GC Chromatograms
GC Chromatograms
GC Chromatograms
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<strong>GC</strong> CHROMATOGRAMS | PETROLEUM & PETROCHEMICAL<br />
Hydrocarbons (High-Temperature)<br />
Diesel #2/Motor Oil on Rtx®-Mineral Oil<br />
NEW!<br />
Mineral Oil and Motor Oil on Rtx®-Mineral Oil<br />
NEW!<br />
<strong>GC</strong>_PC1169<br />
<strong>GC</strong>_PC1168<br />
Column Rtx®-Mineral Oil, 15 m, 0.32 mm ID, 0.15 μm (cat.# 18074)<br />
using IP deactivated guard column 2 m, 0.53 mm ID (cat.# 10047)<br />
Sample Diesel #2/motor oil (cat.# 31682)<br />
Diluent:<br />
Hexane<br />
Conc.:<br />
5,000 μg/mL diluted to 500 ppm<br />
Injection<br />
Inj. Vol.:<br />
0.5 μL cold on-column<br />
Temp. Program: 53 °C to 300 °C at 10 °C/min (hold 20 min)<br />
Oven<br />
Oven Temp: 50 °C to 300 °C at 10 °C/min (hold 20 min)<br />
Carrier Gas H2, constant flow<br />
Linear Velocity: 40 cm/sec @ 50 °C<br />
Dead Time: 0.625 min @ 50 °C<br />
Detector FID @ 330 °C<br />
Make-up Gas<br />
Flow Rate: 30 mL/min<br />
Make-up Gas Type: N2<br />
Data Rate:<br />
20 Hz<br />
Instrument<br />
Notes<br />
Agilent/HP6890 <strong>GC</strong><br />
Black trace = diesel/motor oil<br />
Red trace = C10-C40 standard<br />
Column Rtx®-Mineral Oil, 15 m, 0.32 mm ID, 0.15 μm (cat.# 18074)<br />
using IP deactivated guard column 2 m, 0.53 mm ID (cat.# 10047)<br />
Sample<br />
Custom mineral oil/motor oil mix<br />
Diluent:<br />
Hexane<br />
Conc.:<br />
500 μg/mL<br />
Injection<br />
Inj. Vol.:<br />
0.5 μL cold on-column<br />
Temp. Program: 53 °C to 300 °C at 10 °C/min (hold 20 min)<br />
Oven<br />
Oven Temp: 50 °C to 300 °C at 10 °C/min (hold 20 min)<br />
Carrier Gas<br />
H2, constant flow<br />
Linear Velocity: 40 cm/sec @ 50 °C<br />
Dead Time: 0.625 min @ 50 °C<br />
Detector FID @ 330 °C<br />
Make-up Gas<br />
Flow Rate: 30 mL/min<br />
Make-up Gas Type: N2<br />
Data Rate:<br />
20 Hz<br />
Instrument<br />
Agilent/HP6890 <strong>GC</strong><br />
Notes<br />
Black trace = mineral oil<br />
Green trace = motor oil<br />
Red trace = C10-C40 standard<br />
Diesel #2/Mineral Oil on Rtx®-Mineral Oil<br />
NEW!<br />
Looking for more?<br />
Visit our online technical library<br />
for chromatograms based on<br />
ASTM methods, USP procedures,<br />
and other applications.<br />
<strong>GC</strong>_PC1170<br />
Column Rtx®-Mineral Oil, 15 m, 0.32 mm ID, 0.15 μm (cat.# 18074)<br />
using IP deactivated guard column 2 m, 0.53 mm ID (cat.# 10047)<br />
Sample Diesel #2/mineral oil (cat.# 31676)<br />
Diluent:<br />
Hexane<br />
Conc.:<br />
500 μg/mL<br />
Injection<br />
Inj. Vol.:<br />
0.5 μL cold on-column<br />
Temp. Program: 53 °C to 300 °C at 10 °C/min (hold 20 min)<br />
Oven<br />
Oven Temp: 50 °C to 300 °C at 10 °C/min (hold 20 min)<br />
Carrier Gas H2, constant flow<br />
Linear Velocity: 40 cm/sec @ 50 °C<br />
Dead Time: 0.625 min @ 50 °C<br />
Detector FID @ 330 °C<br />
Make-up Gas<br />
Flow Rate: 30 mL/min<br />
Make-up Gas Type: N2<br />
Data Rate:<br />
20 Hz<br />
Instrument<br />
Notes<br />
Agilent/HP6890 <strong>GC</strong><br />
Black trace = diesel/mineral oil<br />
Red trace = C10-C40 standard<br />
www.restek.com/chromatograms<br />
672 www.restek.com 1-800-356-1688 or 1-814-353-1300
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