 15 H 23 203.1794 -1 205.1954 C 15 H 25 205.1951 -1.5 207.211 C 15 H 27 207.2107 -1.5 209.2266 C 15 H 29 209.2264 -1 211.2422 C 15 H 31 211.242 -1 213.1647 C 16 H 21 213.1638 -4.2 215.1804 C 16 H 23 215.1794 -4.6 217.1956 C 16 H 25 217.1951 -2.3 219.2109 C 16 H 27 219.2107 -0.9 221.2274 C 16 H 29 221.2264 -4.5 223.2427 C 16 H 31 223.242 -3 225.2586 C 16 H 33 225.2577 -4 231.212 C 17 H 27 231.211 -4.3 233.2273 C 17 H 29 233.2264 -3.8 235.2429 C 17 H 31 235.242 -3.8 237.258 C 17 H 33 237.2577 -1.3 239.274 C 17 H 35 239.2733 -3 241.1965 C 18 H 25 241.1958 -2.9 245.2276 C 18 H 29 245.2264 -4.9 247.2432 C 18 H 31 247.242 -4.8 249.2591 C 18 H 33 249.2583 -3.2 251.274 C 18 H 35 251.2733 -2.8 253.2904 C 18 H 37 253.291 2.4 261.2592 C 19 H 33 261.2599 2.6 263.2747 C 19 H 35 263.2752 1.8 265.2884 C 19 H 37 265.289 2.3 267.3051 C 19 H 39 267.3046 -1.9 279.3057 C 20 H 39 279.3046 -4 281.3214 C 20 H 41 281.3203 -3.9 126
Page 1 and 2:
Development of a Novel Mass Spectro
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Declaration of Authorship I ,Nadim
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This work has been carried out unde
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Contents Contents Declaration of Au
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List of Figures List of Figures Fig
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List of Figures Figure 3-39 MS 2 fr
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List of Tables List of Tables Table
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Abbreviations Abbreviations APCI AP
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Abbreviations UV VGOs VOCs VRs ultr
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Introduction Analytical chemistry h
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Introduction 1.2 Presence and Fate
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Introduction aliphatic hydrocarbons
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Introduction Figure 1-1 Examples of
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Introduction Figure 1-2 Range of io
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Introduction fractions. 42 Another
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Introduction 1.3.5 APLI Other crude
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Introduction products). Other molec
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Introduction Other studies performe
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Introduction APLI-FT ICR-MS Crude o
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Introduction spectrometry in as muc
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Introduction catalytic processing t
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Introduction Figure 1-6 Kendrick ma
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Introduction including determinatio
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Introduction 1.5 Scope and Signific
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Experimental e) Other model mixture
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Experimental 2.2.2 Preparation of O
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Experimental 2.4 Graphical Presenta
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Results and Discussion experiment.
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Results and Discussion Intens. [%]
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Results and Discussion common featu
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Results and Discussion 3.2 APCI-TOF
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Results and Discussion These compou
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Results and Discussion Ions were pr
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Results and Discussion procedure ba
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Results and Discussion to produce m
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Results and Discussion 519.5863 519
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Results and Discussion Higher mass
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Results and Discussion isolated fro
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Page 91 and 92: Results and Discussion Intens. [%]
Page 93 and 94: Results and Discussion 3.4.5 Tandem
Page 97 and 98: Results and Discussion injected int
Page 101 and 102: Results and Discussion 3.4.8 Quanti
Page 103 and 104: Results and Discussion Int. x 10000
Page 105 and 106: Results and Discussion Table 3.6 Qu
Page 107 and 108: Results and Discussion assessment o
Page 109 and 110: Results and Discussion hydrocarbons
Page 117 and 118: Results and Discussion of n-alkanes
Page 119 and 120: Results and Discussion flow (in I2)
Page 121 and 122: Results and Discussion Other intere
Page 123 and 124: Results and Discussion Figure 3-80
Page 125 and 126: Results and Discussion KMD 2.4 2.2
Page 127 and 128: Results and Discussion KMD 1.1 1 Le
Page 129 and 130: Results and Discussion 3.6.4 Asphal
Page 131 and 132: Conclusions In conclusion we could
Page 133 and 134: References References 1. Fay, R. M.
Page 135 and 136: References 23. Colavecchia, M. V.,
Page 137 and 138: References 47. Dzidic, I., Petersen
Page 139 and 140: References Hydroconversion Processe
Page 141: References 91. Golovlev, V. V., All
Page 145 and 146: 419.4592 C 30 H 59 419.4611 4.6 421
Page 147 and 148: Liqui Moly car motor oil Meas. m/z
Page 149 and 150: 345.3511 C 25 H 45 345.3516 1.5 349
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