GC Chromatograms

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GC CHROMATOGRAMS | ENVIRONMENTAL Dioxins/Furans Dioxins (PnCDDs) in Fly Ash on Rxi®-5Sil MS NEW! PnCDDs in Fly Ash Column Rxi®-5Sil MS, 60 m, 0.18 mm ID, 0.10 μm (cat.# 43607) Sample Fly ash extract Diluent: Nonane Injection Inj. Vol.: 1 μL splitless Liner: 2 mm splitless liner (cat.# 20712) Oven Oven Temp: 120 °C (hold 1 min) to 160 °C at 10 °C/min to 300 °C at 2.5 °C/min Carrier Gas He, constant flow Flow Rate: 1 mL/min Detector Waters AutoSpec Ultima Mass Spectrometer Source Temp.: 280 °C Ionization Mode: EI Notes Electron Ionization at 40eV Red indicates toxicity Acknowledgement Chromatogram courtesy of Karen MacPherson, Li Shen, Terry Kolic, and Eric Reiner at the Ontario Ministry of the Environment GC_EV1197 Dioxins (HxCDFs) in Fly Ash on Rxi®-5Sil MS NEW! Column Rxi®-5Sil MS, 60 m, 0.18 mm ID, 0.10 μm (cat.# 43607) Sample Fly ash extract Diluent: Nonane Injection Inj. Vol.: 1 μL splitless Liner: 2 mm splitless liner (cat.# 20712) Oven Oven Temp: 120 °C (hold 1 min) to 160 °C at 10 °C/min to 300 °C at 2.5 °C/min Carrier Gas He, constant flow Flow Rate: 1 mL/min Detector Waters AutoSpec Ultima Mass Spectrometer Source Temp.: 280 °C Ionization Mode: EI Notes Electron Ionization at 40eV Red indicates toxicity Acknowledgement Chromatogram courtesy of Karen MacPherson, Li Shen, Terry Kolic, and Eric Reiner at the Ontario Ministry of the Environment HxCDFs in Fly Ash GC_EV1199 www.restek.com 589
GC CHROMATOGRAMS | ENVIRONMENTAL Explosives Explosives on Rtx®-200 Peaks 1. 2-Nitrotoluene 2. 3-Nitrotoluene 3. 4-Nitrotoluene 4. 2,3-Diaminotoluene 5. 2,6-Diaminotoluene 6. 2,4-Diaminotoluene 7. 1,4-Dinitrobenzene 8. 2,6-Dinitrotoluene 9. 2-Amino-6-nitrotoluene 10. 1,3-Dinitrobenzene 11. 2,4-Dinitrotoluene 12. 2-Amino-4-nitrotoluene 13. 2,3-Dinitrotoluene 14. 3,4-Dinitrotoluene 15. 3-Nitrobiphenyl 16. 2,4,6-Trinitrotoluene 17. 2,4,5-Trinitrotoluene 18. 4-Amino-2,6-dinitrotoluene 19. 2,3,4-Trinitrotoluene 20. 1,3-Dinitronaphthalene 21. 2,6-Diamino-4-nitrotoluene 22. 2-Amino-4,6-dinitrotoluene 23. 2,2'-Dinitrobiphenyl Column Rtx®-200, 30 m, 0.25 mm ID, 0.25 μm (cat.# 15023) Sample Explosives sample Conc.: 20 ng/μL Injection Inj. Vol.: 1 μL splitless (hold 0.6 min) Inj. Temp.: 280 °C Oven Oven Temp: 80 °C (hold 2 min) to 260 °C at 3 °C/min (hold 2 min) Carrier Gas He, constant pressure Linear Velocity: 20 cm/sec @ 80 °C Detector MS Mode: Scan Transfer Line Temp.: 300 °C Analyzer Type: Quadrupole Ionization Mode: EI GC_EV00060 Now Online! Our EZGC Web App Will Kick-Start Your GC Method Development • EZ to Register – If you have a Restek login, you’re already done! (And if you don’t, you can get one at no charge and with no hassle.) • EZ to Get Started – A quick, 5-minute video will show you everything you need to know. • EZ to Use – Just enter your target compounds, and in seconds, the EZGC system gives you a customized method, including column, conditions, and model chromatogram. • EZ to Analyze – Model chromatograms are fully interactive. Zoom in, view chemical structures, and even overlay mass spectra. • EZ to Save – Print your chromatogram and custom settings, or save them for future reference. Start developing incredible GC methods today! www.restek.com/ezgc 590 www.restek.com
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GC CHROMATOGRAMS | FOODS, FLAVORS,
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GC CHROMATOGRAMS | FORENSICS Arson
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GC CHROMATOGRAMS | FORENSICS GHB/GB
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GC CHROMATOGRAMS | FORENSICS Inhala
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GC CHROMATOGRAMS | PETROLEUM & PETR
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Ethylene and C1-C5 Hydrocarbons by
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Detailed Hydrocarbon Analysis on Rt
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GC CHROMATOGRAMS | PHARMACEUTICAL O
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Reduce method development time—us
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GC CHROMATOGRAMS | SOLVENTS & CHEMI
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GC Chromatograms

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