GC Chromatograms

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GC CHROMATOGRAMS | CLINICAL Amphetamines, Barbiturates Derivatized Amphetamines (500 ng/mL) on Rxi®-5Sil MS 1 6.0 C 2 Rxi® Technology! Exceptionally inert, ultra low-bleed capillary columns. Excellent peak shape with short run time. 3 4 7.0 8.0 9.0 10.0 Time (min) 5 GC_CF1144 Peaks 1. Amphetamine 2. Methamphetamine 3. MDA 4. MDMA 5. MDEA c = contaminant Column Rxi®-5Sil MS, 30 m, 0.25 mm ID, 0.25 μm (cat.# 13623) Sample Diluent: Butyl chloride Conc.: 500 ng/mL HFAA derivatives Injection Inj. Vol.: 1 μL splitless (hold 1 min) Liner: 3.5 mm splitless taper w/wool (cat.# 22286-200.1) Inj. Temp.: 250 °C Purge Flow: 28 mL/min Oven Oven Temp: 75 °C to 300 °C at 15 °C/min Carrier Gas He, constant linear velocity Linear Velocity: 45 cm/sec, 13.5 psi, 93.1 kPa @ 75 °C Detector MS Mode: Scan Transfer Line Temp.: 250 °C Analyzer Type: Quadrupole Source Temp.: 200 °C Electron Energy: 70 eV Solvent Delay Time: 4 min Tune Type: PFTBA Ionization Mode: EI Scan Range: 40-300 amu Scan Rate: 5 scans/sec Instrument Shimadzu 2010 GC & QP2010+ MS Underivatized Barbiturates (Acidic/Neutral Drugs) on Rtx®-35 Separation optimized using Pro ezGC! Peaks 1. Barbital 2. Aprobarbital 3. Butalbital 4. Amobarbital 5. Talbutal 6. Pentobarbital 7. Methohexital 8. Secobarbital 9. Thiopental 10. Hexobarbital 11. Mephobarbital 12. Phenobarbital Column Rtx®-35, 30 m, 0.32 mm ID, 0.50 μm (cat.# 10439) Sample Barbiturates Injection Inj. Vol.: 1.0 μL split (split ratio 30:1) Inj. Temp.: 300 °C Oven Oven Temp: 210 °C (hold 2 min) to 300 °C at 7 °C/min (hold 2 min) Carrier Gas He, constant pressure Linear Velocity: 35 cm/sec @ 210 °C Detector FID @ 300 °C Notes FID sensitivity: 5.12 x 10 -10 AFS GC_PH00267 www.restek.com 573
GC CHROMATOGRAMS | CLINICAL Barbiturates Underivatized Barbiturates (Acidic/Neutral Drugs) on Rtx®-35 Peaks 1. Ethosuximide 2. Barbital 3. Methyprylon 4. Aprobarbital 5. Butalbital 6. Amobarbital 7. Pentobarbital 8. Secobarbital 9. Meprobamate 10. Carisoprodal 11. Glutethimide 12. Phenobarbital 13. Methaqualone 14. Primidone 15. Carbamazepine 16. Diphenylhydantoin Column Rtx®-35, 30 m, 0.53 mm ID, 1.00 μm (cat.# 10455) Sample Acidic/neutral drugs Conc.: 50 μg/mL Injection Inj. Vol.: 1.0 μL splitless (hold 0.5 min) Inj. Temp.: 250 °C Oven Oven Temp: 100 °C to 280 °C at 10 °C/min (hold 5 min) Carrier Gas He, constant pressure Linear Velocity: 40 cm/sec @ 100 °C Detector FID @ 250 °C Notes FID sensitivity: 5.12 x 10 -10 AFS GC_PH00262 Underivatized Barbiturates (Acidic/Neutral Drugs) on Rtx®-1701 Peaks 1. Ethosuximide 2. Barbital 3. Methyprylon 4. Aprobarbital 5. Butalbital 6. Amobarbital 7. Pentobarbital 8. Secobarbital 9. Meprobamate 10. Carisoprodal 11. Glutethimide 12. Phenobarbital 13. Methaqualone 14. Primidone 15. Carbamazepine 16. Diphenylhydantoin Column Rtx®-1701, 15 m, 0.53 mm ID, 0.50 μm (cat.# 12037) Sample Acidic/neutral drugs Conc.: 50 μg/mL Injection Inj. Vol.: 1.0 μL splitless (hold 0.5 min) Inj. Temp.: 250 °C Oven Oven Temp: 100 °C to 280 °C at 7 °C/min Carrier Gas He, constant pressure Linear Velocity: 40 cm/sec @ 100 °C Detector FID @ 275 °C Notes FID sensitivity: 5.12 x 10 -10 AFS GC_PH00263 574 www.restek.com
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GC CHROMATOGRAMS | FOOD SAFETY Food
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GC CHROMATOGRAMS | FOOD SAFETY Pack
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GC CHROMATOGRAMS | FOOD SAFETY PAHs
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Dietary Supplement (Finished Produc
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GC CHROMATOGRAMS | FOODS, FLAVORS,
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GC CHROMATOGRAMS | FORENSICS Arson
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GC CHROMATOGRAMS | FORENSICS GHB/GB
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GC CHROMATOGRAMS | FORENSICS Inhala
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GC CHROMATOGRAMS | PETROLEUM & PETR
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Ethylene and C1-C5 Hydrocarbons by
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Detailed Hydrocarbon Analysis on Rt
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GC CHROMATOGRAMS | PHARMACEUTICAL O
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Reduce method development time—us
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GC CHROMATOGRAMS | SOLVENTS & CHEMI
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GC Chromatograms

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