Kurzübersicht von ausgewählten chemischen Synthesen im ...

Kurzübersicht von ausgewählten chemischen Synthesen 

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Title Authors Date Publication 

Microwave-Promoted Heck Coupling 

Using Ultralow Metal Catalyst 

Concentrations 

Microwave-Assisted Synthesis of 

Isonitriles: A General Simple 

Methodology 

Microwave-assisted solventless single and 

double addition of HP(O)Ph2 to alkynes 

Organo Soluble Copper Clusters as 

Precatalysts for Carbon-Heteroelement 

Bond-Forming Reactions: Microwave and 

Conventional Heating 

Microwave-Assisted Regioselective 

Addition of P(O)-H Bonds to Alkenes 

without Added Solvent or Catalyst 

Arvela, RK; Leadbeater, NE 2005 J. Org. Chem., 2005, 70, 1786-1790. 

Porcheddu, A.; Giacomelli, G.; 

Salaris, M. 

Stone, JJ; Stockland, RA; Reyes, 

JA; Kovach, J; Goodman, CC; 

Tillman, ES 

Manbeck, GF; Lipman, AJ; 

Stockland, RA; Freidl, AL; 

Hasler, AF; Stone, JJ; Guzei, IA 

Patel, PB; Stockland, RA; Taylor, 

RI; Thompson, LE 

2005 J. Org. Chem., 2005, 70, 2361-63. 

2005 Journal of Molecular Catalysis A: Chemical 226(2005) 11-21 

2005 J Org Chem 2005, 70, 244-250 

2005 Org Lett, Vol Y, No Z, 2005, xxx-xxx+3

Palladium-Catalyzed Cross-Coupling of 

Aryl Triethylammonium Bis(catechol) 

Silicates with Aryl Bromides Using 

Microwave Irradiation 

Efficient Microwave Enhanced 

Synthesis of 4-Thiazolidinones 

Highly Efficient Microwave-assisted 

Fluorous Ugi and Post-condensation 

Reactions for Benzidazoles and 

Quinoxalinones 

A Preparative Microwave Method for the 

Isomerisation of 4,16dibromo[2.2]paracyclophane 

into 4,12dibromo[2.2]paracyclophane 

Microwave-Mediated Intramolecular Diels- 

Alder Cyclization of biodihydroxylated 

Benzoic Acid Derivatives 

Seganish, WM; DeShong, P 2004 Org Lett, Vol 6, No 23, 2004, 4379-4381 

Gududuru, V.; Nguyen, V.; 

Dalton, J. T.; Miller, D. D. 

2004 Synlett, 2004, 2357-2358. 

Tempest, P; Zhang, W 2004 Tetrahedron Lett., 2004, 45, 6757-6760 

Braddock, DC; Ahmad, SM; 

Douglas, GT 

Mihovilovic, MD; Leisch, HG; 

Mereiter, K 

2004 Tetrahedron Lett., 2004, 45, 6583-6585 


Rapid Palladium-Catalyzed Aminations of 

Aryl Chlorides with Aliphatic Amines Maes, BUW; Loones, KTJ; 

Under Temperature-Controlled Microwave Lemiere, GLF; Dommisse, RA 

Heating 

Microwave-Assisted Allylation of Acetals 

2004 Synlett 2003, No. 12, pp.1822-1825 

with Allyltrimethylsilane in the Presence of Jung, ME; Maderna A 

CuBr 

Microwve-assisted preparation of cyclic 

2004 J Org Chem 2004, 69, 7755-7757 

ureas from diamines in the presence of 

ZnO 

Kim YJ; Varma, RS 2004 Tetrahedron Lett., 2004, 45, 7205-7208

Efficient Palladium-Catalyzed Cross- 

Coupling of beta- 

Chloroalkylidene/arylidene Malonates 

Using Microwave Chemistry 

Microwave-assisted Direct Addition of 

Cycloethers to Alkynes 

Recent Advances in Microwave-Assisted 

Synthesis 

Sunfish Amphiphiles: Conceptually New 

Carriers for DNA Delivery 

Rh(I)-catalyzed solvent-free orthoalkylation 

of aromatic imines under 

microwave irradiation 

Efficient O- and N-(B-Fluoroethylation)s 

with NCA [ 18 F] B-Fluoroethyl tosylate with 

amines under microwave-enhanced 

conditions 

Microwave-Assisted Preparation of 

Aryltetrazoleborate Esters 

A Sterochemical Surprise at the Late Stage 

of the Synthesis of Fully N-Differentiated 

Heparin Oligosaccharides Containing 

Amino, Acetoamido, and N-Sulfonate 

Groups 

Microwave Synthesis of Iridium (III) 

Complexes: Synthesis of Highly Efficient 

Orange Emitters in Organic Light- 

Emitting Diodes 

Poondra, RR; Fischer PM; 

Turner, NJ 

2004 J Org Chem 2004, 69, 6920-6922 

Shang, Y; Li, CJ 2004 Tetrahedron Lett., 2004, 45, 7581-7584 

Hayes, BL 2004 Aldrichemica ACTA, Vol 37, No 2, 2004, 66-77 

Hulst, R; et al 2004 Eur J Org Chem, 2004, 835-849 

Thanh, GV; Lohrache, H; Loupy, 

A; Kim, I-J; Chang, D-H; Jun, C- 

H. 

Lu SY; Chin, FT; McCarron, JA; 

Pike V 

Coats, S.J; Hlasta, D.J; Schulz, 

M.J. 

2004 Tetrahedron, 2004, 60, 5539-5543 

2004 J. Labelled Compd. Radiopharm., 2004, 47, 289-297 

2004 Org Lett, Vol 6, No 19, 2004, 3265-3268 

Johman, G.J.S; Seeberger, P. 2004 J Org Chem 2004, 69, 4081-4093 

Saito, K; Matsusue, N; Kanno, H; 

Hamada, Y; Takahashi, H; 

Matsumura, T 

2004 Jpn J Appl Phys, Vol 43, No 5A (2004), 2733-2734

Aqueous N-alkylation of amines using alkyl 

halides: direct generation of tertiary 

amines under microwave irradiation 

Rh(I)-Catalyzed Ring Opening of an 

Ju, Y; Varma, R. 2004 Green Chem., 2004, 6, 219-221 

IMDAF-Derived Oxabicyclo Cycloadduct 

Padwa, A; Wang, Q. 

as the Key Step in the Synthesis of (+/-)-epi- 

Zephyranthine 

2004 Org Lett, 2004, 6(13) 2189-2192 

Fluorous Synthesis of Heterocyclic Systems Zhang, W 2004 Chem Rev. 2004, 104, 2531-2556 

Novelties of microwave assisted liquidliquid 

phase transfer catalysis in 

enhancement rates and selectivities in 

alkylation of phenols under mild conditions 

Yadav, G.P; Bisht, P.M. 2004 Catalysis Communications 5 (2004) 259-263 

Microwave-assisted N-arylation of a 

sulfoximine with aryl chlorides 

Unexpectedly Selective Formation and 

Reactions of Epoxycyclooctenones under 

Microwave-Mediated Conditions 

Harmata, M; Hong, X, Ghosh, SK 2004 Tetrahedron Lett, 2004, 45, 5233-5236 

Fawcett, J; Griffith, G; Percy, J; 

Uneyama, E. 

A traceless perfluorooctosulfonyl tag for 

Zhang, W;Chen, C.H.-T; Lu, Y; 

deoxygenation of phenols under microwave 

Nagashima, T 

irradiation 

Microwave-Assisted Parallel Synthesis of a 

4,6-Diamino-2,2-dimethyl-1,2-dihydro-1phenyl-s-triazine 

Library 

A Highly Efficient Microwave-Assisted 

Suzuki Coupling Reaction of Aryl 

Perfluorooctylsulfonates with Boronic 

Acids 

2004 Org Lett, Vol 6, No 8, 2004, 1277-1280 


Lee, H-K; Rana, T. 2004 J Combi Chem; 2004 6(4); 504-508 

Zhang, W;Chen, C.H.-T; Lu, Y; 

Nagashima, T 

2004 Org Lett, 2004, 6(9); 1473-1476

Molybdenum-catalyzed asymmetric allylic 

alkylations 

Six vs. Five-Membered Ring Formation in 

Radical Cyclizations of 7-Bromo- 

Substituted Hexahydroindolinones 

Belda, O; Moberg, C 2004 Acc. Chem. Res., 2004, 37, in press 

Ozdemir, AD; Padwa, A; 

Rashatasakhon, P; Willis, J. 

2004 Org Lett, 2004, 6(6); 917-920 

Facile syntheses of oxazolines and 

Katritzky, AR; Cai, C; Suzuki, K; 

thiazolines with N-acylbenzotriazoles under 

Singh, SK 


2004 J. Org. Chem., 2004, 69, 811-814 

Microwave-Assisted Paal-Knorr Reaction. 

Minetto, G; Raveglia, LF; Taddei, 

A Rapid Approach to Substituted Pyrroles 

M 

and Furans 

Microwave-assisted synthesis of allylic 

2004 Org Lett, 2004, (6)3; 389-392 

amines: considerable rate acceleration in 

the hydrozirconation-transmetalationaldimine 

addition sequence 

Wipf, P; Janjic, J; Stephenson, 

C.R.J 

2004 Org. Biomol. Chem., 2004, 2, 443-445 

Traceless synthesis of hydantoin by focused 

Lee, MJ; Sun, CM 



Microwave assisted Petasis boronic- 

Mannich reactions 

A "catch and release" strategy for the 

parallel synthesis of 2,4,5-trisubstituted 

pyrimidines 

Green Polymer Chemistry:Microwave- 

Assisted Single Step Synthesis of Various 

(Meth)acrylamides and 

Poly(meth)acrylamides Directly from 

(Meth)acrylic Acid and Amines 

McLean, NJ; Tye, H; Whittaker, 

M 

Porcheddu, A; Giacomelli, G; De 

Luca, L; Ruda, AM 

Goretzki, C: Krlej, J; Ritter, H; 

Steffens, C. 


2004 J. Comb. Chem., 2004, 6, 105-11 

2004 Macromol Rapid Commun, 2004, 25, 513-516

Soluble polymer-supported synthesis of 

thioxotetrapyrimidinone by focused 


Liquid phase synthesis of chiral 

quinoxalinones by microwave irradiation 

Microwave enhanced formation of electron 

rich arylboronates 

Fast and easy halide exchange in aryl 

halides 

Sun, CM; Yeh, WB 2004 J. Comb. Chem., 2004, 6, in press 

Tung, CL; Sun, CM 2004 Tetrahedron Lett., 2004, 45, 1159-62 

Appukkuttan, P; Van der Eycken, 

E; Dehaen, W 

2003 Synlett, 2003, 8, 1204-06 

Arvela, RK; Leadbeater, NE 2003 Synlett, 2003, 8, 1145-48 

Microwave-assisted heterocyclic synthesis Katritzky, AR; Singh, SK. 2003 ARKOVIC 2003 (xiii) 68-86 

Microwave Assisted N-Chlorination of 

Secondary Amines 

Rapid cyanation of aryl iodides in water 

using microwave promotion 

Katritzky, AR; Majumder, S; Jain, 

R 

Arvela, RK; Leadbeater, NE; 

Torenius, HM; Tye, H 

2003 ARKOVIC 2003 (xiii) 74-79 

2003 Org. Biomol. Chem., 2003, 1, 1119-21 

Synthesis of NCA [carbonyl-11C] amides 

by direct reaction of in situ generated [11C] 

Lu SY; Hong, J; Pike V 

carboxymagnesium halides with amines 

under microwave-enhanced conditions 

2003 J. Labelled Compd. Radiopharm., 2003, 46, 1-11 

Rapid, easy cyanation of aryl bromides and 

chlorides using nickel salts in conjunction 

with microwave promotion 

Highly efficient synthesis of pyrimidines 

under microwave-assisted conditions 

Single-mode microwave synthesis in 

organic materials chemistry 

Arvela, RK; Leadbeater, NE 2003 J. Org. Chem, 2003, 68, 9122-25 

Bagley, MC; Hughes, DD; Taylor, 

PH 

2003 Synlett, 2003, 2, 259-61 

Barlow, S; Marder, SR 2003 Adv. Funct. Mater., 2003, 13, 517-18

Microwave-assisted [3 + 2] cycloadditions 

of azomethine ylides 

Rapid synthesis of α-ketoamides using 

microwave irradiation-simultaneous 

cooling method 

Intramolecular cyclization reactions of 5halo- 

and 5-nitro-substituted furans 

Cellulose beads: a new versatile solid 

support for microwave-assisted synthesis. 

Preparation of pyrazole and isoxazole 

libraries. 

Eco-friendly microwave-assisted scaleable 

synthesis of 2-cyanobenzothiazoles via N- 

arylimino-1,2,3-dithiazoles 

Novel 6-substituted benzothiazol-2-yl 

indolo[1,2-c]quinazolines and 

benzimidazo[1,2-c]quinazolines 

Fluorous technologies for solution-phase 

high-throughput organic synthesis 

Bashiardes, G; Safir, I; Mohamed, 

AS; Barbot, F; Laduranty, J 

2003 Org. Lett., 2003, 5, 4915-18 

Chen, JJ; Deshpande, SV 2003 Tetrahedron Lett., 2003, 44, 8873-76 

Crawford, KR; Bur, SK; Straub, 

CS; Padwa, A 

De Luca, L; Giacomelli, G; 

Porcheddu, A; M Salaris; Taddei, 

M 

2003 Org. Lett., 2003, 5, 3337-40 

2003 J. Comb. Chem., 2003, 5, 465-71 

Frere, S; Thiery, V; Besson, T 2003 Synth. Commun., 2003, 33, 3795-804 

Frere, S; Thiery, V; Bailly, C; 

Besson, T 

A method for generating nitrile oxides from 

Giacomelli, G; De Luca, L; 

nitroalkanes: a microwave assisted route 

Porcheddu, A 

for isoxazoles 

Microwave-assisted solution-phase 

synthesis of 1,4,5-trisubstituted pyrazoles 

Microwave-assisted functionalization of 

bromo-fluorescein and bromorhodamine 

derivatives 

A new β-carbolinone synthesis using a 

Rh(II)-promoted [3+2]-cycloaddition and 

Pd(0) cross-coupling/Heck cyclization 

2003 Tetrahedron, 2003, 59, 773-79 

Zhang, W 2003 Tetrahedron, 2003, 59, 4475-4489 

Giacomelli, G; Porcheddu, A; 

Salaris, M; Taddei, M 

2003 Tetrahedron, 2003, 59, 5437-40 

2003 Eur. J. Org. Chem., 2003, 537-41 

Han, JW; Castro, JC; Burgess, K 2003 Tetrahedron Lett., 2003, 44, 9359-62 

Harris, JM; Padwa, A 2003 Org. Lett., 2003, 5, 4195

chemistry 

Solid-supported cyclohexane-1,3-dione 

(CHD): a "capture and release" reagent for Humphrey, CE; Easson, MAM; 

the synthesis of amides and novel scavenger Tierney, JP; Turner, NJ 

resin 

2003 Org. Lett., 2003, 5, 849-52 

Microwave-assisted multi-component 

synthesis of fused 3-aminoimidazoles 

Ireland, SM; Tye, H; Whittaker, M 2003 Tetrahedron Lett., 2003, 44, 4369-71 

Microwave-assisted syntheses of 

regioisomerically pure bromorhodamine 

derivatives 

Jiao, GS; Castro, JC; Thoresen, 

LH; Burgess, K 

2003 Org. Lett., 2003, 5, 3675-77 

Microwave-assisted Mannich-type threecomponent 

reactions 

Leadbeater, NE; Torenius, HM; 

Tye, H 

2003 Molec. Diversity, 2003, 7, 135-44 

Microwave-enhanced transition metalcatalyzed 

decoration of 2(1H)-pyrazinone 

Rapid and amenable Suzuki coupling 

reaction in water using microwave and 

conventional heating 

Transition-metal-free Suzuki-type coupling 

reactions 

Transition-metal-free Suzuki-type coupling 

reactions: scope and limitations of the 

methodology 

Microwave-assisted traceless synthesis of 

thiohydantoin 

The first rapid palladium-catalyzed 

aminations of (azahetero)aryl chlorides 

under temperature-controlled microwave 

Bisztray, K; Dehaen, W; Kappe, 

O; Kaval, N; Van der Eycken, E; 


Leadbeater, NE; Marco, M 2003 J. Org. Chem., 2003, 68, 888-92 

Leadbeater, NE; Marco, M 2003 Angew. Chem. Intl. Ed., Eng., 2003, 42, 1407-09 

Leadbeater, NE; Marco, M 2003 J. Org. Chem., 2003, 68, 5660-67 

Lin, MJ; Sun, CM 2003 Tetrahedron Lett., 2003, 44, 8739-42 

Maes, BUW; Loones, KTJ; 

Lemiere, GLF; Dommisse, RA 

2003 Synlett, 2003, 12, 1822-25

heating 

Microwave-assisted saccharide coupling 

with n-pentenyl glycosyl donors 

Microwave-assisted synthesis of galactooligosaccharides 

from lactose with 

immobilized β-galactosidase from 

Kluyveromyces lactis 

Studies on high-temperature amination 

reactions of aromatic chlorides using 

discrete palladium-N-heterocyclic carbene 

(NHC) complexes and in situ 

palladium/imidazolium salt protocols 

Combination of Microwave reactions with 

fluorous separations in the palladium 

catalyzed synthesis of aryl sulfides 

Focused Microwave-Assisted Synthesis of 

2,5 Dihydrofuran Derivatives as Electron 

Acceptors for Highly Efficient Nonlinear 

Optical Chromophores 

Mathew, F; Jayaprakash, KN; 

Fraser-Reid, B; Mathew, J; 

Scicinski, J 

Maugard, T; Gaunt, D; Legoy, 

MD; Besson, T 

McCarroll, AJ; Sandham, DA; 

Titcomb, LR; de K. Lewis, AK; 

Cloke, FGN; Davies, BP; de 

Santana, AP; Hiller, W; Caddick, 

S 


2003 Biotech. Lett., 2003, 25, 623-29 


Zhang, W;Chen, C.H.-T; Lu, Y 2003 Molec. Diversity, 2003, 7, 199-202 

Liu, S; Haller, MA; Ma, H; Dalton 

LR; Jang SH; Jen, AKY 

High-throughput catch-and-release 

synthesis of oxazoline hydroxamates, 

structure-activity relationships in novel Pirrung, MC; Tumey, LN; 

inhibitors of Escherichia coli LpxC: in vitro McClerren, AL; Raetz, CRH 

enzyme inhibition and antibacterial 

properties 

2003 Adv. Mater. 2003, 15, No. 7-8, April 17 

2003 J. Am. Chem. Soc., 2003, 125, 1575-86

A new, rapid, general procedure for the 

synthesis of organic molecules supported Porcheddu, A; Ruda, GF; Sega, A; 

on methoxy-polyethylene glycol (MeOPEG) Taddei, M 

under microwave irradiation conditions 

A study of the synthesis of triazoles using 


Synthesis of pyridinyl-pyrimidines via Pdcatalyzed 

cross-coupling reactions: a 

comparison of classical thermal and 

microwave assisted reaction conditions 

Stereochemical diversity through 

cyclodimerization: synthesis of polyketide- 

like macrodiolides 

Hydrogen transfer type oxidation of 

alcohols by rhodium and ruthenium 

catalyst under microwave irradiation 

Microwave-assisted ruthenium-catalyzed 

olefin metathesis under solvent-free 

conditions 

Application of microwaves in organic 

synthesis: a rapid and efficient synthesis of 

new 3-aryl-2-imino-4-methyl-2,5dihydrofurans 

and 3-aryl-3-2-(5H)furanones. 

An easy synthesis of thermochromic 

ethylenes under microwave irradiation 

Nickel and palladium catalysed reaction of 

triethyl phosphite with aryl halides under 


Savin, KA; Robertson, M; Gernert, 

D; Green, S; Hembre, EJ; Bishop, 

J 

Stanetty, P; Schnurch, M; 

Mihovilovic, MD 

Su, Q; Beeler, AB; Lobkovsky, E; 

Porco Jr., JA; Panek, JS 

Takahashi, M; Oshima, K; 

Matsubara, S 

2003 Eur. J. Org. Chem., 2003, 907-12 


2003 Synlett, 2003, 12, 1862-64 

2003 Org. Lett., 2003, 5, 2149-52 


Thanh, GV; Loupy, A 2003 Tetrahedron Lett., 2003, 44, 9091-94 

Villemin, D; Liao, L 2003 Synth. Commun., 2003, 33, 1575-86 

Villemin, D; Hachemi, M; 

Hammadi, M 

Villemin, D; Elbilali, A; Simeon, 

F; Jaffres, PA; Maheut, G; 

Mossaddak, M; Hakiki, A 

2003 J. Chem. Res. (S), 2003, 260-61 

2003 J. Chem. Res. (S), 2003, 436-37

Optimisation of solvent free parallel 

synthesis under microwave irradiation: 

synthesis of new arylacrylonitriles 

Synthesis of 4-arylideneisochroman-1,3dione 

under microwave irradiation 

Fluorous dienophiles are powerful diene 

scavengers in Diels-Alder reactions 

Microwave enabled external 

carboxymethyl substituents in the ring- 

closing metathesis 

Microwave-enhanced liquid-phase 

synthesis of thiohydantoins and 

thioxotetrahydropyrimidinones 

Microwave-assisted Niementowski 

reaction. Back to the roots. 

Microwave-assisted synthesis of 5-deaza- 

5,8-dihydropterins 

A new one-step synthesis of pyridines 

under microwave-assisted conditions 

The Claisen RearrangementFollowed by 

Phenol Oxidation: A Simple Route to 

Naturally Occuring Benzoquinones 

Including an Ansa-Bridged Derivative 

Related to Ansamycin Antibiotics 

Microwave-assisted solid-phase synthesis of 

5-carboxamido-N-acetyltryptamine 

derivatives 

Villemin, D; Jullien, A; Bar, N 2003 Green Chem., 2003, 5, 467-69 

Villemin, D; Bar, N; Khalid, M; 

Jaffres, PA; Santos, JSO 

2003 J. Chem. Res. (S), 2003, 433-35 

Werner, S; Curran, DP 2003 Org. Lett., 2003, 5, 3293-96 

Yang, C; Murray, WV; Wilson, LJ 2003 Tetrahedron Lett., 2003, 44, 1783-86 

Yeh, WB; Lin, MJ; Lee, MJ; Sun, 

CM 

Alexandre, FR; Berecibar, A; 

Besson, T 



Bagley, MC; Singh, N 2002 Synlett., 2002, 10, 1718-20 

Bagley, MC; Lunn, R; Xiong, X 2002 Tetrahedron Lett., 2002, 43, 8331-34 

Davis, CJ; Moody, CJ 2002 Synlett 2002, No 11, 1874-1876 

Finaru, A; Berthault, A; Besson, 

T; Guillaumet, G; Berteina- 

Raboin, S 

2002 Org. Lett., 2002, 4, 2613-15

Biosynthesis inspired Diels-Alder route to 

pyridines: synthesis of the 2,3dithiazolylpyridine 

core of thiopeptide 

therapeutics 

Microwave-assisted synthesis of 5carboxymethoxy-N-acetyltryptamine 

derivatives 

Synthesis of C-carbamoyl-1,2,3-triazoles by 

microwave-induced 1,3-dipolar 

cycloaddition of organic azides to 

acetylenic amides 

Ligand-free palladium catalysis of the 

Suzuki reaction in water using microwave 

heating 

A study of the ionic liquid mediated 

microwave heating of organic solvents 

The angiogenesis inhibitor Epoxyquinol A: 

total synthesis and inhibition of 

transcription factor NF-kB. 

Alcaraz, L; Hughes, R A; Moody, 

CJ; Thompson, SP. 

Finaru, A; Berthault, A; Besson, 

T; Guillaumet, G; Berteina- 

Raboin, S 

2002 Chem Comm, 2002, 1760-1761 


Katritzky, AR; Singh, SK 2002 J. Org. Chem., 2002, 67, 9077-79 

Leadbeater, NE; Marco, M 2002 Org. Lett., 2002, 4, 2973-76 

Leadbeater, NE; Torenius, HM 2002 J. Org. Chem., 2002, 67, 3145-48 

Li, C; Bardhan, S; Pace, EA; 

Liang, MC; Gilmore, TD; Porco, 

JA 

2002 Org. Lett., 2002, 4, 3267-70

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