GC Chromatograms
GC Chromatograms
GC Chromatograms
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<strong>GC</strong> CHROMATOGRAMS | CLINICAL<br />
Sympathomimetic Amines<br />
Underivatized Sympathomimetic Amines (Basic Drugs) on Rtx®-5 Amine<br />
Peaks<br />
1. Phenylethylamine<br />
2. Amphetamine<br />
3. Phentermine<br />
4. Methamphetamine<br />
5. Fenfluramine<br />
6. Mephentermine<br />
7. Cathinone<br />
8. Phenylpropanolamine<br />
9. Methcathinone<br />
10. Nicotine<br />
11. Ephedrine<br />
2<br />
4<br />
3<br />
5<br />
6<br />
10<br />
12. Pseudoephedrine<br />
13. Phenmetrazine<br />
14. Phendimetrazine<br />
15. Methylenedioxyamphetamine<br />
16. Diethylpropion<br />
17. Methylenedioxymethamphetamine<br />
18. Methylenedioxyethylamphetamine<br />
19. 4-Methyl-2,5-dimethoxyamphetamine<br />
20. Phenylephrine<br />
21. Caffeine<br />
22. Benzphetamine<br />
13<br />
16<br />
14<br />
17<br />
18<br />
19<br />
21<br />
22<br />
Column<br />
Rtx®-5 Amine, 30 m, 0.25 mm ID, 0.50 μm<br />
(cat.# 12338)<br />
Injection<br />
Inj. Vol.:<br />
1 μL split<br />
Inj. Temp.: 250 °C<br />
Split Vent<br />
Flow Rate: 45 mL/min<br />
Oven<br />
Oven Temp: 100 °C to 310 °C at 10 °C/min<br />
Carrier Gas He<br />
Detector<br />
MS<br />
Mode:<br />
Scan<br />
Scan Range: 40-600 amu<br />
Instrument Varian 3400 coupled with with Varian<br />
Saturn 2000 MS detector<br />
1<br />
7 8 9<br />
11,12<br />
15<br />
Ionization performed in the EI Auto mode.<br />
5 7.5 10 12.5 15 17.5 20 Time (min)<br />
<strong>GC</strong>_PH00438<br />
Sympathomimetic Amines (Basic Drugs) (HFBA Derivatives) on Rtx®-200<br />
Peaks<br />
1. Phenylethylamine - HFBA<br />
2. Amphetamine - HFBA<br />
3. Phentermine - HFBA<br />
4. Methamphetamine - HFBA<br />
5. Fenfluramine - HFBA<br />
6. Mephentermine - HFBA<br />
7. Cathinone - HFBA<br />
8. Phenylpropanolamine - HFBA<br />
9. Methcathinone - HFBA<br />
10. Nicotine - HFBA<br />
11. Ephedrine - HFBA<br />
12. Pseudoephedrine - HFBA<br />
13. Phenmetrazine - HFBA<br />
14. Phendimetrazine - HFBA<br />
15. Methylenedioxyamphetamine - HFBA<br />
16. Diethylpropion - HFBA<br />
17. Methylene dioxymethamphetamine - HFBA<br />
18. Methylene dioxyethylamphetamine - HFBA<br />
19. 4-Methyl-2,5-dimethoxyamphetamine - HFBA<br />
20. Phenylephrine - HFBA<br />
21. Caffeine - HFBA<br />
22. Benzphetamine - HFBA<br />
3<br />
1,2<br />
4<br />
8<br />
11<br />
7<br />
9<br />
12<br />
13<br />
22<br />
15,20<br />
19 17<br />
Column<br />
Rtx®-200, 30 m, 0.25 mm ID, 0.50 μm<br />
(cat.# 15038)<br />
Injection<br />
Inj. Vol.:<br />
1 μL split<br />
Inj. Temp.: 250 °C<br />
Split Vent<br />
Flow Rate: 45 mL/min<br />
Oven<br />
Oven Temp: 100 °C to 310 °C at 10 °C/min<br />
Carrier Gas He<br />
Detector<br />
MS<br />
Mode:<br />
Scan<br />
Ionization Mode: EI<br />
Scan Range: 40-600 amu<br />
Instrument Varian 3400 coupled with with Varian<br />
Saturn 2000 MS detector<br />
10<br />
14<br />
16<br />
21<br />
5<br />
18<br />
5 7.5 10 12.5 15 17.5 Time (min)<br />
<strong>GC</strong>_PH00439<br />
www.restek.com 581
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