Thesis-PDF - IAP/TU Wien
Thesis-PDF - IAP/TU Wien
Thesis-PDF - IAP/TU Wien
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1 µN) between a probe and the sample surface. Soon it became evident that<br />
it was also a convenient tool for obtaining topological information of a surface<br />
by rastering across it. In the recent years probe–sample interactions were also<br />
increasingly used for quantitative analysis of mechanical, electronic, magnetic,<br />
biological, and chemical sample properties. The AFM can map this information<br />
with atomic resolution to the sample surface and in contrast to STM is not limited<br />
to conductive samples. ([34], [8])<br />
3.2 Principles of AFM<br />
The Atomic Force Microscope (AFM) measures the forces between a probe, the<br />
AFM cantilever tip, and the surface. In order to obtain a 3D image [z(x, y)]<br />
of the surface, multiple scans [z(x)] displaced laterally from each other in the y<br />
direction are acquired. The cantilever is rastered across the surface by means of<br />
piezoelectric drives. This can be done either by dragging the tip over the surface<br />
or by oscillating it just above the surface.<br />
Figure 3.1: Generalized scheme of an Atomic Force Microscope (AFM)<br />
with optical beam sensing. Image adapted from [35].<br />
The movement of the cantilever probe can be sensed by either tunneling,<br />
capacitive, or optical detectors. Optical beam deflection methods are often preferred<br />
because of their sensitivity, reliability and ease of implementation ([36],<br />
[37]). Advantages are a large working distance, insensitivity to distance changes<br />
and capability to measure angular changes (i.e. related to friction forces) when<br />
using a four-quadrant optical detector. A laser beam is deflected from the top side<br />
of the cantilever onto a position-sensitive photodetector (see Fig. 3.1). Because<br />
of the relatively large laser travel distance (in the cm range or more) the slightest<br />
skewness or bending of the cantilever or change of resonance frequency while<br />
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