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Lynne Wong's PhD thesis

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In Mauritius, most of the sugar factories use lime saccharate, a mixture of milk of lime and<br />

sucrose syrup, as this liming agent has been found more efficient than milk of lime alone<br />

(Wong Sak Hoi and Chung, 1996). After liming, the juice is superheated to 103 – 105 °C<br />

and allowed to flash to the constant boiling point at atmospheric pressure. This forces out<br />

the air present in the juice and also causes bagacillo particles to burst and sink with the<br />

solids. The flashed limed juice is then sent to decant in a large vessel called a clarifier<br />

where the clear juice separates from the precipitated solids. Flocculation and settling are<br />

aided by the addition of synthetic water soluble flocculants, which are partially hydrolysed<br />

polyacrylamides. The clear juice is removed from the top and sent to evaporators while the<br />

muds are pumped from the bottom of the clarifier to a rotary vacuum filter. The filtered<br />

juice is sent back to process while the filter cake is returned to the fields as soil conditioner<br />

or fertilizer.<br />

The techniques used for clarification and filtration were comprehensively reviewed by<br />

Whayman (1992).<br />

1.2.5 Evaporation<br />

The clear juice from the clarifier contains about 85% water. Two-thirds of this water is<br />

evaporated in a vacuum multiple-effects evaporator consisting of a succession of vacuumboiling<br />

vessels (usually 4 – 5) arranged in series or in parallel so that each succeeding body<br />

has a higher vacuum, and therefore boils at a lower temperature. The vapours from one<br />

body can thus boil the juice in the next one. With this arrangement, the exhaust steam<br />

introduced into the first body of a quadruple-effect evaporator evaporates four times its<br />

mass of water. The vapour from the final body of the evaporator goes to a barometric<br />

condenser. The syrup leaving the evaporator contains about 65% refractometric solids<br />

(Brix) and 35% water.<br />

1.2.6 Crystallization<br />

Crystallization takes place in single-effect vacuum pans, where the syrup is further<br />

evaporated until saturated with sugar. "Seed grain" is then added to serve as nuclei for the<br />

formation of sugar crystals, and more syrup is added as the water evaporates. Crystal<br />

growth continues until the pan is full. For a skilled sugar boiler, the original crystals can<br />

be grown without the formation of additional crystals (false grain), so that when the pan is<br />

8

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