29.12.2013 Views

Lynne Wong's PhD thesis

Lynne Wong's PhD thesis

Lynne Wong's PhD thesis

SHOW MORE
SHOW LESS

Create successful ePaper yourself

Turn your PDF publications into a flip-book with our unique Google optimized e-Paper software.

Figure 3.19. Stalk cake washed<br />

free from Brix (top) and three<br />

fractions after wet-sieving.<br />

Figure 3.20. Rind sample before<br />

and after cutter-grinding.<br />

Figure 3.21. Rind cake washed<br />

free from Brix (top) and three<br />

fractions after wet-sieving.<br />

3.4.4 Characterisation of the sugar cane component parts<br />

3.4.4.1 Gross calorific value<br />

The gross calorific value (GCV) of the extracted fibres was measured with a Parr model<br />

1241 adiabatic oxygen bomb calorimeter (Fig 3.22).<br />

Samples of the four cane varieties R 579, R 570, M 1557/70 and M 1400/86 of the same<br />

age (about 52 weeks old) were obtained. After the nodes were rejected, rind was peeled<br />

off the stalk, and fibres were extracted from both rind and stalk. The combined rind fibre<br />

and fines, as well as stalk fibre, stalk pith and dry leaf were examined. Long fibres in rind,<br />

stalk and dry leaf were cut into fine particles with a pair of scissors, before drying at<br />

105 °C for three hours in a drying oven. Each sample, when required, was removed from<br />

the oven, pressed into a pellet and burnt in the adiabatic oxygen bomb calorimeter to<br />

determine its GCV.<br />

The calorific value of fibre (or bagasse) is determined by burning a weighed sample in an<br />

adiabatic bomb calorimeter under controlled conditions and is computed from the<br />

temperature observations made before and after the combustion, with allowances being<br />

made for the thermometer and thermochemical reactions. Benzoic acid pellets weighing<br />

between 0.9 and 1.25 g were used to calibrate the calorimeter.<br />

86

Hooray! Your file is uploaded and ready to be published.

Saved successfully!

Ooh no, something went wrong!