GC Chromatograms
GC Chromatograms
GC Chromatograms
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<strong>GC</strong> CHROMATOGRAMS | CLINICAL<br />
Basic Drugs, Benzodiazepines<br />
Underivatized Mixed Basic Drugs on Rtx®-35<br />
Peaks<br />
1. Nicotine<br />
2. Benzocaine<br />
3. Cotinine<br />
4. Meperidine<br />
5. Caffeine<br />
6. Benzphetamine<br />
7. Ketamine<br />
8. Diphenhydramine<br />
9. Lidocaine<br />
10. Phenyltoloxamine<br />
11. Tripelennamine<br />
12. Phenothiazine<br />
13. Dextromethorphan<br />
14. Methadone<br />
15. Amitriptyline<br />
16. Trimipramine<br />
17. Tetracaine<br />
18. Pyrilamine<br />
19. Medazepam<br />
20. Bupivacaine<br />
21. Scopolamine<br />
22. Codeine<br />
23. Morphine<br />
24. Diazepam<br />
25. Chlorpromazine<br />
26. Temazepam<br />
27. Flunitrazepam<br />
28. Bromazepam<br />
29. Prazepam<br />
30. Acetopromazine<br />
31. Flurazepam<br />
32. Papaverine<br />
33. Clonazepam<br />
34. Haloperidol<br />
35. Alprazolam<br />
36. Triazolam<br />
37. Thioridazine<br />
38. Trazodone<br />
Column Rtx®-35, 30 m, 0.25 mm ID, 0.25 μm (cat.# 10423)<br />
Sample<br />
Basic drug sample<br />
Conc.:<br />
1,000 ng/μL<br />
Injection<br />
Inj. Vol.: 1.0 μL split (split ratio 50:1)<br />
Inj. Temp.: 250 °C<br />
Oven<br />
Oven Temp: 100 °C to 325 °C at 4 °C/min (hold 10 min)<br />
Carrier Gas He, constant pressure<br />
Linear Velocity: 30 cm/sec @ 100 °C<br />
Detector FID @ 320 °C<br />
Notes<br />
FID sensitivity: 1.28 x 10 -10 AFS<br />
<strong>GC</strong>_PH00236<br />
Benzodiazepines (Underivatized) on Rtx®-200<br />
Peaks<br />
1. Medazepam<br />
2. Lorazepam<br />
3. Diazepam<br />
4. Desmethyldiazepam<br />
5. Bromazepam<br />
6. Prazepam<br />
7. Temazepam<br />
8. Flurazepam<br />
9. Clobazam<br />
10. Flunitrazepam<br />
11. Clonazepam<br />
12. Alprazolam<br />
13. Triazolam<br />
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Column Rtx®-200, 15 m, 0.32 mm ID, 0.25 μm (cat.# 15021)<br />
Sample<br />
Benzodiazepines<br />
Conc.:<br />
15 ng each component<br />
Injection<br />
Inj. Vol.: 1.0 μL split (split ratio 60:1)<br />
Inj. Temp.: 250 °C<br />
Oven<br />
Oven Temp: 225 °C to 325 °C at 8 °C/min<br />
Carrier Gas He, constant pressure<br />
Linear Velocity: 35 cm/sec @ 225 °C<br />
Detector FID @ 320 °C<br />
Notes<br />
FID sensitivity: 5.12 x 10 -10 AFS<br />
576 www.restek.com<br />
<strong>GC</strong>_PH00268
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