COMBI-CRYSTAL-PET® (CC-PET®) - Suurmond
COMBI-CRYSTAL-PET® (CC-PET®) - Suurmond
COMBI-CRYSTAL-PET® (CC-PET®) - Suurmond
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<strong>COMBI</strong>-<strong>CRYSTAL</strong>-PET ® (<strong>CC</strong>-PET ® )<br />
PET direct crystallization – energy savings in a reliable process<br />
<strong>CC</strong>-PET ® combines pelletizing, drying, and<br />
crystallization in a single process. Therefore,<br />
the crystalline PET pellets can directly be used<br />
for extrusion downstream processing. The<br />
pellets are almost dust-free and can be reliably<br />
processed at high bulk density. As pelletizing<br />
and direct crystallizing are combined into one<br />
single step, a lot of energy is saved. <strong>CC</strong>-PET ®<br />
is applied in the production of virgin polymers<br />
and also in recycling processes.<br />
Your benefits<br />
• Reduced investment costs compared to conventional PET processing<br />
• Lower production costs due to high energy savings; additional heating<br />
often required only upon production start-up<br />
• Spherical, almost dust-free and non-sticky pellets<br />
• High bulk density for downstream processing of the material<br />
• Can highly flexibly be adapted to changing process conditions<br />
• Crystallization temperature and dwell time are infinitely variable
<strong>COMBI</strong>-<strong>CRYSTAL</strong>-PET ® (<strong>CC</strong>-PET ® )<br />
PET direct crystallization – significant energy savings, enhanced process reliability<br />
Processes and machines and systems made by Automatik Plastics Machinery stand for cost-effectiveness, flexibility, and<br />
reliability worldwide. With over six decades of experience and an installed base of currently more than 8,000 pelletizing<br />
systems, the company helps its customers to achieve the maximum level of profitability.<br />
Range of applications<br />
<strong>CC</strong>-PET ® combines pelletizing, drying, and crystallization in a single process. Downstream treatment of the pellets, usually<br />
as solid state polymerisation (SSP), is greatly simplified because the semi-crystalline end product does not stick in subsequent<br />
post-processing operations. <strong>CC</strong>-PET ® can be applied to both virgin polymer production and recycling applications with<br />
production capacities ranging from 750 kg/h up to 15,000 kg/h. The output from one reactor may be optionally diverted to<br />
several pelletizing lines and then recombined to a single crystallizer.<br />
Functioning of the <strong>CC</strong>-PET ® system<br />
The PET melt is discharged from the reactor or<br />
the extruder by a melt pump 01.<br />
The material is then processed by a SPHERO ®<br />
02 underwater pelletizer 03.<br />
The hot process water rapidly transports the<br />
pellets to the dryer 04, where the water is separated<br />
from the plastic pellets.<br />
The crystallizer 05 processes the PET pellets<br />
utilizing the residual heat, as well as additional<br />
heating as required.<br />
After crystallizing, the pellets are suitable for<br />
any kind of post-processing 06.<br />
The process water is tempered, filtered and returned<br />
to the points of use in a closed duct 07.<br />
04<br />
04<br />
01<br />
01<br />
02 03<br />
07<br />
07<br />
05<br />
05<br />
06<br />
<strong>CC</strong>-PET ® integrates the crystallization of PET<br />
directly into the SPHERO ® underwater pelletizing<br />
system. The end product does not stick<br />
in subsequent downstream processing operations.<br />
This results in<br />
• Reduced energy consumption, lower<br />
investment costs, and in<br />
• Increased operating profitability for both<br />
the system operator and his customers.<br />
Furthermore, <strong>CC</strong>-PET ® provides for controlled<br />
nucleation, as well as the supply of additional<br />
heating as required, for a wide range of raw<br />
material types. This ensures constant crystallization<br />
conditions which are not sensitive to<br />
fluctuations in material properties, guaranteeing<br />
highly uniform product quality.<br />
Immediately after conventional processing, PET pellets are amorphous.<br />
Such amorphous pellets become sticky when heated to temperatures<br />
above 70 °C and thus are not suitable for subsequent processing such as:<br />
• Post-condensation in the SSP – the pellets must be processed for<br />
several hours at approx. 210 °C.<br />
• Drying prior to downstream processing – due to its distinctive<br />
hygroscopic properties, PET must be intensively dried with hot air at<br />
160-180 °C for up to 6 hours.<br />
Therefore, the PET pellets must first be crystallized, since only this form<br />
is not sticky. For crystallizing, the pellets must be heated for a limited<br />
period of time to a temperature of approx. 130-180 °C. In order to<br />
avoid agglutination during the crystallizing operation, the pellets must<br />
be kept moving, e.g. by vibration, stirring, or fluidizing. The crystallization<br />
process is exothermic, and this reaction heat in combination with<br />
the residual heat can often meet the entire energy need for process<br />
heating. <strong>CC</strong>-PET ® helps to retain as much internal heat from upstream<br />
processing steps in the pellets as possible, thus reducing energy costs.
<strong>COMBI</strong>-<strong>CRYSTAL</strong>-PET ® (<strong>CC</strong>-PET ® )<br />
<strong>CC</strong>-PET ® system components<br />
In order to implement the <strong>CC</strong>-PET ® process, the following system<br />
components are combined in various configurations immediately<br />
following the melt generation unit:<br />
Pelletizing<br />
The pelletizing operation is performed with SPHERO ® for large-scale<br />
production of virgin PET or for recycling applications.<br />
SPHERO ® underwater pelletizer for virgin polymers and recycling<br />
applications<br />
• Suspension system provides optimal access to all pelletizer components<br />
• Die geometry tailored to material properties and desired pellet weight<br />
• Electric or liquid heating<br />
• Excellent cooling and pellet flow due to optimized cutting chamber<br />
design<br />
Featuring<br />
• Gentle melt handling<br />
• Rheologically optimized product channels<br />
• Electric, liquid, or steam heating<br />
• Energy-optimized process chain<br />
Melt handling<br />
• Melt pump<br />
• Polymer filter<br />
• Start-up valve for SPHERO ® systems<br />
CENTRO pellet dryer – for all USG and SPHERO ® systems<br />
• Energy-optimized pellet drying<br />
• Re-feeding of the separated water to the process loop<br />
• Direct transfer of pellets to the crystallizer<br />
<strong>CC</strong>-PET ® direct crystallization for all pelletizing options<br />
• Vibrating conveyor for simple recycling applications<br />
• ΔQ crystallizer for more sophisticated PET types and for highest<br />
throughput rates in automatic operation<br />
• Fluid bed crystallizer available for specialized applications<br />
<strong>CC</strong>-PET ® ΔQ crystallizer<br />
Options for post-processing of pellets<br />
• Classifier<br />
• Spiral cooling conveyor<br />
• SSP<br />
• Dealdehydization<br />
CENTRO pellet dryer<br />
<strong>CC</strong>-PET ® system controls<br />
• From simple machine controls to complex process visualization options<br />
• Function of individual components (e.g. melt pump, polymer filter,<br />
water circuit) can be integrated into the pelletizer controls<br />
• Data exchange with higher-level control systems possible<br />
Process water treatment<br />
Continuous filtration of return water with manual or automatic filters<br />
and automatic compensation for water loss within the system.<br />
<strong>CC</strong>-PET ® vibrating conveyor
<strong>COMBI</strong>-<strong>CRYSTAL</strong>-PET ® (<strong>CC</strong>-PET ® )<br />
Technical data<br />
PET product properties for the <strong>CC</strong>-PET ® process:<br />
IV: 0.50-0.90 dl/g<br />
DEG < 1.5 %w<br />
Co-monomers:<br />
IPA < 2.5 %w<br />
Others 0 %w<br />
Melt temperature T s<br />
:<br />
T S<br />
= TMP + 30 K (TMP = melting point)<br />
Pellet weight:<br />
15-18 mg<br />
Pellet temperature: After crystallizator: 150 °C-170 °C<br />
Global contacts, see www.maag.com<br />
Contact us at contact@maag.com<br />
A_50_2012/3<br />
The data and illustrations refer to the date of printing. Necessary changes can be made at any time without special notice. Maag Group´s products and processes are protected by IP rights.