GC Chromatograms

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GC CHROMATOGRAMS | ENVIRONMENTAL Air Mass APH on Rxi®-1ms Rxi® Technology! Exceptionally inert, ultra low-bleed capillary columns. 1 2 3 4 5 7 6 8 9 10 11 13 14 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 Time (min) GC_AR1145 12 15 16 17 18 20 19 21 22 23 24 25 26 27 28 Peaks 1. 1,3-Butadiene 2. iso-Pentane 3. Methyl tert-butyl ether 4. Bromochloromethane 5. n-Hexane 6. Benzene 7. Cyclohexane 8. 1,4-Difluorobenzene 9. 2,3-Dimethylpentane 10. n-Heptane 11. Toluene 12. n-Octane 13. Chlorobenzene-d5 14. Ethylbenzene 15. 2,3-Dimethylheptane 16. m-Xylene/p-Xylene 17. o-Xylene 18. n-Nonane 19. 4-Bromofluorobenzene 20. Isopropylbenzene 21. 1-Ethyl-3-methylbenzene 22. 1,3,5-Trimethylbenzene 23. n-Decane 24. 1,2,3-Trimethylbenzene/p-Isopropyltoluene 25. Butylcyclohexane 26. n-Undecane 27. Naphthalene 28. n-Dodecane NEW! Column Rxi®-1ms, 60 m, 0.32 mm ID, 1.00 μm (cat.# 13357) Injection Splitless Oven Oven Temp: 35 °C (hold 5 min) to 220 °C at 7 °C/min (hold 2 min) Carrier Gas He, constant flow Flow Rate: 1.2 mL/min Detector MS Mode: Scan Transfer Line Temp.: 240 °C Analyzer Type: Quadrupole Source Temp.: 230 °C Quad Temp.: 150 °C Solvent Delay Time: 4.0 min Ionization Mode: EI Scan Range: 35-250 amu Preconcentrator Entech 7100 Instrument HP6890 GC & 5973 MSD Acknowledgement Courtesy of Mass DEP, Northeast Region How can we help you today? Contact us... customer service: 1-814-353-1300, ext. 3 | e-mail: csreps@restek.com technical service: 1-814-353-1300, ext. 4 | e-mail: support@restek.com sales representatives: 1-814-353-1300, ext. 3 | e-mail: salesreps@restek.com 4 ways to order: 1. CALL: 1-800-356-1688, ext. 3 or 1-814-353-1300, ext. 3 Monday–Friday 8:00 a.m.–6:30 p.m. Eastern Time 2. FAX: 1-814-353-1309 24 hours a day 3. ONLINE: www.restek.com 24 hours a day 4. E-MAIL: csreps@restek.com 24 hours a day Outside the U.S.? Find a distributor at www.restek.com/distributor www.restek.com 585
GC CHROMATOGRAMS | ENVIRONMENTAL Brominated Flame Retardants Brominated Flame Retardants on Rtx®-1614 Get results 3 times faster with a short column method! Peaks 1. BDE-10 2. BDE-7 3. BDE-8 4. BDE-11 5. BDE-12 6. BDE-13 7. BDE-15 8. BDE-30 9. BDE-32 10. BDE-17 11. BDE-25 12. BDE-28 13. BDE-33 14. BDE-35 15. BDE-37 16. BDE-75 17. BDE-49 18. BDE-71 19. BDE-47 20. BDE-66 21. BDE-77 22. BDE-100 23. BDE-119 24. BDE-99 25. BDE-116 26. BDE-118 27. BDE-85 28. BDE-155 29. BDE-126 30. BDE-154 31. BDE-153 32. BDE-138 33. BDE-166 34. BDE-183 35. BDE-181 36. BDE-190 37. BDE-208 38. BDE-207 39. BDE-206 40. BDE-209 Column Rtx®-1614, 15 m, 0.25 mm ID, 0.10 μm (cat.# 10296) Sample 100 - 300 ppb PBDE PAR solution (#EO-5113, Cambridge Isotope Laboratories Inc.) 500 ppb decabromodiphenyl ether (#BDE-209, Wellington Laboratories) Injection Inj. Vol.: 1 μL splitless (hold 1 min) Liner: 4 mm cyclo double taper (cat.# 20896) Inj. Temp.: 340 °C Oven Oven Temp: 120 °C (hold 1 min) to 275 °C at 15 °C/min to 300 °C at 5 °C/min (hold 5 min) Carrier Gas He, constant linear velocity Linear Velocity: 60 cm/sec @ 120 °C Detector μ-ECD @ 345 °C Great peak shape for BDE 209! also see: PCBs and Brominated Flame Retardants ➲ pages 603–604 GC_EV01025 Brominated Flame Retardants on Rtx®-1614 Column Rtx®-1614, 30 m, 0.25 mm ID, 0.10 μm (cat.# 10295) Sample 100 - 300 ppb PBDE PAR solution (cat.# EO-5113, Cambridge Isotope Laboratories Inc.) 500 ppb decabromodiphenyl ether (cat.# BDE-209, Wellington Laboratories) Injection Inj. Vol.: 1 μL splitless (hold 1 min) Liner: Cyclo double taper (4 mm) (cat.# 20896) Inj. Temp.: 300 °C Oven Oven Temp: 100 °C (hold 3 min) to 320 °C at 5 °C/min (hold 15 min) Carrier Gas He, constant linear velocity Linear Velocity: 20 cm/sec @ 100 °C Detector μ-ECD @ 340 °C Peaks 1. BDE-10 2. BDE-7 3. BDE-8 4. BDE-11 5. BDE-12 6. BDE-13 7. BDE-15 8. BDE-30 9. BDE-32 10. BDE-17 11. BDE-25 12. BDE-28 13. BDE-33 14. BDE-35 15. BDE-37 16. BDE-75 17. BDE-49 18. BDE-71 19. BDE-47 20. BDE-66 21. BDE-77 22. BDE-100 23. BDE-119 24. BDE-99 25. BDE-116 26. BDE-118 27. BDE-85 28. BDE-155 29. BDE-126 30. BDE-154 31. BDE-153 32. BDE-138 33. BDE-166 34. BDE-183 35. BDE-181 36. BDE-190 37. BDE-208 38. BDE-207 39. BDE-206 40. BDE-209 GC_EV01019 586 www.restek.com
Page 2 and 3: Chromatograms GC Chromatograms GC C
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Page 6 and 7: GC CHROMATOGRAMS | CLINICAL Ampheta
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GC CHROMATOGRAMS | FORENSICS Arson
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GC CHROMATOGRAMS | FORENSICS GHB/GB
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GC CHROMATOGRAMS | FORENSICS Inhala
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GC CHROMATOGRAMS | PETROLEUM & PETR
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Ethylene and C1-C5 Hydrocarbons by
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Detailed Hydrocarbon Analysis on Rt
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GC CHROMATOGRAMS | PHARMACEUTICAL O
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Reduce method development time—us
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GC CHROMATOGRAMS | SOLVENTS & CHEMI
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