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Lynne Wong's PhD thesis

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ased on the manner in which the Brix-free water determination is performed on the<br />

sample (Mangion and Player, 1991). This is done by adding 150 mL of a 10° Brix sucrose<br />

solution to 8 g of dry sample (here the moist cake is assumed to contain 50% moisture and<br />

hence double this mass is used in the calculation), and measuring the increase of Brix in<br />

the resulting solution. The washing was repeated on the remainder of the sample until all<br />

was free from residual Brix.<br />

To separate pith from the fibre, the cakes from the Pinette Emidecau press were soaked in<br />

a bucket of water. A sieve assembly was mounted with a 2 mm, 1.18 mm and 38 μm sieve<br />

in order on top of each other. A handful of fibre and pith mixture was put onto the top<br />

sieve, and running tap water was used to wash the pith into the bottom sieve. Separation of<br />

pith from the fibre in the sample was thus effected. The separated fibre was hand pressed<br />

and placed in a metal tray for drying in an oven at 65 °C to constant mass. The separated<br />

pith was also dried in the same way.<br />

The dried fibre samples sometimes still contained some pith, and dry sieving by using a<br />

1.18 mm sieve mounted on top of a receiver was used to ensure complete separation.<br />

3.4.3.2 Rind, dry leaves and green leaves<br />

These samples were treated as for the cane stalk. Pre-treatment in a Jeffco cutter-grinder<br />

was necessary, the sample mass and the time of disintegration are indicated in Table 3.4.<br />

Table 3.4. Preparatory treatment process for fibre extraction<br />

from sugar cane plant components.<br />

Sample<br />

Cutter-grinder<br />

Mass used in<br />

the Jeffco wet<br />

disintegrator/g<br />

Disintegration<br />

time/s<br />

Top<br />

Stalk<br />

Rind<br />

Dry leaves<br />

Green leaves<br />

-<br />

<br />

<br />

<br />

<br />

400<br />

500<br />

300<br />

100<br />

300<br />

60<br />

30<br />

75<br />

60<br />

30<br />

3.4.3.3 Cane tops<br />

After the cane tops were detached from the stalks at the point where they naturally broke<br />

off the stalks, they were cut into 10 cm lengths and into thin strips lengthwise; in so doing,<br />

83

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