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A N T I M O N Y : ITS HISTORY, CHEMISTRY, MINERALOGY ...

A N T I M O N Y : ITS HISTORY, CHEMISTRY, MINERALOGY ...

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THE METALLURGY OF AXT1M0XY.<br />

The prodticts of roasting (Sb2O3) are:—<br />

1st condensing chamber .<br />

2nd<br />

3rd<br />

4th<br />

5th<br />

6t-h<br />

7th<br />

8th<br />

9th<br />

5 J3<br />

> ><br />

><br />

76 kgs.<br />

. . . 65 „<br />

65 „<br />

48 „<br />

49 ,.<br />

44 ,,<br />

34 „<br />

• • • 24 „<br />

. . 19 ,,<br />

Total = 424 kgs.<br />

101<br />

It should he noted that the cleaning of the chambers and pipes for<br />

the removal of all the oxide was carried out in the next experiment.<br />

(b) Second Experiment—The first charge in the second experiment<br />

commenced at 11.5 a.m. on the 25th of April, and the last charge<br />

stopped at 10.30 p.m. of the same day, thus giving a total of 11<br />

hours 25 minutes working time. Each charge consisted of 50 kgs.<br />

of ore mixed with 4 per cent, of charcoal. The total charges<br />

amounted to 2725 kgs. of ore.<br />

The products of roasting (Sbo03) are :—<br />

1st condensing chamber .<br />

2nd<br />

3rd<br />

,.<br />

4th ,<br />

5th<br />

6th ,<br />

7th ,<br />

8th<br />

9th ,<br />

. 176 kgs.<br />

103 .,<br />

96 ,,<br />

61 ,<br />

45 „<br />

38 ,<br />

32 ,.<br />

28 „<br />

23 „<br />

Total = 602 kes.<br />

These numbers represent the actual amount of oxide extracted<br />

from the ore, plus the cleanings of oxide, due in part to the first<br />

experiment<br />

Further cleaning of the pipes and chambers gave 32 kgs. The<br />

condensing tanks, n, in fig. 4 of fig. 45, gave 1V8 kgs. of dried oxide.<br />

Now, if all had been thoroughly cleaned up—the pipes, the condensing<br />

chambers of the coke-tower, and the precipitating tanks—there would<br />

have resulted at least 5 kgs. of oxide more.<br />

(c) Conclusion.—The ore treated contained 19*5 per cent, of<br />

antimony.<br />

The oxide found in the first chamber contained 23 per cent, of<br />

impurities.

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