A N T I M O N Y : ITS HISTORY, CHEMISTRY, MINERALOGY ...
A N T I M O N Y : ITS HISTORY, CHEMISTRY, MINERALOGY ...
A N T I M O N Y : ITS HISTORY, CHEMISTRY, MINERALOGY ...
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THE METALLURGY OF ANTIMONY. 117<br />
by the workmen. The flues generally require cleaning four times<br />
a year.<br />
In the process described above, the first operation of smelting the<br />
ore with iron is called "singling," the second operation, or resmelting<br />
the singles for the production of the bowl metal, is called "doubling,"<br />
and the last operation is called "refining" or "frenching."<br />
On an average, one man can smelt 10 to 11 cwts. of ore in twelve<br />
hours. It has been observed that a small quantity of the oxide<br />
mixed with the sulphide improves the appearance of the metal.<br />
The following table shows the number of men required to work a<br />
furnace:—<br />
Firemen . . . ' .<br />
Furnacemen . . . .<br />
Refiners<br />
Metal-breakers . . . .<br />
Charge-mixer . . . .<br />
Workers on day-shift only, viz. \<br />
one smith, one boiler and engine- >man,<br />
and three labourers J<br />
Per Side of<br />
the Furnace<br />
per Shift,<br />
12 Hours.<br />
1<br />
4<br />
For the Whole<br />
Furnace per<br />
Shift,<br />
12 Hours.<br />
2<br />
2 1<br />
Total<br />
Per<br />
Day of<br />
24<br />
Hours.<br />
At Magurka, in Hungary, the precipitation method was formerly<br />
in use; pot furnaces and graphite crucibles were employed. The<br />
charges consisted of 20 to 22 lbs. of antimony sulphide, with iron,<br />
potash, and pan scale (from salt-works). There were only two<br />
operations in the process.<br />
At Linz and Schleiz in Germany, and at Alais in France, reverberatory<br />
furnaces are still in use. There is a great loss due to volatilisation<br />
in these furnaces; and hence condensing flues are connected with<br />
the furnaces for the collecting of the metallic fume. The bed must<br />
also be tight enough to prevent any loss due to leakage.<br />
According to M. Herrenschmidt, it is better to cover the bed of<br />
the reverberatory furnace with a thin layer of regulus in order to<br />
prevent the corrosion of the scoria.<br />
3. Direct Processes, i.e. Extraction of Metallic Antimony direct<br />
from the Ore.—(a) Bath Furnaces.—T. C. Sanderson has patented * a<br />
process for the smelting of antimony sulphide in a bath of ferrous<br />
* United States patent No. 714,040, Nov. 18, 1902.<br />
4<br />
16 442<br />
5<br />
35