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Thesis-PDF - IAP/TU Wien

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1 µN) between a probe and the sample surface. Soon it became evident that<br />

it was also a convenient tool for obtaining topological information of a surface<br />

by rastering across it. In the recent years probe–sample interactions were also<br />

increasingly used for quantitative analysis of mechanical, electronic, magnetic,<br />

biological, and chemical sample properties. The AFM can map this information<br />

with atomic resolution to the sample surface and in contrast to STM is not limited<br />

to conductive samples. ([34], [8])<br />

3.2 Principles of AFM<br />

The Atomic Force Microscope (AFM) measures the forces between a probe, the<br />

AFM cantilever tip, and the surface. In order to obtain a 3D image [z(x, y)]<br />

of the surface, multiple scans [z(x)] displaced laterally from each other in the y<br />

direction are acquired. The cantilever is rastered across the surface by means of<br />

piezoelectric drives. This can be done either by dragging the tip over the surface<br />

or by oscillating it just above the surface.<br />

Figure 3.1: Generalized scheme of an Atomic Force Microscope (AFM)<br />

with optical beam sensing. Image adapted from [35].<br />

The movement of the cantilever probe can be sensed by either tunneling,<br />

capacitive, or optical detectors. Optical beam deflection methods are often preferred<br />

because of their sensitivity, reliability and ease of implementation ([36],<br />

[37]). Advantages are a large working distance, insensitivity to distance changes<br />

and capability to measure angular changes (i.e. related to friction forces) when<br />

using a four-quadrant optical detector. A laser beam is deflected from the top side<br />

of the cantilever onto a position-sensitive photodetector (see Fig. 3.1). Because<br />

of the relatively large laser travel distance (in the cm range or more) the slightest<br />

skewness or bending of the cantilever or change of resonance frequency while<br />

25

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