GC Chromatograms
GC Chromatograms
GC Chromatograms
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<strong>GC</strong> CHROMATOGRAMS | CLINICAL<br />
Phenothiazines, Sympathomimetic Amines<br />
Underivatized Phenothiazines (Basic Drugs) on Rtx®-5<br />
Separation optimized<br />
using Pro ez<strong>GC</strong>!<br />
Peaks<br />
1. Phenothiazine<br />
2. Promethazine<br />
3. Trimeprazine<br />
4. Promazine<br />
5. Chlorprothixene<br />
6. Chlorpromazine<br />
7. Trifluoperazine<br />
8. Acetopromazine<br />
9. Prochlorperazine<br />
10. Thioridazine<br />
Looking for more?<br />
Visit our online technical library<br />
for chromatograms based on<br />
ASTM methods, USP procedures,<br />
and other applications.<br />
www.restek.com/chromatograms<br />
Column Rtx®-5, 15 m, 0.32 mm ID, 0.50 μm (cat.# 10236)<br />
Sample<br />
Conc.:<br />
2,000 ng/μL<br />
Injection<br />
Inj. Vol.: 1.0 μL split (split ratio 30:1)<br />
Inj. Temp.: 250 °C<br />
Oven<br />
Oven Temp: 200 °C to 325 °C at 5 °C/min<br />
Carrier Gas He, constant pressure<br />
Linear Velocity: 25 cm/sec @ 200 °C<br />
Detector FID @ 315 °C<br />
Notes<br />
FID sensitivity: 2.56 x 10 -10 AFS<br />
<strong>GC</strong>_PH00269<br />
Underivatized Sympathomimetic Amines (Basic Drugs) on Rtx®-35 Amine<br />
1<br />
2<br />
3<br />
5<br />
8<br />
10<br />
Peaks<br />
1. Amphetamine<br />
2. Methamphetamine<br />
3. N-Ethylamphetamine<br />
4. p-Methoxyamphetamine (PMA)<br />
5. p-Methoxymethamphetamine (PMMA)<br />
6. Methylenedioxyamphetamine (MDA)<br />
7. Methylenedioxymethamphetamine (MDMA)<br />
8. Methylenedioxyethylamphetamine (MDEA)<br />
9. HMMA<br />
10. MBDB<br />
4<br />
6 7<br />
9<br />
Column<br />
Rtx®-35 Amine, 30 m, 0.25 mm ID, 0.50 μm<br />
(cat.# 11338)<br />
Sample<br />
Underivatized sympathomimetic amines<br />
Conc.:<br />
1,000 ng/μL<br />
Injection<br />
Inj. Vol.:<br />
1.0 μL split<br />
Inj. Temp.: 250 °C<br />
Oven<br />
Oven Temp: 150 °C to 240 °C at 7 °C/min<br />
Carrier Gas He, constant flow<br />
Linear Velocity: 30 cm/sec<br />
Detector<br />
MS<br />
Mode:<br />
Scan<br />
Ionization Mode: EI<br />
Scan Range: 40-450 amu<br />
3.00<br />
4.00 5.00<br />
6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00<br />
Time (min)<br />
<strong>GC</strong>_PH00574<br />
580 www.restek.com
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