O FLIX

O 

FLIX

CHLOROMETHANE PLANT 

FLIX 

CONTENTS 

1.-PURPOSE 

2.- PROCESS DESCRIPTION 

3.- MECHANICAL EQUIPMENT INVENTORY 

4.- INSTRUMENTATION INVENTORY

1.- PURPOSE 

The Flix CHLOROMETHANE plant is designed for the production of 80 tonnes/day of 

methanol-derived halogenated solvents, specifically chloroform and methylene chloride. The 

raw materials used in this process are chlorine (105 /day) and methanol (25 t/day). Carbon 

tetrachloride (8-10 t/day) and 30% hydrochloric acid (80 t/day) are also produced as residual 

products. 

2.- PROCESS DESCRIPTION 

2.1 Hydrochlorination Section 

Hydrochlorination is the section in which methyl chloride is produced by the chlorination of 

methanol in gas phase. 

To explain how this stage works, it has been divided into three systems: 

1.- Reaction system

2.- CH 3 Cl purification system. 

3.- CH 3 Cl condensation system. 

2.1.1 Reaction System 

2.1.1.1 Methanol Hydrochlorination 

In the methanol hydrochlorination system, the reaction of methanol with hydrogen chloride in 

the presence of a catalyst to produce methyl chloride is represented by the following equation: 

CH 3 OH + HCl -------------> CH 3 Cl + H 2 O 

The catalyst used in hydrochlorination is gamma alumina. 

2.1.1.2 Methanol Supply System 

The methanol supply system consists of a methanol vaporiser (I-1101) and a methanol reheater 

(I-1102). 

The vaporised methanol is fed into the methanol re-heater, I-1102, where it is reheated to 180- 

205º C by the recirculation of thermal oil. 

2.1.1.3 Hydrogen Chloride Supply System 

The hydrogen chloride supply system consists of a hydrogen chloride re-heater (I-1103) and a 

hydrogen chloride absorption column (C-1106). 

The hydrogen chloride generated in the chlorination reactor, R-1201, is sent to the 

hydrochlorination stage, passing through the heat exchanger I-1109. One part of the hydrogen 

chloride passes through I-1103, where it is heated to 180-205º C, the same as the methanol, to 

prevent corrosion. 

The remaining hydrogen chloride is sent to the HCl absorption column, C1106, to produce 

hydrochloric acid at between 21% and 30%. The hydrochloric acid produced is sent to TK- 

1101, the hydrochloric acid collector tank, which is then sent to the storage section 4400 by 

pump B-1105. 

2.1.1.4 Reactor and Thermal Oil System 

This section consists of the hydrochlorination reactor (R-1101) and a thermal oil circulation 

system. 

The reactor tubes are full of the catalyst. 

The reheated hydrogen chloride and methanol are mixed just before entering the 

hydrochlorinator R-1101 and supply it.

The methanol reacts with the hydrogen chloride on the surface of the catalyst, producing 

methyl chloride and generating water, in accordance with the abovementioned reaction. 

The thermal oil passes through the thermal oil cooler, I-2501, through the casing of the 

hydrochlorinator R-1101 to eliminate the heat from the reaction and to control the reaction 

temperature (max. 300º C) and through the two reheaters I-1102 and I-1103, where it is used 

as a source of heat. The start-up heater, H-2501, is only used in the stoppages to keep the oil 

hot or to heat itself if it has cooled. 

The reactor effluent, methyl chloride and water together with small amounts of methanol and 

hydrogen chloride that have not reacted, are sent to the CH 3 Cl purification system. 

2.1.2 CH 3 Cl Purification System 

This system consists of a gas cooler (I-1104), a water washer (C-1101), a soda washer (C- 

1102) and three drying columns (C-1103 / C-1104 / C-1105). 

2.1.2.1 Gas Cooler and Water Washer 

The gas effluent from the reactor is cooled to approximately 30º C in the gas cooler I-1104 

with cooling water, mostly condensed by the water generated and the methanol and hydrogen 

chloride that has not reacted. The gases are sent through the bottom of the water washer C- 

1101, where the uncondensed hydrogen chloride and methanol are eliminated. The bottom, 

diluted waste hydrochloric acid, is sent to effluent treatment by means of pump B-1101, 

together with the waste caustic soda from the washer C-1102. 

2.1.2.2 Caustic Soda Washer 

The gas from the head of the water washer is sent to the bottom of the caustic soda washer C- 

1102, where it is washed with diluted soda solution to eliminate the acid, cooling to approx. 

18º C, to save on sulphuric acid consumption. From there, it is sent to the NaOH drop 

separator, which also serves to save on sulphuric acid consumption. The 40% MEG circulates 

through the soda washer cooler I-1105, in the recirculation system. The bottom of the column, 

waste caustic soda, is sent to the effluent treatment system by means of pump B-1102. 

2.1.2.3 Drying Column 

The drying system consists of three columns (C-1103 / C-1104 / C-1105), three coolers (I- 

1106 / I-1107 / I-1108) and four pumps (B-1103-1-2-3-s). 

Each one of these columns has a cooling system for the sulphuric acid in circulation. 

The NaOH drip separator, S-1101, is supplied by the bottom of the first drying column, C- 

1103, then passes to the second, C-1104, and finally the third, C-1105 to eliminate water, then 

being sent to the methyl chloride condensation system through the sulphuric drip separator, S- 

1102. The three towers require a graduation of the H 2 SO 4 richness, maintaining a minimum 

concentration of 92% in column C-1105, feeding 96% sulphuric acid into it to eliminate the 

water completely. The sulphuric acid from C-1105 passes by overflow to C-1104 and then

also by overflow to C-1103. The waste sulphuric acid is extracted from the bottom of C-1103 

and is sent to effluent treatment. 

The methyl chloride gas from C-1105 is sent to the CH 3 Cl condensation system after passing 

through the sulphuric acid drip separator. 

2.1.3 CH 3 Cl Condensation System 

The system consists of a CH 3 Cl pre-cooler (I-1109), a CH 3 Cl condenser (I-1110) and a CH 3 Cl 

receptor tank (D-1101). 

2.1.3.1 CH 3 Cl Pre-cooler 

To save energy in cooling, the CH 3 Cl gas is cooled in the CH 3 Cl pre-cooler, 

I-1109, before entering the CH 3 Cl condenser, I-1110. 

The CH 3 Cl exchanges heat with the cold HCl gas in column C-1201, condensing some of the 

CH 3 Cl. 

2.1.3.2 CH 3 Cl Condenser, Receptor Tank and Pump 

The CH 3 Cl is fed into the CH 3 Cl condenser, I-1110, where it is cooled, condensed and subcooled 

to under -20º C to prevent losses of CH 3 Cl. Cooling liquid (R-22) circulates through 

the casing of I-1110. The methyl chloride leaving the condenser passes on to the methyl 

chloride receptor tank, D-1101. 

2.1.4 Interrelation with the Rest of the Plant 

The chlorination section provides hydrogen chloride, from D-1205 (column C-1201 reflow 

ball), to the hydrochlorination section. Also, the excess hydrogen chloride goes to the acid 

absorption column, C-1106. 

Furthermore, the hydrochlorination provides methyl chloride to the chlorination section 

before passing through I-1111 (methyl chloride heater) and storage in D-1201 (storage tank 

for methyl chloride to the reactor). 

This is indirectly related to the thermal oil circuit through the thermal oil cooler, I-2501. It is 

also used in the cooling of the pumps in the thermal oil closed circuit B-2501-1/S. 

There is a cooling group that cools the I-1110 (methyl chloride condenser) and I-1205 

(condenser of column C-1201, HCl distiller), in the chlorination section. 

The methanol (CH 3 OH) has two tanks (TK-3101-1/2) with pumps (B-3102-1/S) to supply the 

process. 

The plant has a tank (TK-5201) for 98% sulphuric acid connected to a line with a pump to 

unload the tanker trucks. There are three supply pumps (B-5202-1/2/3) which supply the 

drying column C-1105.

The sulphuric acid from the bottom of C-1103 is sent to TK-6201 for regeneration. 

In column C-1106, 21-30% hydrochloric acid is produced which, by means of a pump, is sent 

to the storage tank (TK-4401) to be sent next to the dicalcium phosphate plant. 

2.2 Chlorination Section 

The chlorination section produces chloromethanes (methylene chloride, chloroform and 

carbon tetrachloride) by means of chlorination of liquid phase methyl chloride. 

To explain how this section works, it has been divided into three systems: 

1.- Chlorination reaction section. 

2.- HCl and CH 3 Cl recovery system. 

3.- CH 2 Cl 2 and CHCl 3 rectification system. 

2.2.1 Chlorination Reaction System 

2.2.1.1 Methyl Chloride Chlorination 

In the reaction system, the methyl chloride reacts with the chlorine in the presence of a 

catalyst to produce methylene chloride, chloroform and carbon tetrachloride, in accordance 

with the following reactions: 

CH 3 Cl + Cl 2 -----> CH 2 Cl 2 + HCl 

CH 2 Cl 2 + Cl 2 -----> CHCl 3 + HCl 

CHCl 3 + Cl 2 ------> CCl 4 + HCl 

The reactions occur using azobisisobutyronitrile (AIBN) as an initiator. 

2.2.1.2 Process Description 

The methyl chloride is supplied from D-1101 passing through the CH 3 Cl heater I-1111 to D- 

1201. The recycled methyl chloride passes through D-1206 and is then supplied to D-1201. 

The methyl chloride D-1201 is pressurised to approx. 35 kg/cm 2 by means of pump B-1201 

and is supplied to the methyl chloride filter, F-1201, where the iron impurities are eliminated. 

The filter output liquid current enters the line mixer M-1201. 

Also, the recycled liquid methylene chloride that passes through D-1203 is pressurised to 

approximately 35 kg/cm 2 by means of pump B-1204 and is supplied to the line mixer M- 

1201.

The methyl chloride and methylene chloride mixture enters through the bottom of R-1201 

through the distributor ring. 

The chlorine is supplied from the LIQUID CHLORINE STORAGE plant or the chlorine 

tank, to the D-1204, being pressurised to up to 35 kg/cm 2 by means of pump B-1205 which 

sends it to I-1202. Once vaporised, the chlorine gas is fed to the bottom of R-1201 through the 

distributor ring. 

The catalyst solution is pressurised to up to approximately 30 kg/cm 2 and is sent to R-1201 by 

two routes: half the solution is fed to the methyl chloride line with a constant flow, entering 

the bottom of R-1201 through the distributor ring and the rest is supplied directly to R-1201, 

dissolving in the reactor chloromethanes. The total amount of catalyst solution added is 

determined by the chlorine flow and controlled by B-1207-1/2/S with a variable speed motor. 

The liquid effluent from the reactors contains methyl chloride, methylene chloride, 

chloroform and carbon tetrachloride and the sub-product hydrogen chloride and is sent to the 

hydrogen chloride column C-1201. 

The effluent gas from the reactor that contains hydrogen chloride, methyl chloride and 

methylene chloride leaves from the heads of the reactor and is supplied to the chlorinator 

partial condenser, I-1203, where it is cooled to approx. 40º C and partially condensed. 

The effluent from I-1203 is separated into two parts: the liquid returns to the bottom of reactor 

R-1201 by gravity; the gas is fed to the hydrogen chloride column. 

2.2.1.3 Catalyst Preparation System 

The TK-1201 is first filled with methylene chloride, later adding the solid catalyst to prepare a 

5% AIBN solution. 

The catalyst is dissolved evenly by recirculation of the solution with B-1206. The TK-1201 

solution is transferred to TK-1202 through the same pump. TK-1201 is refilled with 

methylene chloride in the same amount to dissolve the remaining catalyst in the deposit. The 

solution goes to TK-1202. The TK-1202 solution is homogenised by recirculation with B- 

1206. The catalyst solution must always be below +5º C to prevent decomposition. 

2.2.2 HCl and CH 3 Cl Recovery System 

2.2.2.1 Hydrogen Chloride Column 

In the hydrogen chloride column, C-1202, the chloromethanes produced from the hydrogen 

chloride are separated. 

The gas current leaving I-1203 enters the hydrogen chloride column in plate no. 45. The 

liquid from the reactor enters plate no. 50. The column C-1202 operates at a pressure of 12 

kg/cm 2 . The amount of heat supplied by the re-boiler I-1204 is determined by the flow of 

steam.

One part of the steam from the heads condenses in I-1205, to then pass to the reflow ball, D- 

1205. The condenser of the HCl distillation column, I-1205, is cooled with R-22. The 

condensed product is returned, by means of B-1208, to the top of C-1201. 

The liquid at the bottom of column C-1201 that contains methylene chloride, chloroform, 

carbon tetrachloride and methyl chloride that has not reacted is fed to the methyl chloride 

column, C-1202, by pressure difference, through filter F-1203. 

2.2.2.2 Methyl Chloride Column 

In the methyl chloride column, C1202, the methyl chloride that has not reacted is separated 

from the crude product that contains methylene chloride, chloroform and carbon tetrachloride. 

The C-1201 operates at a pressure between 5.5 kg/cm 2 g and 7.0 kg/cm 2 g. 

The liquid current from the bottom of C-1201 enters the column through plate no. 19. The 

heat load from re-boiler I-1206 is determined by the steam flow. 

The steam of the column heads condenses in I-1207, the methyl chloride column condenser. 

The condensed product is sent to the methyl chloride reflow ball, D-1206. The condenser I- 

1207 is cooled with cooling water. One part of the condensed product returns as reflow to the 

head of C-1202. The rest of the condensed product, recycled methyl chloride, is sent to D- 

1201. The amount of recycled methyl chloride is determined by the level of reflow ball D- 

1206. 

The recycled methyl chloride is dried with calcium chloride in D-1207. 

The bottom of column C-1202 that contains methylene chloride, chloroform and carbon 

tetrachloride passes, by pressure difference, to the crude thermal recoverer, I-1208, to the 

crude cooler, I-1209 and from here to the crude ball, D-1208, The flow of this current is 

determined by the level of liquid at the bottom of C-1202. 

2.2.3 CH 2 Cl 2 and CH 3 Cl Rectification System 

2.2.3.1 Methylene Chloride Column 

The crude product is fed by means of B-1210 to the methylene chloride column, C-1203. 

In the methylene chloride column, C-1203, the methylene chloride is separated from the crude 

product that contains chloroform and carbon tetrachloride. 

The supply from D-1208 enters plate no. 48 of C-1203. The heat load of the re-boiler I-1211 

is determined by the flow of steam. 

The steam from the head of C-1203 is condensed in the methylene chloride column 

condenser, I-1212, by means of cooling water and passes on to the methylene chloride reflow 

ball, D-1210. Part of the liquid from D-1210 is sent as reflow to the top of C-1203. The reflow 

ratio is determined by the level of liquid in D-1210. The rest of the condensed product,

ecycled methylene chloride, is sent to the methylene chloride recycling tank, D-1203, after 

passing through the methylene chloride recycling cooler, I-1214. 

The methylene chloride is extracted in liquid phase from the 5th plate of C-1203 and is cooled 

in I-1215, the methylene chloride product cooler, where it goes to TK-1205-1/2, daily 

methylene chloride tanks. 

The bottom of C-1203, which contains chloroform and carbon tetrachloride, is sent to C- 

1204. 

2.2.3.2 Chloroform Column 

In the chloroform column, C-1204, the chloroform is separated from the carbon tetrachloride. 

The supply, from C-1203, may vary at the entry to the column depending on the chloroform 

supplied to the reaction. If it is debrominated chlorine, the entry is through plate 80; whereas 

if the chlorine is not distilled it is fed through plate no. 61 of C-1204. The head load supplied 

by the re-boiler, I-1216, is determined by the flow of steam, which depends on the amount of 

liquid fed to C-1204. 

The steam at the head is condensed in I-1217 by means of cooling water, passing to the reflow 

ball, D-1212. Part of the condensed product is returned to C-1204 as reflow. A small part of 

the condensed product is sent to D-1208. 

The chloroform product is extracted as liquid from plate no. 5 of C-1204; it is cooled with 

cooling water in I-1219, the chloroform cooler, and is then sent to the daily chloroform tanks, 

TK-1206-1/2. 

The crude carbon tetrachloride that contains some chloroform and heavy products is 

removed from the bottom of C-1204 and is sent by pump B-1205 to the carbon 

tetrachloride storage section.

CHLOROMETHANE PRODUCTION PROCESS 

Organic gas effluent 

Thermal 

treatment plant 

Water 

NaOH 

Soda 

H 2 SO 4 

Sulphuric 

HCl 

Hydrogen chloride 

Methane 

Hydrochlorination 

Chlorine 

Methyl chloride 

Methylene chloride 

Chlorination 

Methyl 

chloride 

HCl 

CH 2 Cl 2 , CHCl 3 ,CCl 4 

Rectification 

Carbon tetrachloride 

Chloroform 


Recovery of methanol, 

hydrochloric acid 

and sulphuric acid 

30% hydrochloric 

acid to 

dicalcium phosphate 

Cooling water 

Regenerated sulphuric 

acid for marketing 

Process waters treated in 

stripping section 

Outlet to 

collector

2.3 Services 

2.3.1 MEG Cooling System to -20º C 

2.3.2 R-22 Cooling System to -40º C 

2.3.3 Demineralising Lines 

The chloroform plant has a double installation of water demineralising lines. Their 

operation is automatic and can treat a flow of 20 m 3 /h and a production of up to 160 m 3 per 

cycle. 

Each treatment line consists of a sand filter, a strong cation column and weak anion 

column. The filtration speed is 10 m/sec. 

For the regeneration of the lines per 160 m 3 production cycle, the following reagents are 

consumed: 

- 28 % HCl 

- 20 % NaOH 

The water in the factory mains system is fed to a sand filter F-2101-1/2. From there, it 

passes on to the first cation line D-2101-1/2 where the positive saline ions are retained by 

the line resins through chemical exchange. 

Next, and in series, this water is fed to a second anion line D-2101-1/2 where the negative 

saline ions are exchanged and retained by the resins. 

Finally, neutral water is obtained with a quality of: 

- Max. 12.5 ppm chlorines (10 ppm normal). 

- Total hardness of 10 ppm as CaCo 3 . 

After a production cycle, the automatic regeneration feeds hydrochloric acid to the cation 

column and sodium hydroxide to the anion column. The reagents are decanted by pump 

from the storage tanks and are diluted with water in a mixing chamber before entering the 

lines. 

The sand filter is washed against the current with a flow of 40 m 3 of factory mains water. 

This water is sent to the rainwater drains. 

The saline water from the line regeneration goes to the neutralisation pool, TK-2105, with 

a capacity of 30 m 3 , where the hydrochloric acid or caustic soda is added to obtain a neutral 

pH. From here, it is sent to the rainwater drains by pump B-2106. 

2.4 Effluents 

2.4.1 Organic Hydrochloric Plant

The bottom of columns C-1101 (aqueous wash) and C-1102 (caustic wash) of the 

hydrochlorination section are sent to this section for recovery of the hydrochloric acid, 

methyl chloride and methanol. 

The bottom of this column is sent to the column C-6101, before reheating in I-6105. The 

water vapour, methyl chloride and methanol are released from the head, condensed in I- 

6104 and collected in ball D-6101. The uncondensed methyl chloride is sent to the head of 

the aqueous wash column C-1101. 

Also, the condensed products from D-6101 are sent partly as reflow to C-6101 and partly 

to supply the methanol distillation column C-6102. 

The bottom of C-6101, with a composition of approximately 6% weight of hydrochloric 

acid, is cooled in I-6105 and sent to the hydrogen chloride absorption column C-1106 

through pumps B-6101-1/S. 

Under normal operation conditions, steam is injected in the bottom of C-6101 at approx. 

3.5 kg/cm 2 g to obtain perfect separation. 

The column C-6102 separates water at the bottom and methanol at the head which, once 

condensed in I-6102 and collected in D-6102, is sent partly as reflow to the head of C- 

6102 and partly returned again to the methanol vaporiser, I-1101, by means of pumps B- 

6102-1/S. 

The thermal load in this column is provided by the re-boiler I-6103 by means of steam at 

approx 3.5 kg/cm 2 g. 

The water at the bottom is released by means of a siphon and is sent to the slop tank, so 

that the level of this column remains constant. 

2.4.2 Sulphuric Acid Regeneration Plant 

The purpose of the sulphuric acid regeneration plant is to eliminate organic material in the 

sulphuric acid from the drying columns and concentrate it. 

The plant is divided into two stages. In the first, which operates at 80 mBar, the organic 

material is eliminated and the acid is concentrated to approximately 85%. In the second, 

which operates at 20mBar, the acid is concentrated to approx. 92%. 

The acid from the drying columns is stored in the TK-6301 from where it is pumped by 

means of the B-6301-1/S to the regeneration plant. 

The acid enters the D-6302. A current of N 2 also reaches this tank, varying on the plant 

load. A flash is produced at the tank entry (P = 80 mBar) which, together with the N 2 

current, eliminates most of the dimethyl ether and the methyl chloride (approximately 

95%). 

The pressure in this stage is controlled by the N 2 flow. If the pressure in the stage 

increases, the N 2 input valve is closed. However, this valve is not completely closed

ecause, for safety reasons, it is important for N 2 to circulate constantly, so a minimum 

flow is ensured. 

The acid from D-6302 enters the heads of the stripping column C-6301. The N 2 together 

with the dimethyl ether and methyl chloride are sent to the flare through the vacuum pump 

K-6301-1/S. 

The C-6301 is the stripping column. The acid diluted with water from D-6302 (max. 

concentration 60%) enters it at the head and a current of dry N 2 (approx. 3 kg/h) enters at 

the bottom. The N 2 produces the stripping of the rest of the dimethyl ether and the methyl 

chloride that leaves the head with some water. The N 2 flow is measured by rotameter and 

is variable. 

The N 2 current with dimethyl ether, methyl chloride and water vapour goes to the I-6305 

condenser. The current at the bottom, approximately 80% sulphuric acid, enters the I-6303 

where it is heated with steam at approx. 11.5 bar to 150º C, separating the eliminated water 

vapour and sulphuric acid with a concentration of approximately 85% in D-6307. 

The water vapour passes to the condenser I-6306. 

The sulphuric acid passes on to the 2nd concentration stage in D-6303. From D-6303 the 

acid enters the column C-6302. The head of this column is connected to the ejector E-6301 

which produces the vacuum in the 2nd stage. The acid continues to concentrate in C-6302. 

The current at the bottom is pumped by B-6303, and passes through the thermal oil heater 

where it is heated to 180º C and enters D-6305. In D-6305 the water vapour, which enters 

from the bottom of C-6302, and the sulphuric acid, concentrated to 96%, is separated. 

The concentrated acid enters the D-6306 where one part overflows to I-6302 and the rest is 

recycled to the thermal oil heater. 

The approx. 92% acid that overflows from D-6306 enters I-6302, where is it cooled with 

water. 

The acid released from I-6302 finishes cooling in I-6308 with water. It is released at 

approx. 40º C and enters D-6301 where it drops to atmospheric pressure and is pumped by 

B-6302-1/S to the storage tank. 

The steam from the heads of C-6302, together with the steam from the ejector and the D- 

6307 enter the condenser I-6306. The condensed water is sent to D-6304. The steams that 

are not condensed join the current from the head of C-6301 and go to condenser I-6305. 

The condensed liquid in I-6305 goes to D-6304 as well as the water used by the vacuum 

pumps K-6301-1/2, where it is sent to the drains. 

In order to prevent the build up of carbon in the system, a small amount of nitric acid is 

continually dosed, which destroys the carbon as it forms.

3.- MECHANICAL EQUIPMENT INVENTORY 

1.- COOLING UNITS 

2.- PUMPS 

3.- COLUMNS 

4.- TANKS 

5.- EXCHANGERS 

6.- REACTORS 

7.- TANKS 

8.- SEPARATORS 

9.- BOILERS 

10.- COMPRESSORS 

11.- VENTILATORS 

12.- HEATERS 

13.- FILTERS - TUBS

1.- COOLING UNITS 

A-2301 (-20º C) 

SUPPLIER: SULZER 

COOLANT LIQUID: R-22 

COOLED PRODUCT: ETHYLENE GLYCOL 

WORKING CONDITIONS: -25 / +40º C 

COOLING POWER: 58 kW 

INSTALLATION: 

- 2 Motorcompressors K-2301-1/S 

- 2 Viking oil motor-pump sets B-2303 -1/S 

- 2 Oil coolers I-2303-1/S 

- 2 Oil separators S-2301-1/S 

- 1 Condenser I-2302 

- 1 Monoethylene glycol cooler I-2301 

- 1 Glycol accumulator recipient D-2301 

- 2 Glycol secondary circuit motor-pump sets B-2301 -1/S 

- 2 Primary circuit motor-pump sets B-2302 -1/S 

Characteristics of the Equipment in this Cooling Unit 

K-2301-1/S Compressor -20º C Cooling Unit 

ITEM: K-2301-1/S 

NAME: MONOETHYLENE GLYCOL COOLING 

COMPRESSOR UNIT –20º C 


TYPE: GHH-MAN SCREW 

MODEL: CR-90 

VOLUMETRIC RATIO: VI = 4.8 


ABSORBED POWER: 31 kW 

SPEED: 2,950 r.p.m. 

SUCTION PRESSURE: +2.016 bar abs.(-25º C) 

DISCHARGE PRESSURE: 14.54 bar abs.(+38º C) 

CAPACITY RATIO: FROM 10 % TO 100 % 

MOTOR POWER: 37 kW 

MOTOR SPEED: 2,950 r.p.m. 

MOTOR-COMPRESSION TRANS.: COUPLING 

VULKAN NORMEX H-14 

No. UNITS: 2

B-2303 -1/S Oil Circulation Pump 2300 – Closed MEG Circuit (-20ºC) 

ITEM: B-2303 1/S 

NAME: OIL CIRCULATION PUMP 

MAKE: VIKING 

MODEL: HL-4195 (geared) 

LIQUID: MEG –20ºC 

Flow: 98 litres/min 

Discharge pressure: 

Suction pressure: 14.58 bars abs 

Differential pressure: 20 bar 

R.P.M.: 1.450 

POWER: 2.2 KW 

No. UNITS: 2 

I-2303-1/S Oil Cooler 2300 – MEG Closed Circuit (-20ºC) 

ITEM: I-2303-1/S 

NAME: OIL COOLER 

MANUFACTURER: SULZER ESPAÑA 

TYPE: Oil cooler 

EXCHANGE SURFACE: 24.8 m2 

BODY SIDE: 

LIQUID: Oil 

SERVICE PRESSURE: 17 kg/cm2 

DESIGN PRESSURE: 27 kg/cm2 

SERVICE TEMPERATURE: 45º C 

DESIGN TEMPERATURE: 80º C 

BODY MATERIAL: API-SL-B 

TUBE SIDE: 

LIQUID: water 


DESIGN PRESSURE: 10.5 kg/cm2 


DESIGN TEMPERATURE: 50ºC 

MATERIAL: API-SL-B / H-II 

SIZE: 

LENGTH: 2,544 mm 

DIAMETER: 220 mm 

INSULATION: NO 

No. UNITS: 2

S-2301-1/S Oil Separator 2300 – MEG Closed Circuit (-20ºC) 

ITEM: S-2301 1/S 

NAME: OIL SEPARATOR 

SUPPLIER: SULZER ESPAÑA 

LIQUID: NH3 gas + oil 



SERVICE PRESSURE: 13.5 bar 

DESIGN PRESSURE: 21 bar 

CAPACITY: 0.32 m 3 

MATERIAL: H-II 

SIZE: 

- Length: 1,750 mm 

- Diameter: 500 mm 


No. UNITS: 2 

I-2302 Freon Condenser 2300 – MEG Closed Circuit (-20ºC) 

ITEM: I-2302 

NAME: FREON CONDENSER 


TYPE: Freon condenser 

EXCHANGE SURFACE: 238 m2 

BODY SIDE: 

LIQUID: R-22 

SERVICE PRESSURE: 14.8 bars abs 


SERVICE TEMPERATURE: 38 → 38º C 


BODY MATERIAL: H-II 

TUBE SIDE: 

LIQUID: WATER 

SERVICE PRESSURE: 3.5 bars abs 



DESIGN TEMPERATURE: 50ºC 

MATERIAL: SF-Cu Trufin 19 fpi 

SIZE: 




No. UNITS: 1

I-2301 Monoethylene glycol Cooler 2200 – MEG Closed Circuit (-20ºC) 

ITEM: I-2301 

NAME: MONOETHYLENE GLYCOL COOLER 


TYPE: Cooler 

EXCHANGE SURFACE: 

BODY SIDE: 

LIQUID: Ethylene glycol 



SERVICE TEMPERATURE: -20º C 

DESIGN TEMPERATURE: -30º C 

BODY MATERIAL: API-SL-Gr.B 

TUBE SIDE: 

LIQUID: R-22 





MATERIAL: API-SL-Gr.B 

SIZE: 




No. UNITS: 1 

D-2301 EG Supply Tank 2300 – Cold 

ITEM: D-2301 

NAME: EG LUNG TANK 


LIQUID: ETHYLENE GLYCOL 

MATERIALS: 

- Ferrule and floors: H-II 

TEMPERATURE: 

- Service: -20º C 

- Design: 

PRESSURE: 

- Service: 4 kg/cm2 g 

- Design: 6 bar 

SIZE: 

- Height: 3,000 mm 

- Diameter: 1,250 mm 


INSULATION: YES 

No. UNITS: 1

B-2301 -1/S Cooling Unit Pump 2300 – Cold 

ITEM: B-2301 1/S 

NAME: SECONDARY CIRCUIT CIRCULATION 

PUMP 

MAKE: ITUR 

MODEL: INP-50/315 


Q (m 3 /h): 20 

Discharge pressure: 

Suction pressure: 

Differential pressure: 3.6 kg/cm2 

Available NPSH (m): 

R.P.M.: 1,450 

POWER: 7.5 KW 

MATERIALS: GG-25 

No. UNITS: 2 

B-2302 -1/S EG Service Pump 2300 – Cold 

ITEM: B-2302-1/S 

NAME: MEG 20º C CLOSED PRIMARY CIRCUIT 

CIRCULATION PUMP 

MAKE: ITUR 

MODEL: INP-40/250 


Q (m 3 /h): 20 

Discharge pressure: 1.5 kg/cm2 

Suction pressure: 

Differential pressure: 1.5 kg/cm2 


R.P.M.: 1.450 

POWER: 2.2 KW 

MATERIALS: GG-25 

No. UNITS: 2

A-2701 (-40º C) 


COOLANT LIQUID: R-22 

COOLED PRODUCT: HYDROGEN CHLORIDE AND METHYL CHLORIDE 

WORKING CONDITIONS: -40 / +40º C 


INSTALLATION: 

- Motor- compressor K-2701 

- Condenser I-2702 

- Freon accumulator D-2703 

- Economiser D-2702 

- HCl evaporator I-1205 

- ClCH3 evaporator I-1110 

- Suction drip separator: D-2701 

- Oil separator S-2701 

- Oil cooler I-2703 

- 2 Oil motor-pump B-2701 -1/S 

- 2 Oil discharge filters F-2701 

- 3 Oil recoverers 

Characteristics of the Equipment in this Cooling Unit 

K-2701 Freon Compressor 2700 - R-22 Cooling System (-40ºC) 

ITEM: K-2701 

NAME: FREON COMPRESSOR 


TYPE: GHH-MAN SCREW 

MODEL: CR-200/1.60 

VOLUMETRIC RATIO: VI = 4.8 


ABSORBED POWER: 324 kW 


ASPIRATION PRESSURE: +1.155 bar abs.(-38 ºC) 

INTERMEDIATE PRESSURE: 3,807 bar abs. (-8º C) 

DISCHARGE PRESSURE: 14,54 bar abs.(+38º C) 

CAPACITY RATIO: FROM 10 % TO 100 % 

OIL INPUT TEMPERATURE +40º C 

DISCHARGE TEMP. OIL: +70º C. 

MOTOR POWER: 400 kW 

MOTOR SPEED: 2,950 r.p.m. 

MOTOR-COMPRESSION TRANS.: COUPLING 

VULKAN H-240/180 

No. UNITS: 1

I-2702 Freon Condenser 2700 - R-22 Cooling System (-40ºC) 

ITEM: I-2702 

NAME: FREON CONDENSER 


TYPE: Freon condenser 


BODY SIDE: 

LIQUID: R-22 

SERVICE PRESSURE: 14.6 kg/cm2 



DESIGN TEMPERATURE: 80º C. 


TUBE SIDE: 

LIQUID: water 






SIZE: 




No. UNITS: 1 

D-2703 Freon Accumulator 2700 - R-22 Cooling System (-40ºC) 

ITEM: D-2703 NAME: R-22 COOLING SYSTEM SERVICE FREON 

ACCUMULATOR TANK (- 40º C) 

LIQUID: R-22 

MATERIALS: 


- Receptacle support: A 283 

TEMPERATURE: 

- Service: +38º C 

- Calculation: 80º C. 

PRESSURE: 

- Service: 14.6 kg/cm2 g 

- Calculation: 21 kg/cm2 g 

SIZE: 





No. UNITS: 1

D-2702 Freon Economiser 2700 - R-22 Cooling System (-40ºC) 

ITEM: D-2702 

NAME: R-22 COOLING SYSTEM SERVICE FREON 

ECONOMISER TANK (–40º C) 

CASING 

LIQUID: R-22 

MATERIALS: 


TEMPERATURE: 


PRESSURE: 



SIZE: 





No. UNITS: 1 

COIL 

LIQUID: R-22 

MATERIALS: 

- Tubes: A-333 Gr.60 

TEMPERATURE: 


PRESSURE: 


- Calculation: 21 kg/cm2 g

I-1205 HCl Distillation Column Condenser 1200 – Chlorination 

ITEM: I-1205 

NAME: HCL DISTILLATION COLUMN CONDENSER 


TYPE: R-22 Evaporator / HCl Condenser 


BODY SIDE: 

LIQUID: R-22 

SERVICE PRESSURE: 1.155 bar abs. 

DESIGN PRESSURE: 10.5 kg/cm2 g 

SERVICE TEMPERATURE: -38 → -38º C 


BODY MATERIAL: A-516-60 

TUBE SIDE: 

LIQUID: HCl 

SERVICE PRESSURE: 12.75 bar abs. 




MATERIAL: A-213 TP 316 L 

No. TUBES: 339 

SIZE: 

LENGTH: 3,200 / 4,192 mm 

DIAMETER: 550 / 650 mm 


No. UNITS: 1 

I-1110-A Oil Recoverer 1100 – Hydrochlorination 

ITEM: I-1110 A 

NAME: OIL RECOVERER 

MANUFACTURER: SULZER 

TYPE: Oil recoverer 


BODY SIDE: 

LIQUID: R-22 





BODY MATERIAL: St.35 

TUBE SIDE: 

LIQUID: R-22 + oil 






No. TUBES: 

SIZE: 


DIAMETER: DN 125 


No. UNITS: 1

D-2701 Drip Separator 2700 - R-22 Cooling System (-40ºC) 

ITEM: D-2701 

NAME: R-22 COOLING SYSTEM SERVICE DRIP 

SEPARATOR TANK (-40º C) 

LIQUID: R-22 

MATERIALS: 


- Receptacle support: H-II 

TEMPERATURE: 


- Calculation: -40º C 

PRESSURE: 


- Calculation: 10.5 kg/cm2 g 

SIZE: 





No. UNITS: 1 

S-2701 Oil Separator 2700 - R-22 Cooling Circuit (-40ºC) 

ITEM: S-2701 

NAME: OIL SEPARATOR 


LIQUID: R-22 gas + oil 

SERVICE TEMPERATURE: 80º C. 


SERVICE PRESSURE: 15 bar 




SIZE: 




No. UNITS: 1

I-2703 Oil Cooler 2700 - R-22 Cooling System (-40ºC) 

ITEM: I-2703 

NAME: OIL COOLER 


TYPE: Oil cooler 


BODY SIDE: 

LIQUID: Oil 





BODY MATERIAL: API-SL-B 

TUBE SIDE: 

LIQUID: water 





MATERIAL: API-SL-B / H-II 

SIZE: 




No. UNITS: 1 

B-2701 -1/S Oil Pump 2600 - R-22 Cooling System (-40ºC) 

ITEM: B-2701 1/S 

NAME: OIL PUMP 

MAKE: LEISTRITZ 

MODEL: L3MG 52/85 – IHOKI - G 

LIQUID: synthetic oil 

Q (l/min): 280 

Discharge pressure (bar): 

Suction pressure (bar): 14 - 17 

Differential pressure (bar): 3 – 6 

R.P.M.: 2.900 

POWER: 5.5 kW 

No. UNITS: 2

F-2701 -1/S Oil Filter 2600 - R-22 Cooling System (-40ºC) 

ITEM: F-2701 1/S NAME: OIL FILTER 


LIQUID: OIL

2.- PUMPS 

B-1101 -1/S Water Washer Pump 1100 – Hydrochlorination 

ITEM: B-1101 1/S 

NAME: WATER WASHER PUMP 

MAKE: VICARB 

MODEL: P-20 

LIQUID: H 2 O, HCl 

Q (m 3 /h): 2.1 

Discharge pressure: (kg/cm2 r): 4 

Suction pressure (kg/cm2 r): 1.2 

Differential pressure (kg/cm2): 2.8 

Available NPSH (m): 2 min 

R.P.M.: 3,000 

POWER: 6.3 CV 

MATERIALS: C.S.+(ETFE) lining 

No. UNITS: 2 

B-1102 -1/S Soda Washer Pump 1100 – Hydrochlorination 

ITEM: B-1102 

1/S 

NAME: SODA WASHER PUMP 

MAKE: G.I.E. MARELLI, S.A. 

MODEL: SMKDO-1 ½ x 2 x 7 

LIQUID: H 2 O 

Q (m 3 /h): 10.4 

Discharge pressure: (kg/cm2 r): 4 




R.P.M.: 3,000 

POWER: 3.4 CV 

MATERIALS: A 216WCB 

No. UNITS: 2

B-1103-1/2/3/S Drying Column 1st Pump 1100 – Hydrochlorination 

ITEM: B-1103 1/2/3/S 

NAME: DRYING COLUMN PUMP 

MAKE: MAZDA PUMP MFG CO, LTD 

MODEL: SV-403MS 

LIQUID: SO 4 H 2 (69 – 91 %) 

Q (m 3 /h): 8 

Discharge pressure: (kg/cm2 r): 4.11 



Available NPSH (m): 2.6 min 

R.P.M.: 1,450 

POWER: 

MATERIALS: SWEISEN 

No. UNITS: 4 

B-1104 -1/S Methyl Chloride Pump 1100 – Hydrochlorination 

ITEM: B-1104-1/S NAME: METHYL CHLORIDE PUMP 

MAKE: NIKKISO 

MODEL: HQ23F-C3 

LIQUID: methyl chloride 

Q (m 3 /h): 1.8 

Discharge pressure (kg/cm2 r): 11.7 

Suction pressure (kg/cm2 r): 1 

Differential pressure (kg/cm2):10.7 


R.P.M.: 3,000 

POWER: 18.5 kW 

MATERIALS: A 351CF8M 

No. UNITS: 2

B-1105 -1/S Hydrochloric Acid Pump 1100 – Hydrochlorination 

ITEM: B-1105-1/S 

NAME: HYDROCHLORIC ACID PUMP 

MAKE: VICARB 

MODEL: P-20 

LIQUID: H 2 O, HCl 

Q (m 3 /h): 2.3 

Discharge pressure (kg/cm2 r): 4 




R.P.M.: 3,000 

POWER: 10 CV 

MATERIALS: C.S.+(ETFE) lining 

No. UNITS: 2 

B-1106 Methanol Drainage Pumps 1100 – Hydrochlorination 

ITEM: B-1106 

NAME: METHANOL DRAINAGE PUMP 

MAKE: DOSAPRO MILTON 

MODEL: A 112-FR-111 (MEMBRANE) 

LIQUID: Methanol 

Q (m 3 /h): 10 l/h(max.);1 l/h(min.) 

Discharge pressure: (kg/cm2 r): 3.5 



Available NPSH (m): 0 

PISTON: 1 

R.P.M.: 1,500 

POWER: 0.33 CV 

MATERIALS: 

- Body 18-8-Mo 

- TEFLON diaphragm 

No. UNITS: 1

B-1107 Water Accelerator Pump 1100 – Hydrochlorination 

ITEM: B-1107 

NAME: WATER ACCELERATOR PUMP 

MAKE: ITUR 

MODEL: IN 32-250 bF 

LIQUID: water 

Q (m 3 /h): 2 

Total height (m): 1 

R.P.M.: 1.430 

POWER: 1.8 CV 

No. UNITS: 1 

B-1201 -1/S Methyl Chloride Supply Pumps 1200 – Chlorination 

ITEM: B-1201 

1/S 

NAME: METHYL CHLORIDE SUPPLY PUMP 

MAKE: HERMETIC PUMPEN GMBH 

MODEL: CAM 25/6+6 


Q (m 3 /h): 3 



Differential pressure (kg/cm2):27 


R.P.M.: 3,000 

POWER: 15 kW 

MATERIALS: 1.4581 

No. UNITS: 2

B-1202 Methyl Chloride Load Pump 1200 – Chlorination 

ITEM: B-1202 

NAME: METHYL CHLORIDE LOAD PUMP 

MAKE: NIKKISO 

MODEL: CANNET 

LIQUID: Methyl Chloride Q (m 3 /h): 5 

Discharge pressure: (kg/cm2 g): 10.1 




R.P.M.: 3,000 

POWER: 5.1 kW 

MATERIALS: A351CF8M 

No. UNITS: 1 

B-1203 Methyl Chloride Decanting Pump 1200 – Chlorination 

ITEM: B-1203 

NAME: METHYL CHLORIDE DECANTING PUMP 

MAKE: NIKKISO 

MODEL: CANNET 


Q (m 3 /h): 5 





R.P.M.: 3,000 



No. UNITS: 1

B-1204 -1/S Methylene Chloride Supply Pump 1200 – Chlorination 

ITEM: B-1204 1/S 

NAME: METHYLENE CHLORIDE SUPPLY PUMP 



LIQUID: Methylene chloride 

Q (m 3 /h): 1.9 





R.P.M.: 3,000 

POWER: 17 kW 


No. UNITS: 2 

B-1205 -1/S Chlorine Supply Pump 1200 – Chlorination 

ITEM: B-1205 1/S 

NAME: HERMETIC CHLORINE SUPPLY PUMP 



LIQUID: chlorine 

Q (m 3 /h): 3.4 





R.P.M.: 3,000 

POWER: 17 kW 


No. UNITS: 2

B-1206 Catalyst Preparation Pump 1200 – Chlorination 

ITEM: B-1206 NAME: CATALYST PREPARATION PUMP 

MAKE: NIKKISO 

MODEL: CANNED 


Q (m 3 /h): 11.2 





R.P.M.: 3,000 

POWER: 17 kW 


No. UNITS: 1 

B-1207-1/2/S Catalyst Supply Pump 1200 – Chlorination 

ITEM: B-1207 1/2/S 

NAME: CATALYST SUPPLY PUMP 

MAKE: NIKKISO 

MODEL: CANNED 


Q (m 3 /h): 18.5 





R.P.M.: Variable 

POWER: 0.4 kW 

MATERIALS: SUS316 

No. UNITS: 3

B-1208 -1/S HCl Distillation Reflow Pump 1200 – Chlorination 

ITEM: B-1208 1/S NAME: HCL DISTILLATION REFLOW PUMP 

MAKE: NIKKISO 

MODEL: CANNED 

LIQUID: HCL 

Q (m 3 /h): 2.4 





R.P.M.: 3,000 

POWER: 1.6 kW 


No. UNITS: 2 

B-1209 -1/S Methyl Chloride Reflow Pumps 1200 – Chlorination 

ITEM: B-1209 1/S NAME: METHYL CHLORIDE REFLOW PUMP 

MAKE: NIKKISO 

MODEL: CANNED 


Q (m 3 /h): 2.7 





R.P.M.: 3,000 

POWER: 2.3 kW 


No. UNITS: 2

B-1210 -1/S Crude Pumps 1200 – Chlorination 

ITEM: B-1210 1/S 

NAME: CRUDE PUMP 

MAKE: NIKKISO 

MODEL: CANNED 


Q (m 3 /h): 4.7 





R.P.M.: 3,000 

POWER: 3.1 kW 

MATERIALS: A351CF8 

No. UNITS: 2 

B-1211 -1/S Methylene Chloride Reflow Pump 1200 – Chlorination 

ITEM: B-1211 1/S 

NAME: METHYLENE CHLORIDE REFLOW PUMP 

MAKE: NIKKISO 

MODEL: CANNED 


Q (m 3 /h): 9.7 





R.P.M.: 3,000 

POWER: 5.1 kW 


No. UNITS: 2

B-1212 -1/S Methylene Chloride Bottom Pump 1200 – Chlorination 

ITEM: B-1212 1/S NAME: METHYLENE CHLORIDE BOTTOM PUMP 

MAKE: NIKKISO 

MODEL: CANNED 


Q (m 3 /h): 2.5 





R.P.M.: 3,000 

POWER: 0.9 kW 


No. UNITS: 2 

B-1214 -1/S Chloroform Reflow Pump 1200 – Chlorination 

ITEM: B-1214 1/S NAME: CHLOROFORM REFLOW PUMP 

MAKE: NIKKISO 

MODEL: CANNED 

LIQUID: chloroform 

Q (m 3 /h): 12.3 





R.P.M.: 3,000 

POWER: 11 kW 


No. UNITS: 2

B-1215 -1/S Chloroform Bottom Pump 1200 – Chlorination 

ITEM: B-1215 

1/S 

NAME: CHLOROFORM BOTTOM PUMP 

MAKE: NIKKISO 

MODEL: CANNED 


Q (m 3 /h): 0.4 





R.P.M.: 3.000 



No. UNITS: 2 

B-1217 Daily Methylene Chloride Tank Pump 1200 – Chlorination 

ITEM: B-1217 

1/S 

NAME: DAILY METHYLENE CHLORIDE TANK PUMP 

MAKE: NIKKISO 

MODEL: CANNED 


Q (m 3 /h): 10.5 





R.P.M.: 

POWER: 3.1 kW 


No. UNITS: 2

B-1218 Daily Chloroform Tank Pump 1200 – Chlorination 

ITEM: B-1218 

1/S 

NAME: DAILY CHLOROFORM TANK PUMP 

MAKE: NIKKISO 

MODEL: CANNED 


Q (m 3 /h): 47.1 





R.P.M.: 3,000 



No. UNITS: 2 

B-2104 CIDA 28% Hydrochloride Regeneration Line Pump 

ITEM: B-2104 

NAME: CIDA 28% HYDROCHLORIDE REGENERATION 

LINE PUMP 

MAKE: SOINER 

MODEL: PN/80-50-315 

LIQUID: 28% HYDROCHLORIC ACID 

Q (m 3 /h): 5 

Manometric height: 26.70 m.c.l. 

R.P.M.: 1,450 

POWER: 7.5 CV 

MATERIALS: Polypropylene 

No. UNITS: 1

B-2105 CIDA 20 % Sodium Hydroxide Line Pump 

ITEM: B-2105 NAME: CIDA 20% SODIUM HYDROXIDE LINE PUMP 

MAKE: SOINER 

MODEL: IN/80-50-315 

LIQUID: 20% SODIUM HYDROXIDE 

Q (m 3 /h): 3 

Manometric height: 24.60 m.c.l. 

R.P.M.: 1,450 

POWER: 7.5 CV 

MATERIALS: stainless steel 

No. UNITS: 1 

B-2106 CIDA Water Pool Emptying Pump 

ITEM: B-2106 

NAME: CIDA WATER POOL EMPTYING PUMP 

MAKE: SOINER 

MODEL: PN/65-40-250 

LIQUID: EFFLUENTS 

Q (m 3 /h): 8 

Manometric height: 20 m.c.l. 

R.P.M.: 1,415 

POWER: 4 CV 

MATERIALS: Polypropylene 

No. UNITS: 1

B-2107-s Demineralised Water Pump Cooling 

ITEM: B-2107 

1/S 

NAME: COOLING WATER SERVICE DEMINERALISED 

WATER PUMP 

MAKE: SERRANO INDUSTRIAL 

MODEL: 32-160/Q-31669/322 

LIQUID: DEMINERALISED WATER 

Q (m 3 /h): 20 

Discharge pressure: 3 kg/cm2 

Suction pressure: atmospheric 

Differential pressure: 3 kg/cm2 


R.P.M.: 2,900 

POWER: 4 CV 

MATERIALS: 14408 

No. UNITS: 2 

B-2401 -1/S Ethylene Glycol Pumps 2400 - MEG Cooling Circuit (+8ºC) 

ITEM: B-2401 

1/S 

NAME: MEG +8º C ETHYLENE GLYCOL RECOVERY 

CIRCUIT 

MAKE: NIKKISO 

MODEL: CANNED 

LIQUID: Ethylene Glycol 

Q (m 3 /h): 11.8 





R.P.M.: 

POWER: 2.6 kW 


No. UNITS: 2

B-2501 -1/S Thermal Oil Pumps 2500- Thermal Oil Circuit 

ITEM: B-2501 

1/S 

NAME: THERMAL OIL CIRCUIT THERMAL OIL PUMP 

MAKE: G.I.E. MARELLI 

MODEL: SMK-4 x 6 x 13 

LIQUID: Thermal Oil 

Q (m 3 /h): 60.7 


Suction pressure (kg/cm2 g): 0.6 



R.P.M.: 1,500 


MATERIALS: C.S. casting 

No. UNITS: 2 

B-2901-1/2 Chlorinator Cooling Water Pump 2900 – Chlorinator Cooling 

Circuit 

ITEM: B-2901 

1/S 

NAME: DEMINERALISED WATER CIRCUIT 

CHLORINATOR COOLING WATER PUMP 


MODEL: SMKD-3 x 4 x 7 

LIQUID: Demineralised water 

Q (m 3 /h): 48.1 





R.P.M.: 

POWER: 10 kW 

MATERIALS: A216WCB 

No. UNITS: 2

B-2902-1/2 

Circuit 

ITEM: B-2902 

1/S 

Chlorinator Condenser Water Pump 2900 – Chlorinator Cooling 

NAME: DEMINERALISED WATER CIRCUIT 

CHLORINATOR CONDENSER WATER PUMP 


MODEL: SMKDO-3 x 5 x 7 


Q (m 3 /h): 105.7 





R.P.M.: 2,900 

POWER: 25 CV 

MATERIALS: A216WCB 

No. UNITS: 2 

B-3101 Methanol Tanker Unloading Pump 3100 – Methanol 

ITEM: B-3101 

NAME: METHANOL TANKER UNLOADING PUMP 

MAKE: NIKKISO 

MODEL: CANNED 


Q (m 3 /h): 50 





R.P.M.: 3,000 

POWER: 2.6 kW 


No. UNITS: 1

B-3102 -1/S Methanol Decanting Pump 3100 – 

Methanol 

ITEM: B-3102 

1/S 

NAME: METHANOL DECANTING PUMP 

MAKE: NIKKISO 

MODEL: CANNED 


Q (m 3 /h): 1.6 



Differential pressure (kg/cm2): 4 


R.P.M.: 

POWER: 2.3 kW 


No. UNITS: 2 

B-4101 -1/S Methylene Chloride Truck Loading Pump 4100- Methylene chloride 

ITEM: B-4101 

1/S 

NAME: METHYLENE CHLORIDE TRUCK LOADING 

PUMP 

MAKE: NIKKISO 

MODEL: CANNED 


Q (m 3 /h): 50 





R.P.M.: 3,000 



No. UNITS: 2

B-4201 -1/S Chloroform Truck Loading Pump 4200- Chloroform 

ITEM: B-4201 

1/S 

NAME: 

CHLOROFORM TRUCK LOADING PUMP 

MAKE: NIKKISO 

MODEL: CANNED 


Q (m 3 /h): 50 





R.P.M.: 3,000 

POWER: 11 kW 


No. UNITS: 2 

B-4301 -1/S Tetrachloride Decanting Pump 4300 - Carbon Tetrachloride 

ITEM: B-4301 

1/S 

NAME: CARBON TETRACHLORIDE DECANTING PUMP 

MAKE: NIKKISO 

MODEL: CANNED 

LIQUID: carbon tetrachloride 

Q (m 3 /h): 5.5 





R.P.M.: 3,000 

POWER: 5.7 kW 


No. UNITS: 2

B-4401 -1/S Hydrochloric Acid Decanting Pump 4400 – Hydrochloric Acid 

ITEM: B-4401 

1/S 

NAME: HYDROCHLORIC ACID DECANTING PUMP 

MAKE: VICARB 

MODEL: 65 – 40 - 200 

LIQUID: carbon tetrachloride 

Q (m 3 /h): 11 





R.P.M.: 3,000 

POWER: 7.5 kW 

MATERIALS: VGC 

No. UNITS: 2 

B-5101 20% Soda Decanting Pump 5100 – 20 % Soda 

ITEM: B-5101 

1/S 

NAME: AUXILIARY CHEMICAL PRODUCT 20% CAUSTIC 

SODA DECANTING PUMP 

MAKE: SUNFLO 

MODEL: FMDP – 1DHA 

LIQUID: 20% Caustic Soda 

Q (m 3 /h): 1 





R.P.M.: 1,500 

POWER: 2.5 kW 

MATERIALS: CARBON STEEL 

No. UNITS: 2

B-5201 Sulphuric Tanker Unloading Pump 5200 - 98% Sulphuric Acid 

ITEM: B-5201 

1/S 

NAME: AZOBIS SOLUTION 98% SULPHURIC 

DISCHARGE PUMP 

MAKE: WORTHINGTON 

MODEL: ECP 6 65 - 200 

LIQUID: 98% Sulphuric Acid 

Q (m 3 /h): 30 





R.P.M.: 1,000 

POWER: 1.5 kW 

MATERIALS: A-216WCB 

No. UNITS: 2 

B-5202 -1/S Sulphuric Decanting Pump 5200 - 98% Sulphuric Acid 

ITEM: B-5202 

1/S 

NAME: DRYING TOWERS H2SO4 ACID SUPPLY PUMP 

MAKE: SUNFLO 

MODEL: FMDP-1DHA 

LIQUID: 98% Sulphuric Acid 

Q (m 3 /h): 1 





R.P.M.: 1,500 

POWER: 4 kW 

MATERIALS: DUCTILE IRON 

No. UNITS: 3

B-6101 -1/S Methanol Recovery Column Reflow Pump 6100 – Organic Hydrochloric Acid 

ITEM: B-6101 

1/S 

NAME: METHANOL RECOVERY COLUMN REFLOW 

PUMPS 

MAKE: SUNFLO 

MODEL: FMDP-1DFA 

LIQUID: 80% Methanol 

Q (m 3 /h): 0.5 





R.P.M.: 1,500 

POWER: 2.5 kW 

MATERIALS: CARBON STEEL / STAINLESS 

STEEL 

No. UNITS: 2 

B-6102 -1/S Methanol Distillation Column Reflow Pump 6100 – Organic Hydrochloric Acid 

ITEM: B-6102 

1/S 

NAME: METHANOL DISTILLING COLUMN REFLOW 

PUMP 

MAKE: SUNFLO 

MODEL: FMP-1LSB 


Q (m 3 /h): 0.16 





R.P.M.: 1,500 

POWER: 1 kW 

MATERIALS: AISI 410 

No. UNITS: 2

B-6103 -1/S Methanol Bottom Recovery Column Pump 6100 – Organic Hydrochloric Acid 

ITEM: B-6103 

1/S 

NAME: METHANOL RECOVERY COLUMN BOTTOM 

PUMP 

MAKE: VICARB 

MODEL: 50-32-160 

LIQUID: HCl solution 

Q (m 3 /h): 2.85 





R.P.M.: 3,000 

POWER: 1.1 kW 

MATERIALS: VGC 

No. UNITS: 2 

B-6301 -1/S Schott Diluted Sulphuric Supply Pump 6300 – Sulphuric Acid Regeneration 

ITEM: B-6301 

1/S 

NAME: H2SO4 REGENERATION RESIDUAL EFFLUENT 

SULPHURIC ACID PUMPS 

MAKE: SERRANO - BOMINSA 

MODEL: 32-125 Q-31229/622 

LIQUID: 76% residual sulphuric acid 

Q (m 3 /h): 2.85 

Discharge pressure: (kg/cm2 g): 1 




R.P.M.: 2,900 

POWER: 2.52 CV 


No. UNITS: 2

B-6302 -1/S Regenerated Sulphuric to D-5201 Pump 6300 – Sulphuric Acid Regeneration 

ITEM: B-6302 1/S 

NAME: REGENERATED SULPHURIC ACID PUMP 

MAKE: ATLAS COMERCIAL 

MODEL: FMDP-1DBB SUNFLO 

LIQUID: 96% regenerated sulphuric acid 

Q (m 3 /h): 1 





R.P.M.: 1,450 

POWER: 3.6 CV 

MATERIALS: DUCTILE IRON 

No. UNITS: 2 

B-6303 Schott 2nd Stage Sulphuric Recirculation Pump 6300 – Sulphuric Acid Regeneration 

ITEM: B-6303 

NAME: SCHOTT PLANT 2ND STAGE SULPHURIC ACID 

RECIRCULATION PUMP 

MAKE: RHEINHUETTE 

MODEL: RCE 40/200 D2 

LIQUID: 96 % Sulphuric Acid 

Q (m 3 /h): 6.4 

Discharge pressure: (bar): 5 

Suction pressure (kg/cm2 r): 

Differential pressure (kg/cm2): 


R.P.M.: 1,450 

POWER: 2.2 kW 

MATERIALS: SILICON CAST IRON 

No. UNITS: 1

B-6304 Nitric Acid Dosing Pump 6300 – Sulphuric Acid Regeneration 

ITEM: B-6304 

NAME: H2SO4 REGENERATION EFFLUENT NITRIC ACID 

DOSAGE PUMP 

MAKE: 

MODEL: DOPU 40/EX/Y 

LIQUID: 65 % nitric acid 

Q (m 3 /h): 0.04 

Discharge pressure: (bar): 3.5 

Suction pressure (kg/cm2 g): 



R.P.M.: 2,900 


MATERIALS: GLASS / PTFE 

No. UNITS: 1 

B-6305 Schott Thermal Oil Pump 6300 – Sulphuric Acid Regeneration 

ITEM: B-6305 

NAME: SCHOTT PLANT THERMAL OIL RECIRCULATION 

PUMP 

MAKE: 

MODEL: NTT 32-160 

LIQUID: Thermal Oil 

Q (m 3 /h): 12 

Discharge pressure: (bar): 25 

Suction pressure (kg/cm2 g): 



R.P.M.: 2,900 

POWER: 2.2 kW 

MATERIALS: CAST IRON: GGG 40 

No. UNITS: 1

B-6503 -1/S Chemical Drainage Discharge Pump 6500 – Chemical Drainage Treatment 

ITEM: B-6503-1/S NAME: CHEMICAL DRAINAGE EVACUATION PUMP 

MAKE: CASALS S CARDONA 

MODEL: BTSLL 416 

LIQUID: contaminated water 

Q (m 3 /h): 14 





R.P.M.: 1,450 

POWER: 2.2 kW 

MATERIALS: PVDF 

No. UNITS: 2

3.- COLUMNS 

C-1101 Water Washer 1100 – Hydrochlorination 

ITEM: C-1101 

NAME: WATER WASHER COLUMN 

MANUFACTURER: LE CARBONE 

LORRAINE 

MATERIALS: 

- Ferrule and floors: 

- Receptacle support: 

LIQUID: 




CAPACITY: 

TOTAL HEIGHT: 7,330 mm 

No. UNITS: 1 

C-1102 Soda Washer 1100 – Hydrochlorination 

ITEM: C-1102 

NAME: CAUSTIC SODA WASHER COLUMN 

MANUFACTURER: 

MATERIALS: 

- Ferrule and floors: ASTM A-516 Gr.60 

- Receptacle support: ASTM A-283 Gr.C 

LIQUID: DILUTED CAUSTIC SODA 

CALCULATION TEMPERATURE: 60º C 

CALCULATION PRESSURE: 3 Kg/cm2 g 

TOP PART: 

- Service temperature: 15º C 

- Service pressure: 1.10 kg/cm2g 

BOTTOM PART: 

- Service temperature: 40 / 15º C 

- Service pressure: 1.12 kg/cm2 


CAPACITY: 3 m 3 


No. UNITS: 1

C-1103 1st Drying Column 1100 – Hydrochlorination 

EM : C-1103 NAME: 1st DRYING COLUMN 

MANUFACTURER: 

MATERIALS: 



LIQUID: VARIOUS 



TOP PART: 



BOTTOM PART: 

- Service temperature: 40º C. 





No. UNITS: 1 

C-1104 2nd Drying Column 1100 – Hydrochlorination 

ITEM: C-1104 NAME: 2nd DRYING COLUMN 

MANUFACTURER: 

MATERIALS: 






TOP PART: 



BOTTOM PART: 






No. UNITS: 1

C-1105 3rd Drying Column 1100 – Hydrochlorination 

ITEM: C-1105 NAME: 3rd DRYING COLUMN 

MANUFACTURER: 

MATERIALS: 

- Ferrule and floors: ASTM A-240 Tp.340L 





TOP PART: 



BOTTOM PART: 






No. UNITS: 1 

C-1106 HCl Absorption Column 1100 – Hydrochlorination 

ITEM: C-1106 

NAME: HCl ABSORPTION COLUMN 

MANUFACTURER: LE CARBONE LORRAINE 

MATERIALS: 



LIQUID: 

TEMPERATURE: 130º C 

PRESSURE: 5 bar 




No. UNITS: 1

C-1201 HCl Distillation Column 1200 – Chlorination 

ITEM: C-1201 

NAME: HCl DISTILLATION COLUMN 

MANUFACTURER: 

MATERIALS: 



LIQUID: HCl and CHLOROMETHANES 

CALCULATION TEMPERATURE: - 30º C / + 130º C 

CALCULATION PRESSURE: 15 kg/cm2 g 

TOP PART: 

- Service temperature: - 25º C 

- Service pressure: 12 kg/cm2 

BOTTOM PART: 

- Service temperature: + 107º C 





No. UNITS: 1 

C-1202 Methyl Chloride Column 1200 – Chlorination 

ITEM: C-1202 

NAME: METHYL CHLORIDE COLUMN 

MANUFACTURER: 

MATERIALS: 

- Ferrule and floors: ASTM A-240 Tp340L 

ASTM A-516 Gr.60 

- Receptacle support: - 

LIQUID: CHLOROMETHANES 



TOP PART: 



BOTTOM PART: 






No. UNITS: 1

C-1203 Methylene Chloride Column 1200 – Chlorination 

ITEM: C-1203 

NAME: METHYLENE CHLORIDE COLUMN 

MANUFACTURER: 

MATERIALS: 







TOP PART: 



BOTTOM PART: 






No. UNITS: 1

C-1204 Chloroform Column 1200 – Chlorination 

ITEM: C-1204 

NAME: CHLOROFORM COLUMN 

MANUFACTURER: 

MATERIALS: 







TOP PART: 



BOTTOM PART: 






No. UNITS: 1 

C-6101 Methanol Recovery Column 6100 – Organic Hydrochloric Acid 

ITEM: C-6101 

NAME: METHANOL RECOVERY COLUMN 

MANUFACTURER: 

MATERIALS: 











No. UNITS: 1

C-6102 Methanol Distillation Column 6100 – Organic Hydrochloric Acid 

ITEM: C-6102 

NAME: METHANOL RECOVERY COLUMN 

MANUFACTURER: SCHWARTZ - HAUTMONT 

MATERIALS: 






SERVICE PRESSURE: atmospheric 





No. UNITS: 1 

C-6301 1st Stage Sulphuric Desorption Column 6300 – Sulphuric Regeneration and Recovery MEOH 

ITEM: C-6301 

NAME: EFFLUENT DESORPTION COLUMN 

MANUFACTURER: SCHOTT ENGINEERING 

TYPE: PACKED COLUMN 

MATERIALS: 

- Ferrule and floors: GLASS 

- Seals PTFE 

LIQUID: WSA liquid (bottom) 

Vapour gas (top) 

DESIGN 

- Temperature: 150º C 

- Pressure: -1 bar 

BOTTOM: 

- Temperature: 80º C. 

- Pressure: 0.08 bar 

TOP: 

- Temperature: 75º C. 


INTERNAL: Raschig Rings 15 x 15 

COLUMN HEIGHT: 2,300 mm 

Diameter: 200 mm 

Volume: 0.08 m 3 

No. UNITS: 1

C-6302 Desorption Column R-1 6300 – Sulphuric Acid Regeneration 

ITEM: C-6302 

NAME: EFFLUENT DESORPTION COLUMN 


TYPE: PACKED COLUMN 

MATERIALS: 

- Ferrule and floors: GLASS 

- Seals PTFE 

LIQUID: H2SO4 liquid (bottom) 

Vapour gas (top) 

DESIGN 


- Pressure: -1 bar 

BOTTOM: 



TOP: 



INTERNAL: Raschig Rings 15 x 15 

COLUMN HEIGHT: 3,300 mm 

Diameter: 200 mm 

Volume: 0.09 m 3 

No. UNITS: 1 

C-6601 Desorption Stripping Column 6600 – Moist Solvents 

ITEM: C-6601 

NAME: DESORPTION STRIPPING COLUMN 

MANUFACTURER: LE CARBONE LORRAINE 

MATERIALS: 



LIQUID: 


PRESSURE: 6 bar 




No. UNITS: 1

4.- TANKS 

D-1101 Methyl Chloride Receiver 1100 – Hydrochlorination 

ITEM: D-1101 

NAME: METHYL CHLORIDE RECEIVER TANK 

LIQUID: METHYL CHLORIDE 

MATERIALS: 

- Ferrule and floors: A-240 Tp.304L 

- Receptacle support: A7 

TEMPERATURE: 



PRESSURE: 



SIZE: 





No. UNITS: 1

D-1102 Methanol Drainage Tank 1100 – Hydrochlorination 

ITEM: D-1102 NAME: METHANOL DRAINAGE TANK 

LIQUID: METHANOL 

MATERIALS: 

- Ferrule and floors: AISI 304L 

- Receptacle support: Carbon steel 

TEMPERATURE: 

- Service: 95º C 

- Calculation: 120º C 

PRESSURE: 



SIZE: 


- Diameter: 18 inches 



No. UNITS: 1 

D-1201 Methyl Chloride Supply Tank 1200 – Chlorination 

ITEM: D-1201 

NAME: METHYL CHLORIDE SUPPLY TANK 


MATERIALS: 

- Ferrule and floors: A-240 Tp. 304L 


TEMPERATURE: 



PRESSURE: 



SIZE: 





No. UNITS: 1

D-1202 Methyl Chloride Decanting Tank 1200 – Chlorination 

ITEM: D-1202 

NAME: METHYL CHLORIDE DECANTING TANK 


MATERIALS: 



TEMPERATURE: 



PRESSURE: 



SIZE: 





No. UNITS: 1 

D-1203 Methylene Chloride Recycling Tank 1200 – Chlorination 

ITEM: D-1203 

NAME: METHYL CHLORIDE RECYCLING TANK 


MATERIALS: 



TEMPERATURE: 

- Service: 40º C. 


PRESSURE: 



SIZE: 





No. UNITS: 1

D-1204 Chlorine Supply Tank 1200 – Chlorination 

ITEM: D-1204 

NAME: CHLORINE SUPPLY TANK 

LIQUID: CHLORINE 

MATERIALS: 


- Receptacle support: A-240 Tp. 304L / 

/ A-283 Gr.C 

TEMPERATURE: 



PRESSURE: 



SIZE: 





No. UNITS: 1 

D-1205 HCl Distillation Reflow Ball 1200 – Chlorination 

ITEM: D-1205 

NAME: HCL DISTILLATION REFLOW BALL TANK 

LIQUID: HYDROGEN CHLORIDE 

MATERIALS: 


- Receptacle support: A-283 Gr.C 

TEMPERATURE: 



PRESSURE: 



SIZE: 





No. UNITS: 1

D-1206 Methyl Chloride Reflow Ball 1200 – Chlorination 

ITEM: D-1206 

NAME: METHYL CHLORIDE REFLOW BALL 


MATERIALS: 



TEMPERATURE: 



PRESSURE: 



SIZE: 





No. UNITS: 1 

D-1207-1/S Methyl Chloride Drying Drum 1200 – Chlorination 

ITEM: D-1207 1/S 

NAME: METHYL CHLORIDE DRYING DRUM TANK 


MATERIALS: 



/ A-283 Gr.C 

TEMPERATURE: 



PRESSURE: 



SIZE: 





No. UNITS: 2

D-1208 Crude Ball 1200 – Chlorination 

ITEM: D-1208 

NAME: CRUDE BALL TANK 

LIQUID: CRUDE 

MATERIALS: 

- Ferrule and floors: A-515 Gr.60 


TEMPERATURE: 



PRESSURE: 

- Service: atmospheric 


SIZE: 





No. UNITS: 1 

D-1209-1/S Crude Neutralisation Drum 1200 - Chlorination 

ITEM: D-1209-1/s 

NAME: CRUDE NEUTRALISATION DRUM TANK 

LIQUID: CRUDES 

MATERIALS: 



TEMPERATURE: 



PRESSURE: 



SIZE: 





No. UNITS: 2

D-1210 Methylene Chloride Reflow Ball 1200 – Chlorination 

ITEM: D-1210 

NAME: METHYLENE CHLORIDE REFLOW BALL 

TANK 

LIQUID: METHYLENE CHLORIDE 

MATERIALS: 



TEMPERATURE: 



PRESSURE: 



SIZE: 





No. UNITS: 1 

D-1211-1/S 

ITEM: D-1211 1/S 

Methylene Chloride Neutralisation Drum 1200 – Chlorination 

NAME: METHYLENE CHLORIDE NEUTRALISATION 

DRUM TANK 


MATERIALS: 



/ A-283 Gr.C 

TEMPERATURE: 



PRESSURE: 



SIZE: 





No. UNITS: 2

D-1212 Chloroform Reflow Ball 1200 – Chlorination 

ITEM: D-1212 

NAME: CHLOROFORM REFLOW BALL TANK 

LIQUID: CHLOROFORM 

MATERIALS: 



TEMPERATURE: 



PRESSURE: 



SIZE: 





No. UNITS: 1 

D-1213-1/S Chloroform Neutralisation Drum 1200 – Chlorination 

ITEM: D-1213 1/S 

NAME: CHLOROFORM NEUTRALISATION DRUM 

TANK 


MATERIALS: 



/ A-283 Gr.C 

TEMPERATURE: 



PRESSURE: 



SIZE: 





No. UNITS: 2

D-1214 Solvent Recovery Tank 1200 – Chlorination 

ITEM: D-1214 

NAME: SOLVENT RECOVERY TANK 

LIQUID: SOLVENT MIXTURE 

MATERIALS: 

- Ferrule and floors: AISI 316 L 

- Receptacle support: AISI 316 / A-42.b 

TEMPERATURE: 


- Design: 100º C 

PRESSURE: 

- Service: 4 bar 

- Design: 6 bar 

SIZE: 





No. UNITS: 1 

D-2101-S Demineralised Water Tank 2100 – Cooling Water 

ITEM: D-2101 1/S NAME: DEMINERALISED WATER TANK 

SUPPLIER: CIDA 


MATERIALS: 

- Ferrule and floors: A-42.b 

- Receptacle support: A-42.b 

TEMPERATURE: 


PRESSURE: 

- Design: 4 kg/cm2 g 

SIZE: 




No. UNITS: 2

D-2102-S Demineralised Water Tank 2100 – Cooling Water 

ITEM: D-2102 1/S NAME: DEMINERALISED WATER TANK 

SUPPLIER: CIDA 


MATERIALS: 

- Ferrule and floors: A-42.b 

- Receptacle support: A-42.b 

TEMPERATURE: 


PRESSURE: 


SIZE: 




No. UNITS: 2 

D-2401 Ethylene Glycol Tank (+8º C) 2400 - MEG Cold Cooling Circuit (+8ºC) 

ITEM: D-2401 

NAME: MEG +18 ºC COLD RECOVERY CIRCUIT 

SERVICES ETHYLENE GLYCOL TANK 

LIQUID: MIXED ETHYLENE GLYCOL 

MATERIALS: 

- Ferrule and floors: A-283 Gr.C 


TEMPERATURE: 



PRESSURE: 



SIZE: 





No. UNITS: 1

D-2501 Thermal Oil Tank 2500- Thermal Oil Circuit 

ITEM: D-2501 

NAME: THERMAL OIL TANK 

LIQUID: THERMAL LIQUID 

MATERIALS: 

- Ferrule and floors: A-515 Gr.60 

- Receptacle support: A-283-Gr.C 

TEMPERATURE: 



PRESSURE: 



SIZE: 





No. UNITS: 1 

D-2901 Demineralised Water Tank 2900 – Chlorinator Cooling Circuit 

ITEM: D-2901 

NAME: CHLORINATOR COOLING WATER TANK 


MATERIALS: 

- Ferrule and floors: A283 Gr.C 


TEMPERATURE: 



PRESSURE: 



SIZE: 





No. UNITS: 1

D-2902 Cooling Water Tank 2900 – Chlorinator Cooling Circuit 

ITEM: D-2902 

NAME: CHLORINATOR COOLING WATER TANK 


MATERIALS: 



TEMPERATURE: 



PRESSURE: 



SIZE: 





No. UNITS: 1 

D-3220-1/2 

DCL 

ITEM: D-3220-1/2 

NAME: CICLON DEHYDRATOR TANK 


MATERIALS: 

- Ferrule and floors: PVDF + Fr 


TEMPERATURE: 

- Service: 

- Calculation: 

PRESSURE: 

- Service: 


SIZE: 



CAPACITY: 


No. UNITS: 2

D-3223 DCL 

ITEM: D-3223 

NAME: LIQUID / GAS CHLORINE VERTICAL TANK 

BODY 

LIQUID: Liquid chlorine / gas 

MATERIALS: 

- Ferrule and floors: A-333 Gr.6 / A-516 Gr.60 

TEMPERATURE: 

- Service: 

- Design: 80 / -50º C 

PRESSURE: 

- Service: 


SIZE: 





No. UNITS: 1 

COIL 

LIQUID: steam 

MATERIALS: 

- Tubes: A-106 Gr.B 

TEMPERATURE: 


PRESSURE: 


D-5201 Regenerated Sulphuric Tank 5200 - Sulphuric Acid 

ITEM: D-5201 

NAME: REGENERATED SULPHURIC TANK 

LIQUID: sulphuric acid 

MATERIALS: 

- Ferrule and floors: stainless steel 

- Receptacle support: St 37.2 

TEMPERATURE: 

- Service: 


PRESSURE: 

- Service: 


SIZE: 



CAPACITY: 


No. UNITS: 1

D-6101 Methanol Recovery Column Reflow Ball 6100 – Organic Hydrochloric Acid 

ITEM: D-6101 

NAME: REFLOW BALL TANK 

LIQUID: Various 

MATERIALS: 



TEMPERATURE: 



PRESSURE: 



SIZE: 


- Diameter: 16” 



No. UNITS: 1 

D-6102 Methanol Distillation Column Reflow Ball 6100 – Organic Hydrochloric Acid 

ITEM: D-6102 

NAME: REFLOW BALL TANK 

LIQUID: Methyl chloride + methanol 

MATERIALS: 



TEMPERATURE: 



PRESSURE: 



SIZE: 





No. UNITS: 1

D-6201 Vent Receiver Lung 6200 – Gas Effluent Treatment 

ITEM: D-6201 

NAME: DG-1 VENT BALL TANK 

LIQUID: Various gases 

MATERIALS: 



TEMPERATURE: 



PRESSURE: 

- Service: Partial vacuum 

- Calculation: Complete vacuum 

SIZE: 





No. UNITS: 1 

D-6301 Sulphuric Acid Tank 6300 – Sulphuric Acid Regeneration 

ITEM: D-6301 

NAME: SHOTT PROCESS COLLECTION TANK 

SUPPLIER: SCHOTT ENGINEERING 


MATERIALS: 

- Ferrule and floors: Glass 

- Seals PTFE 

- Receptacle support: Stc 

TEMPERATURE: 



PRESSURE: 

- Service (abs): 1 bar 

- Design: 

SIZE: 


- Diameter: DN 600 



No. UNITS: 1

D-6303 Distilled Receiver Tank 6300 – Sulphuric Acid 

Regeneration 

ITEM: D-6303 

NAME: DISTILLED RECEIVER TANK 



MATERIALS: 


- Seals PTFE 


TEMPERATURE: 



PRESSURE: 

- Service (abs): 0.02 bar 

- Design: 

SIZE: 



CAPACITY: 


No. UNITS: 1 

D-6304 Distilled Tank 6300 – Sulphuric Acid Regeneration 

ITEM: D-6304 

NAME: NITRIC ACID TANK 


LIQUID: Nitric acid 

MATERIALS: 


- Seals PTFE 


TEMPERATURE: 



PRESSURE: 

- Service (bar): 1 bar 

SIZE: 

- Height: 900 mm 




No. UNITS: 1

D-6305 Flash Tank 6300 – Sulphuric Acid Regeneration 

ITEM: D-6305 

NAME: H2S04 REGENERATION TANK 



MATERIALS: 

- Ferrule and floors: Glass lined steel 

- Seals PTFE 


TEMPERATURE: 



PRESSURE: 

- Service (bar): 0.02 bar 

- Admissible service: -113 bar 

SIZE: 





No. UNITS: 1 

D-6306 Vacuum Pump Supply Tank 6300 – Sulphuric Acid Regeneration 

ITEM: D-6306 

NAME: H2SO4 REGENERATION TANK 



MATERIALS: 

- Ferrule and floors: Glass lined steel 

- Seals PTFE 


TEMPERATURE: 



PRESSURE: 


- Admissible service: -1 / 3 bar 

SIZE: 





No. UNITS: 1

D-6307 Separator 6300 – Sulphuric Acid Regeneration 

ITEM: D-6307 




MATERIALS: 


- Seals: PTFE 


TEMPERATURE: 



PRESSURE: 


- Admissible service: -1 bar 

SIZE: 





No. UNITS: 1 

D-6308 Nitric Acid Storage 6300 – Sulphuric Acid Regeneration 

ITEM: D-6308 



LIQUID: 50 % nitric acid 

MATERIALS: 


- Seals PTFE 


TEMPERATURE: 



PRESSURE: 

- Service (bar): 1 bar 

- Design: 

SIZE: 





No. UNITS: 1

D-7103 Foam Tank Fire-fighting System 

ITEM: D-7103 

NAME: FIRE-EXTINGUISHING FOAM TANK 

TYPE: Diaphragm tank with supplier 

LIQUID: Foam 

MATERIALS: 

- Ferrule and floors: Stc 


TEMPERATURE: 

- Service: 


PRESSURE: 


SIZE: 



CAPACITY: 600 litres 


No. UNITS: 1 

5.- EXCHANGERS 

I-1101 Methanol Vaporiser 1100 – Hydrochlorination 

ITEM: I-1101 NAME: METHANOL VAPORISER 

MANUFACTURER: AGUILAR Y SALAS 

TYPE: Methanol vaporiser 


BODY SIDE: 

LIQUID: Steam 



BODY MATERIAL: A-285 Gr.C 

TUBE SIDE: 




MATERIAL: A-213 Tp 304L 

SIZE: 


DIAMETER: 992 mm / 1.200 mm 


No. UNITS: 1

I-1102 Methanol Reheater 1100 – Hydrochlorination 

ITEM: I-1102 

NAME: METHANOL REHEATER 

MANUFACTURER: 

TYPE: Methanol reheater 


BODY SIDE: 

LIQUID: 



BODY MATERIAL: 

TUBE SIDE: 

LIQUID: 



MATERIAL: 

SIZE: 


DIAMETER: 12” / 324 mm 


No. UNITS: 1 

I-1103 Hydrogen Chloride Reheater 1100 – Hydrochlorination 

ITEM: I-1103 

NAME: HYDROGEN CHLORIDE REHEATER 

MANUFACTURER: 

TYPE: Hydrogen chloride reheater 


BODY SIDE: 

LIQUID: 




TUBE SIDE: 

LIQUID: 



MATERIAL: 

SIZE: 


DIAMETER: 323 mm / 436 mm 


No. UNITS: 1

I-1104 Hydrochlorination Gas Cooler 1100 – Hydrochlorination 

ITEM: I-1104 NAME: GAS COOLER 

MANUFACTURER: SIGRI GmbH 

TYPE: Gas cooler 

EXCHANGE SURFACE: 56.4 m 2 

BODY SIDE: 

LIQUID: 




TUBE SIDE: 

LIQUID: 




TUBE LENGTH: 6,100 mm 

MATERIAL: Diabon graphite NS2 

SEALS: PTFE 

SIZE: 




No. UNITS: 1 

I-1105 Soda Washer Cooler 1100 – Hydrochlorination 

ITEM: I-1105 

NAME: SODA WASHER COOLER 

MANUFACTURER: VICARB 

TYPE: PLATES (soda washer cooler) 


PLATE MATERIAL AISI304 

SEALS: Nitrile 

PROCESS SIDE: 

LIQUID: NaOH (waste) 





TUBE SIDE: 

LIQUID: Glycol 40 % 





SIZE: 840 x 280 x 116 mm 


No. UNITS: 1

I-1106 1st Drying Column Cooler 1100 – Hydrochlorination 

ITEM: I-1106 

NAME: FIRST DRYING COLUMN COOLER 


TYPE: PLATES (first drying column cooler) 1.76 m 2 

PLATE MATERIAL: HASTELLOY B 

SEALS: Viton E 

PROCESS SIDE: 

LIQUID: H2SO4 (waste) 


SERVICE TEMPERATURE: 40 → 37.5º C 



TUBE SIDE: 

LIQUID: Water 





SIZE: 585 x 150 x 168 mm 


No. UNITS: 1 

I-1107 2nd Drying Column Cooler 1100 – Hydrochlorination 

ITEM: I-1107 

NAME: SECOND DRYING COLUMN COOLER 


TYPE: PLATES (second drying column cooler) EXCHANGE 

SURFACE: 1.85 m 2 

PLATE MATERIAL: AISI 316 Ti 


PROCESS SIDE: 






TUBE SIDE: 

LIQUID: Water 





SIZE: 585 x 150 x 168 mm 


No. UNITS: 1

I-1108 3rd Drying Column Cooler 1100 – Hydrochlorination 

ITEM: I-1108 

NAME: THIRD DRYING COLUMN COOLER 


TYPE: PLATES (third drying column cooler) 

SURFACE: 2.02 m 2 

PLATE MATERIAL: AISI 316 Ti 


PROCESS SIDE: 






TUBE SIDE: 

LIQUID: Water 





SIZE: 585 x 150 x 171 mm 


No. UNITS: 1 

EXCHANGE 

I-1109 Methyl Chloride Pre-cooler 1100 – Hydrochlorination 

ITEM: I-1109 

NAME: METHYL CHLORIDE PRE-COOLER 

MANUFACTURER: 

TYPE: Methyl chloride pre-cooler 


BODY SIDE: 

LIQUID: 




TUBE SIDE: 

LIQUID: 



MATERIAL: 

SIZE: 


DIAMETER: 508 mm / 620 mm 


No. UNITS: 1

I-1110 Methyl Chloride Condenser 1100 – Hydrochlorination 

ITEM: I-1110 

NAME: METHYL CHLORIDE CONDENSER 


TYPE: R-22 evaporator / Methyl chloride condenser 


BODY SIDE: 

LIQUID: R-22 

DESIGN PRESSURE: 10.5 kg/cm2 abs 



BODY MATERIAL: A-516-60 

TUBE SIDE: 

LIQUID: Methyl chloride 




MATERIAL: A-240 Tp.304L / A-213 

Tp.316L 


SIZE: 




No. UNITS: 1 

I-1111 Methyl Chloride Heater 1100 – Hydrochlorination 

ITEM: I-1111 

NAME: METHYL CHLORIDE HEATER 

MANUFACTURER: BROWN FINTUBE FRANCE 

TYPE: Methyl chloride heater 


BODY SIDE: 

LIQUID: 



BODY MATERIAL: A-312 to 304 L 

TUBE SIDE: 

LIQUID: 



MATERIAL: A-312 Tp. 304 L 

No. TUBES: 

SIZE: 




No. UNITS: 1

I-1112 Methanol Drainage Cooler 1100 – Hydrochlorination 

ITEM: I-1112 

NAME: METHANOL DRAINAGE COOLER 

MANUFACTURER: 

TYPE: Methanol drainage cooler 


BODY SIDE: 

LIQUID: Water 


DESIGN PRESSURE: atmospheric 



BODY MATERIAL: A-53 Gr.B 

TUBE SIDE: 






MATERIAL: A-312 Tp.304L 

No. TUBES: 1 

SIZE: 

LENGTH: 610 mm 



No. UNITS: 1 

I-1201 Methylene Chloride Gas Condenser 1200 – Chlorination 

ITEM: I-1201 

NAME: METHYLENE CHLORIDE GAS CONDENSER 


TYPE: Condenser 


BODY SIDE: 


SERVICE PRESSURE: 


SERVICE TEMPERATURE: 


BODY MATERIAL: A-312 Tp.304L 

TUBE SIDE: 

LIQUID: 40% MEG 






No. TUBES: 

SIZE: 3,588 x 428 x 197 


No. UNITS: 1

I-1202 Chlorine Vaporiser 1200 – Chlorination 

ITEM: I-1202 

NAME: CHLORINE VAPORISER 

MANUFACTURER: CHEMTEC, B.V. 

TYPE: Chlorine vaporiser 


BODY SIDE: 

LIQUID: 


DESIGN PRESSURE: 32 kg/cm2 g 



BODY MATERIAL: SA-240 Type 316L 

TUBE SIDE: 

LIQUID: 





MATERIAL: SB-163 ALLOY 400 

No. TUBES: 

SIZE: 




No. UNITS: 1 

I-1203 Partial Chlorinator Condenser 1200 – Chlorination 

ITEM: I-1203 

NAME: PARTIAL CHLORINATOR CONDENSER 

MANUFACTURER: 



BODY SIDE: 

LIQUID: 






TUBE SIDE: 

LIQUID: 





MATERIAL: 

No. TUBES: 

SIZE: 




No. UNITS: 1

I-1204 HCl Distillation Column 1200 – Chlorination 

ITEM: I-1204 

NAME: HCL DISTILLATION RE-BOILER 

MANUFACTURER: 

TYPE: HCl Distillation re-boiler 


BODY SIDE: 

LIQUID: 






TUBE SIDE: 

LIQUID: 





MATERIAL: 

No. TUBES: 

SIZE: 




No. UNITS: 1 

I-1205-A Oil Recoverer 1200 – Chlorination 

ITEM: I-1205 A 

NAME: OIL RECOVERER EXCHANGER 




BODY SIDE: 

LIQUID: R-22 



SERVICE TEMPERATURE: +38º C 

DESIGN TEMPERATURE: +80º C 

BODY MATERIAL: St.35 

TUBE SIDE: 

LIQUID: R-22 + OIL 





MATERIAL: St.35 

No. TUBES: 

SIZE: 




No. UNITS: 1

I-1206 Methyl Chloride Column Re-boiler 1200 – Chlorination 

ITEM: I-1206 

NAME: METHYL CHLORIDE COLUMN RE-BOILER 

MANUFACTURER: 

TYPE: Re-boiler 


BODY SIDE: 

LIQUID: 






TUBE SIDE: 

LIQUID: 





MATERIAL: 

No. TUBES: 

SIZE: 




No. UNITS: 1 

I-1207-A/B Methyl Chloride Column Condenser 1200 – Chlorination 

ITEM: I-1207 

A/B 

NAME: METHYL CHLORIDE COLUMN CONDENSER 

MANUFACTURER: 



BODY SIDE: 

LIQUID: 






TUBE SIDE: 

LIQUID: 





MATERIAL: AISI 304 L 


SIZE: 




No. UNITS: 2

I-1208 Crude Thermal Recoverer 1200 – Chlorination 

ITEM: I-1208 

NAME: CRUDE THERMAL RECOVERER 

MANUFACTURER: 

TYPE: Thermal recoverer 


BODY SIDE: 

LIQUID: 






TUBE SIDE: 

LIQUID: 





MATERIAL: 

No. TUBES: 

SIZE: 




No. UNITS: 1 

I-1209 Crude Cooler 1200 – Chlorination 

ITEM: I-1209 

NAME: CRUDE COOLER 

MANUFACTURER: 

TYPE: Thermal recoverer 


BODY SIDE: 

LIQUID: 






TUBE SIDE: 

LIQUID: 





MATERIAL: 

No. TUBES: 

SIZE: 




No. UNITS: 1

I-1210 Crude Gas Condenser 1200 – Chlorination 

ITEM: I-1210 

NAME: CRUDE GAS CONDENSER 




BODY SIDE: 

LIQUID: N2+CH2Cl2+CHCl3+CCl4 






TUBE SIDE: 







No. TUBES: 

SIZE: 3,588 x 428 x 197 


No. UNITS: 1 

I-1211 Methylene Chloride Column Re-boiler 1200 – Chlorination 

ITEM: I-1211 

NAME: METHYLENE CHLORIDE COLUMN RE- 

BOILER 

MANUFACTURER: 



BODY SIDE: 

LIQUID: 






TUBE SIDE: 

LIQUID: 





MATERIAL: 

No. TUBES: 

SIZE: 


DIAMETER: 1,130 / 1,254 mm 


No. UNITS: 1

I-1212 Methylene Chloride Column Condenser 1200 – Chlorination 

ITEM: I-1212 

NAME: METHYLENE CHLORIDE COLUMN 

CONDENSER 

MANUFACTURER: 



BODY SIDE: 

LIQUID: 






TUBE SIDE: 

LIQUID: 





MATERIAL: 

No. TUBES: 

SIZE: 




No. UNITS: 1 

I-1213 Methylene Chloride Column Gas Condenser 1200 – Chlorination 

ITEM: I-1213 

NAME: METHYLENE CHLORIDE COLUMN GAS 

CONDENSER 




BODY SIDE: 







TUBE SIDE: 







No. TUBES: 

SIZE: 3,588 x 428 x 197 


No. UNITS: 1

I-1214 Methylene Chloride Recycling Cooler 1200 – Chlorination 

ITEM: I-1214 

NAME: METHYLENE CHLORIDE RECYCLING COOLER 


TYPE: Cooler 


BODY SIDE: 

LIQUID: Water 






TUBE SIDE: 







No. TUBES: 

SIZE: 3,588 x 1,288 mm 


No. UNITS: 1 

I-1215 Methylene Chloride Production Cooler 1200 – Chlorination 

ITEM: I-1215 

NAME: METHYLENE CHLORIDE PRODUCTION 

COOLER 


TYPE: Cooler 


BODY SIDE: 







TUBE SIDE: 

LIQUID: Water 






No. TUBES: 

SIZE: 3,588 x 1,718 mm 


No. UNITS: 1

I-1216 Chloroform Column Re-boiler 1200 – Chlorination 

ITEM: I-1216 

NAME: CHLOROFORM COLUMN RE-BOILER 

MANUFACTURER: 



BODY SIDE: 

LIQUID: 






TUBE SIDE: 

LIQUID: 





MATERIAL: 

No. TUBES: 

SIZE: 


DIAMETER: 1,254 / 1,378 mm 


No. UNITS: 1 

I-1217 Chloroform Column Condenser 1200 – Chlorination 

ITEM: I-1217 

NAME: CHLOROFORM COLUMN CONDENSER 

MANUFACTURER: 



BODY SIDE: 

LIQUID: 






TUBE SIDE: 

LIQUID: 





MATERIAL: 

No. TUBES: 

SIZE: 




No. UNITS: 1

I-1218 Chloroform Column Gas Condenser 1200 – Chlorination 

ITEM: I-1218 

NAME: CHLOROFORM COLUMN GAS CONDENSER 




BODY SIDE: 

LIQUID: CHCl3 + N2 






TUBE SIDE: 







No. TUBES: 

SIZE: 3,588 x 428 x 197 mm 


No. UNITS: 1 

I-1219 Chloroform Cooler 1200 – Chlorination 

ITEM: I-1219 

NAME: CHLOROFORM COOLER 


TYPE: Cooler 


BODY SIDE: 

LIQUID: Chloroform 






TUBE SIDE: 

LIQUID: Water 




DESIGN 



No. TUBES: 

SIZE: 3,588 x 1,718 mm 


No. UNITS: 1

I-1220 Methylene Chloride Tank Gas Condenser 1200 – Chlorination 

ITEM: I-1220 





BODY SIDE: 

LIQUID: N2 + CH2Cl2 






TUBE SIDE: 





DESIGN 

TEMPERATURE: -20º C 


No. TUBES: 

SIZE: 3,588 x 858 mm 


No. UNITS: 1 

I-1221 Chloroform Tank Gas Condenser 1200 – Chlorination 

ITEM: I-1221 

NAME: CHLOROFORM TANK GAS CONDENSER 




BODY SIDE: 

LIQUID: CHCl3 






TUBE SIDE: 





DESIGN 



No. TUBES: 

SIZE: 3,588 x 858 mm 


No. UNITS: 1

I-1222 Tetrachloride Cooler 1200 – Chlorination 

ITEM: I-1222 

NAME: TETRACHLORIDE COOLER 


TYPE: Carbon tetrachloride cooler 


BODY SIDE: 

LIQUID: Carbon tetrachloride 




TUBE SIDE: 

LIQUID: Cooling water 



MATERIAL: A-285 Gr.C 

No. TUBES: 24 

SIZE: 




No. UNITS: 1 

I-1223 Chlorinator Demineralised Water Heater 1200 – Chlorination 

ITEM: I-1223 

NAME: CHLORINATOR DEMINERALISED WATER 

HEATER 

INPUT WATER: 

- Flow: 48.1 m3/h. 


- Pressure: 2.9 kg/cm2 g 

INPUT STEAM: 

- Normal flow: 470 kg/h 

- Maximum flow: 590 kg/h 


- Pressure: 2.9 kg/cm2 g 

DESIGN CONDITIONS: 

- Design pressure: 4 kg/cm2 

- Design temperature: 160º C 

- Insulation: 80 mm fibreglass 

MATERIALS: 

- Body: A-106 Gr. B / A-285 Gr. C 

- Deflectors: A-285 Gr. C / A-240 Tp. 304 

- Seals: Compressed asbestos

I-1224 Methyl Chloride Cooler 1200 – Chlorination 

ITEM: I-1224 

NAME: METHYL CHLORIDE COOLER 


TYPE: Carbon tetrachloride cooler 


BODY SIDE: 





TUBE SIDE: 

LIQUID: Methyl chloride 



MATERIAL: A-213 Tp. 304 L 

No. TUBES: 46 

SIZE: 




No. UNITS: 1 

I-2201 Condensed Flash Condenser 2200 – Steam – Condensed Products 

ITEM: I-2201 NAME: CONDENSED FLASH CONDENSER 


TYPE: Condensador 


BODY SIDE: 

LIQUID: Water vapour 




TUBE SIDE: 




MATERIAL: A -179 

No. TUBES: 33 

SIZE: 




No. UNITS: 1

I-2501 Thermal Oil Pumps 2500- Thermal Oil Circuit 

ITEM: I-2501 

NAME: THERMAL OIL COOLER 


TYPE: Cooler 


BODY SIDE: 

LIQUID: Water 






TUBE SIDE: 

LIQUID: Marlotherm 




DESIGN 


MATERIAL: A-106 Gr.B 

No. TUBES: 

SIZE: 2,149 x 486 mm 


No. UNITS: 1 

I-2704 Oil Recoverer 2700 - R-22 Cooling System (-40ºC) 

ITEM: I-2704 NAME: R-22 COOLING SYSTEM OIL RECOVERER 




BODY SIDE: 

LIQUID: R-22 





BODY MATERIAL: St -25 

TUBE SIDE: 

LIQUID: R-22 + oil 






SIZE: 




No. UNITS: 1

I-2901 Chlorinator Cooling Water Cooler 2900 – Cooling Circuit 

ITEM: I-2901 

NAME: COOLING WATER COOLER DEMINERALISED 

WATER CIRCULATION SYSTEM 

MANUFACTURER: GEA IBERICA 

TYPE: PLATES 


PLATE MATERIAL: 14401 

SEALS: NBR 



PROCESS SIDE: 

LIQUID: water 


SIDE: 

LIQUID: Water 


SIZE: 1,814 x 1,395 x 530 mm 


No. UNITS: 1 

SERVICE 

I-2902 Chlorinator Condenser Water Cooler 2900 – Cooling Circuit 

ITEM: I-2902 

NAME: COOLING WATER COOLER DEMINERALISED 

WATER CIRCULATION SERVICE 

MANUFACTURER: GEA IBERICA 

TYPE: PLATES 


PLATE MATERIAL: 14401 

SEALS: NBR 



PROCESS SIDE: 

LIQUID: water 


SIDE: 

LIQUID: Water 


SIZE: 1,607 x 510 x 530 mm 


No. UNITS: 1 

SERVICE

I-4101 Methylene Chloride Gas Condenser 4100- Methylene chloride 

ITEM: I-4101 





BODY SIDE: 

LIQUID: CH2Cl2 






TUBE SIDE: 





DESIGN 



No. TUBES: 

SIZE: 3,586 x 1,660 x 254 mm 


No. UNITS: 1 

I-4201 Chloroform Gas Condenser 4200- Chloroform 

ITEM: I-4201 

NAME: CHLOROFORM GAS CONDENSER 




BODY SIDE: 

LIQUID: Chloroform 






TUBE SIDE: 





DESIGN 



No. TUBES: 

SIZE: 3,586 x 1,660 x 254 mm 


No. UNITS: 1

I-6101 Methanol Rectification Column Condenser 

6100 – Organic Hydrochloride Acid Effluent 

ITEM: I-6101 

NAME: METHANOL RECTIFICATION COLUMN 

CONDENSER 


TYPE: GRAPHITE BLOCKS 


BLOCK MATERIAL: VGC 

SEALS: EPDM 

PROCESS SIDE: 

LIQUID: CH3Cl + H2O 


SERVICE TEMPERATURE: 101.5 → 48.8º C 



TUBE SIDE: 

LIQUID: Water 





SIZE: 4,161 x 455 x 395 mm 


No. UNITS: 1

I-6102 Methanol Distillation Column Condenser 


ITEM: I-6102 

NAME: METHANOL DISTILLATION COLUMN 

CONDENSER 




BODY SIDE: 

LIQUID: CH3Cl +CH3OH 




TUBE SIDE: 





No. TUBES: 40 

SIZE: 




No. UNITS: 1 

I-6103 Methanol Distillation Column Re-boiler 


ITEM: I-6103 

NAME: METHANOL DISTILLATION COLUMN RE- 

BOILER 




BODY SIDE: 

LIQUID: Water vapour 




TUBE SIDE: 

LIQUID: Water 




No. TUBES: 21 

SIZE: 




No. UNITS: 1

I-6104 CH 3 OH Rectification Column Gas Condenser 


ITEM: I-6104 

NAME: METHANOL RECTIFICATION COLUMN GAS 

CONDENSER 




BODY SIDE: 

LIQUID: Chloroform + methanol + water 




TUBE SIDE: 

LIQUID: Water 




No. TUBES: 26 

SIZE: 




No. UNITS: 1 

I-6105 Residual HCl Pre-heater 6100 – Organic Hydrochloride Acid Effluent 

ITEM: I-6105 

NAME: RESIDUAL HCL PRE-HEATER 


TYPE: GRAPHITE BLOCKS 


BLOCK MATERIAL: VGC 

SEALS: PTFE 

PROCESS SIDE: 

LIQUID: 6% HCL 





SERVICE SIDE 1: 

LIQUID: HCl+CH3OH+CH3Cl+H2O 





SERVICE SIDE 2: 

LIQUID: H2O 





SIZE: 3,371 x 480 x 345 mm 


No. UNITS: 1

I-6301 Methanol Desorption Column Condenser 

6300 – MEOH Recovery and Sulphuric Regeneration Effluents 

ITEM: I-6301 

NAME: C-6301 CONDENSER 




BODY SIDE: 

LIQUID: 96% H2SO4 

DESIGN PRESSURE: -1 kg/cm2 


BODY MATERIAL: Glass 

SEALS: PTFE 

TUBE SIDE: 

LIQUID: WSA 



MATERIAL: Glass 

No. TUBES: 

SIZE: 

LENGTH: 



No. UNITS: 1 

I-6302 Residual Sulphuric Acid Pre-heater 

6300 – Sulphuric Regeneration and Recovery Effluents MEOH 

ITEM: I-6302 

NAME: RESIDUAL SULPHURIC ACID PRE-HEATER 


TYPE: Pre-heater 


BODY SIDE: 





SEALS: PTFE 

TUBE SIDE: 

LIQUID: H2O 



MATERIAL: Tantalum 

No. TUBES: 11 

SIZE: 




No. UNITS: 1

I-6303 C-6302 Re-boiler 6300 – Sulphuric Acid Regeneration Effluents 

ITEM: I-6303 

NAME: C-6302 RE-BOILER 




BODY SIDE: 

LIQUID: WSA 




SEALS: PTFE 

TUBE SIDE: 

LIQUID: Steam 



MATERIAL: Tantalum 

No. TUBES: 

SIZE: 

LENGTH: 825 mm 



No. UNITS: 1 

I-6305 Barometric Condenser 6300 – Sulphuric Acid Regeneration Effluents 

ITEM: I-6305 

NAME: BAROMETRIC CONDENSER 




BODY SIDE: 

LIQUID: steam 




SEALS: PTFE 

TUBE SIDE: 

LIQUID: WC 




No. TUBES: 

SIZE: 




No. UNITS: 1

I-6306 Post-condenser 6300 – Sulphuric Acid Regeneration Effluents 

ITEM: I-6306 

NAME: POST-CONDENSER 




BODY SIDE: 

LIQUID: steam 




SEALS: PTFE 

TUBE SIDE: 

LIQUID: WC 




No. TUBES: 

SIZE: 




No. UNITS: 1 

I-6307 Sulphuric Acid Heater 6300 – Sulphuric Acid Regeneration Effluents 

ITEM: I-6307 

NAME: 2nd STAGE HEATER 


TYPE: Heater 


BODY SIDE: 

LIQUID: Thermal oil 



BODY MATERIAL: Carbon steel 

SEALS: PTFE / IT 

TUBE SIDE: 




MATERIAL: GLASS LINED STEEL 

No. TUBES: 

SIZE: 




No. UNITS: 1

I-6308 Regenerated Sulphuric Acid Cooler 6300 – Sulphuric Acid Regeneration 

ITEM: I-6308 

NAME: H2SO4 REGENERATION EXCHANGER 


TYPE: Cooler 


BODY SIDE: 





SEALS: PTFE 

TUBE SIDE: 

LIQUID: WC 




No. TUBES: 

SIZE: 

LENGTH: 



No. UNITS: 1 

I-6309 Pre-heater 6300 – Sulphuric Acid Regeneration 

ITEM: I-6309 

NAME: H2S04 REGENERATION PRE-HEATER 


TYPE: Pre-heater 


BODY SIDE: 

LIQUID: WH 




SEALS: PTFE 

TUBE SIDE: 

LIQUID: WSA 




No. TUBES: 

SIZE: 

LENGTH: 



No. UNITS: 1

I-6601 Stripping Column Head Condenser 6600 – Stripping Column 

ITEM: I-6601 

NAME: STRIPPING COLUMN HEAD CONDENSER 


TYPE: PLATES 

EXCHANGE SURFACE: 10.2 M2 

PLATE MATERIAL: TITANIUM T35 

SEALS: VITON 

PROCESS SIDE: 

LIQUID: Alkaline water 




No. STEPS: 2 

TUBE SIDE: 

LIQUID: Water + solvent 




No. STEPS: 2 

SIZE: 1,607 x 510 x 530 mm 


No. UNITS: 1 

I-6602 Stripping Column Head Condenser 6600 – Stripping Column 

ITEM: I-6602 

NAME: STRIPPING COLUMN HEAD CONDENSER 

MANUFACTURER: ALFA LAVAL 

TYPE: PLATES 

MODEL: M10BW-FG 


PLATE MATERIAL: TITANIUM 

SEALS: 

No. PLATES: 10 

PROCESS SIDE: 

LIQUID: STEAM 

SERVICE TEMPERATURE: 101.6º C → 101.1º C 

DESIGN PRESSURE: 2 atg 


TUBE SIDE: 

LIQUID: WATER 

SERVICE TEMPERATURE: 29º C → 37.5º C 



SIZE: 710 x 470 x 981 mm 


No. UNITS: 1

I-6603 Stripping Column Cooler 6600 – Stripping Column 

ITEM: I-6603 

NAME: COOLER TO STRIPPING COLUMN 

MANUFACTURER: ALFA LAVAL 

TYPE: PLATES 

MODEL: M10BW-FD 


PLATE MATERIAL: TITANIUM 

SEALS: 

No. PLATES: 4 

PROCESS SIDE: 

LIQUID: STEAM 

SERVICE TEMPERATURE: 101º C → 40º C 



TUBE SIDE: 

LIQUID: WATER 

SERVICE TEMPERATURE: 29º C → 37.5º C 



SIZE: 800 x 470 x 981 mm 


No. UNITS: 1

6.- REACTORS 

R-1101 Hydrochlorinator 1100 – Hydrochlorination 

ITEM: R-1101 

NAME: HYDROCHLORINATOR REACTOR 

MANUFACTURER 

TYPE: BEM VERTICAL reactor 

SURFACE: 216 M2 

No. STEPS: Casing: 1; Tubes: 1 

BODY SIDE: 

LIQUID: HEAT MED. 

OPERATING TEMPERATURE: 256 / 260º C 


OPERATING PRESSURE: 2 / 0.8 kg/cm2 g 



BODY AND HEAD MATERIAL: A-515 Gr.60 

TUBE SIDE: 

LIQUID: REACTAN GAS 

OPERATING TEMPERATURE: 300º C 


OPERATING PRESSURE: 1.24 / 1.17 kg/cm2 g 



TUBE MATERIAL: A-240 Tp.347 

SEAL MATERIAL: 

CASING: Spiral wound type (ASBESTOS) 

+ CS Inner & Outer ring 

CHANNEL: Asbestos covered by 2 sheets 

of SS type 347 

SIZE: 


DIAMETER: 1,600 mm 


No. UNITS: 1

R-1201 Chlorinator 1200 – Chlorination 

ITEM: R-1201 

NAME: CHLORINATOR REACTOR 

MANUFACTURER: 

CAPACITY: 9.81 m3 

BODY SIDE: 

LIQUID: REACTOR LIQUID AND GAS 

OPERATING TEMPERATURE: 105º C 


OPERATING PRESSURE: 27 kg/cm2 g 


BODY AND HEAD MATERIAL: A-515 Gr.70 

TUBE SIDE: 

LIQUID: CLOS. COOL. WATER 

OPERATING TEMPERATURE: 51 / 70º C 


OPERATING PRESSURE: 2.4 / 1.7 kg/cm2 g 


TUBE MATERIAL: B-161-200 

SEAL MATERIAL: 

CASING: 

INTERNAL: Solid PTFE 

SIZE: 


DIAMETER: 1,050 mm 


No. UNITS: 1

7.- TANKS 

TK-1101 Hydrochloric Collector Tank 1100 – Hydrochlorination 

ITEM: TK-1101 

NAME: HYDROCHLORIC COLLECTOR TANK 

LIQUID: HYDROCHLORIC ACID 


CALCULATION PRESSURE: 0.05 kg/cm2 

COIL: NO 

TYPE OF CEILING: DOMED 

CAPACITY IN SERVICE: 1.98 m 3 

MATERIAL: FRP 

SIZE: 




No. UNITS: 1

TK-1201 Catalyst Preparation Tank 1200 – Chlorination 

ITEM: TK-1201 

NAME: CATALYST PREPARATION TANK 


CALCULATION TEMPERATURE: 40º C. 


COIL: NO 

TYPE OF CEILING: CONICAL 

CAPACITY IN SERVICE: 4 m 3 


SIZE: 




No. UNITS: 1 

TK-1202 Catalyst Supply Tank 1200 – Chlorination 

ITEM: TK-1202 

NAME: CATALYST SUPPLY TANK 




COIL: YES 

- CALCULATION TEMPERATURE: -20º C 

- CALCULATION PRESSURE: 0 kg/cm2 




SIZE: 




No. UNITS: 1

TK-1205-1/2 Daily Methylene Chloride Tank 1200 – Chlorination 

ITEM: TK-1205 1/2 

NAME: DAILY METHYLENE CHLORIDE TANK 




COIL: NO 




SIZE: 




No. UNITS: 2 

TK-1206-1/2 Daily Chloroform Tank 1200 – Chlorination 

ITEM: TK-1206 1/2 

NAME: DAILY CHLOROFORM TANK 




COIL: NO 




SIZE: 




No. UNITS: 2

TK-2103 Hydrochloric Acid Tank 2300 – Cooling Water Service 

ITEM: TK-2103 

NAME: HCL TANK 

LIQUID: 30 % HCL 

CALCULATION TEMPERATURE: 

CALCULATION PRESSURE: 

COIL: NO 


CAPACITY IN SERVICE: 

MATERIAL: POLYESTER FIBREGLASS 

SIZE: 




No. UNITS: 1 

TK-2104 Hydrochloric Acid Tank 2300 – Cooling Water Service 

ITEM: TK-2104 

NAME: SODA TANK 

LIQUID: 20-50% NaOH 


CALCULATION PRESSURE: atmospheric 

COIL: NO 

TYPE OF CEILING: KLOPPER 


MATERIAL: A-42 b 

SIZE: 




ACCESSORIES: Electrical resistance 

No. UNITS: 1

TK-2106 Water Tank 2300 – Cooling Water Service 

ITEM: TK- 

NAME: DEMINERALISED WATER TANK 

2106 

LIQUID: WATER 

CALCULATION TEMPERATURE: Ambient 


COIL: NO 




SIZE: 




No. UNITS: 1 

TK-3101-1/2 Methanol Storage Tank 3100 – Methanol 

ITEM: TK-3101-1/2 

NAME: METHANOL STORAGE TANK 

LIQUID: METHANOL 



COIL: NO 




SIZE: 




No. UNITS: 2

TK-4101-1/2 Methylene Chloride Storage Tank 

4100- Methylene chloride 

ITEM: TK-4101-1/2 

NAME: METHYLENE CHLORIDE STORAGE TANK 




COIL: NO 




SIZE: 




No. UNITS: 2 

TK-4201-1/2 Chloroform Storage Tank 4200- Chloroform 

ITEM: TK-4201-1/2 

NAME: CHLOROFORM STORAGE TANK 




COIL: NO 




SIZE: 




No. UNITS: 2

TK-4301 

ITEM: TK-4301 

Tetrachloride Storage Tank 4300 - Carbon Tetrachloride Transfer 

NAME: CARBON TETRACHLORIDE STORAGE 

TANK 

LIQUID: CARBON TETRACHLORIDE 



COIL: NO 




SIZE: 




No. UNITS: 1 

TK-4402 Hydrochloric Storage Tank 4400 – Hydrochloric Acid Transfer 

ITEM: TK-4402 

NAME: HYDROCHLORIC ACID STORAGE TANK 

LIQUID: 30% HCL 



COIL: NO 



MATERIAL: 

SIZE: 




No. UNITS: 1

TK-5101 

ITEM: TK-5101 

Soda Storage Tank 

NAME: SODA STORAGE TANK 

LIQUID: 20% CAUSTIC SODA 



COIL: NO 




SIZE: 




No. UNITS: 1 

TK-5201 

ITEM: TK-5201 

Concentrated Sulphuric Acid Tank 

NAME: CONCENTRATED SULPHURIC ACID TANK 

LIQUID: 98% SULPHURIC ACID 



COIL: NO 




SIZE: 




Nº UNITS: 1

TK-6301 Residual Storage Tank 6300 – Sulphuric Acid Regeneration 

ITEM: TK-6301 

NAME: RESIDUAL SULPHURIC STORAGE TANK 

LIQUID: 75-85% SULPHURIC ACID 



COIL: NO 



MATERIAL: PVDF + FRP (Derakane 411/45) 

SIZE: 




Nº UNITS: 1 

TK-6601 Moist Solvent Collector Tank 6600 – Stripping Column 

ITEM: TK-6601 

NAME: STRIPPING MOIST SOLVENT COLLECTOR 

TANK 

LIQUID: MOIST SOLVENTS 



COIL: NO 

TYPE OF CEILING: 


MATERIAL: 

SIZE: 


- Diameter: 


Nº UNITS: 1

TK-6602 Water Pump Priming Tank 6600 – Stripping Column 

ITEM: TK-6602 

NAME: CHLORINATED SOLVENTS TO STRIPPING 

WATER DISCHARGE PUMP PRIMING TANK 

LIQUID: CHLORINATED SOLVENTS 



COIL: NO 

TYPE OF CEILING: FLAT 


MATERIAL: 

SIZE: 

- Height: 700 mm 



Nº UNITS: 1 

8.- SEPARATORS 

S-1101 Soda Drip Separator 1100 – Hydrochlorination 

ITEM: S-1101 

NAME: SODA DRIP SEPARATOR 

LIQUID: CH3Cl gas + NaOH 



SERVICE PRESSURE: 1.1 kg/cm2 g 



MATERIAL: A-240 Tp.304 L 

SIZE: 




Nº UNITS: 1

S-1102 Sulphuric Drip Separator 1100 – Hydrochlorination 

ITEM: S-1102 

NAME: SULPHURIC DRIP SEPARATOR 

LIQUID: CH3Cl gas + liquid H2SO4 






MATERIAL: A-240 Tp.304 L 

SIZE: 




Nº UNITS: 1 

S-1201 to S-1206 Gas Condenser Separator 1200 – Chlorination 

ITEM: S-1201 NAME: GAS CONDENSER SEPARATOR 

LIQUID: 


DESIGN TEMPERATURE: 


DESIGN PRESSURE: 

CAPACITY: 

MATERIAL: 

SIZE: 

- Length: 960 mm 



Nº UNITS: 6

S-4101 Gas Condenser Separator 4100- Methylene Chloride 

ITEM: S-4101 

NAME: METHYLENE CHLORIDE FINISHED PRODUCT 

GAS CONDENSER SEPARATOR 






CAPACITY: 

MATERIAL: 

SIZE: 




Nº UNITS: 1 

S-4201 Gas Condenser Separator 4200- Chloroform 

ITEM: S-4201 

NAME: CHLOROFORM FINISHED PRODUCT GAS 

CONDENSER SEPARATOR 






CAPACITY: 

MATERIAL: 

SIZE: 




Nº UNITS: 1 

S-6201 Drip Separator 6200 - DG-1 Gas Effluents 

ITEM: S-6201 NAME: EFFLUENT DRIP SEPARATOR 

LIQUID: 





CAPACITY: 

MATERIAL: 

SIZE: 

- Length: 650 mm 



Nº UNITS: 1

S-6301 Vacuum Pump Separator 6300 – Sulphuric Acid Regeneration 

ITEM: S-6301 

NAME: H2SO4 REGENERATION SEPARATOR 


LIQUID: water vapour 



SERVICE PRESSURE (abs): 1 bar 

DESIGN PRESSURE: atmospheric 


MATERIAL: stainless steel 

SIZE: 


Nº UNITS: 1 

S-6601 Phase Separator 

ITEM: S-6601 

NAME: PHASE SEPARATOR 

SUPPLIER: CASALS CARDONA 

LIQUID: 




DESIGN PRESSURE: 1.1 kg/cm2 g 

CAPACITY: 304 litres 

MATERIAL: 

- Chemical barrier: PVDF 3 mm 

- Mechanical reinforcement: Derakane resin 411/45 

SIZE: 




Nº UNITS: 1

9.-BOILERS 

E-1201, E-1202, E-1203, E-4101, E-4201, E-3101 

ITEM: E-1201, E-1202, E-1203, 

NAME: BOILER 

E-4101, E-4201, E-3101 

Boiler 

OPERATION DATA: 

- Temperature: Ambient 

- Pressure: atmospheric 

- Flow: 1 m3/h. 

MATERIAL: 

-Ferrule: A-240 TP -304 L 

-Tubes: A-312 TP -304 L 

- Seals: Klinger 300 

SIZE: 



- Lock: 100 mm 

Nº UNITS: 6 

E-2401, E-2502, E-4301, E-6101 

ITEM: E-2401, E-2502, E-4301, 

E-6101, E-6303 

NAME: BOILER 

Boiler 


- Temperature: Ambient 

- Pressure: atmospheric 

- Flow: 1 m3/h. 

MATERIAL: 

-Ferrule: A-283-Gr.C 

-Tubes: A-106-Gr.B 


SIZE: 



- Lock: 100 mm 

Nº UNITS: 5

E-6302 TK-6301 Boiler 

ITEM: E-6302 

NAME: TK-6301 BOILER 


- Temperature: 

- Pressure: 

- Flow: 

MATERIAL: 

-Ferrule: A-283-Gr.C 

-Tubes: St -35 


SIZE: 

- Height: 


- Lock: 

Nº UNITS: 1

10.- COMPRESSORS 

K-2702 Compressor R.V. -40º C Refrigeration Unit 

ITEM: K-2702 

NAME: -40º C GROUP SUB-COOLING R.V. 

REFRIGERATION COMPRESSOR 

SUPPLIER: RAMÓN VIZCAINO 

WORKING CONDITIONS: -25º C/ +35º C 

COOLING POWER: 87.290 F/h 

COMPRESSOR: FRICK – YORK 

COMPRESSOR MODEL: 1216.22 M 6 V 


ABSORBED POWER: 68.7 CV 

R-22 CONDENSER: CBF-12-300ª-2P 

HEAT TO DISSIPATE: 130,600 Kcal/h 

WATER FLOW: 30 m3/h. 

MAXIMUM WATER INPUT TEMPERATURE: 26º C 

R-22 RECIPIENT: NRU-4-3000 

VOLUME 223 litres 

R-22 COOLER: HORIZONTAL MULTITUBULAR 

MODEL: DXRF-08-240-4P 

MOTOR POWER: 100 CV 


Nº UNITS: 1 

K-6201-1/2/S Gas Effluent Compressors 6200 - DG1 Gas Effluents 

ITEM: K-6201-1/2/S 

NAME: DG-1 GAS EFFLUENTS BUSCH 

COMPRESSOR 

MANUFACTURER: BUSCH 

SUCTION PRESSURE: 0.96 kg/cm2 g 

DISCHARGE PRESSURE: 1.8 kg/cm2 g 

FLOW: 43.8 kg/h 

Nº UNITS: 3

K-6301-1/S Vacuum Pump 6300 – Sulphuric Acid Regeneration 

ITEM: K-6301 1/S 

NAME: LIQUID RING VACUUM PUMP 


TYPE: LIQUID RING VACUUM PUMP 

MODEL: 2BE1102-OH Y 92 

RING LIQUID: WATER 

WATER FLOW: 11 m3/h. 

SUCTION PRESSURE: 33 m bar 

DISCHARGE PRESSURE: 1,100 m bar 

MAXIMUM CASING DIAMETER: 255.5 mm 

MAXIMUM CASING DIAMETER: 249 mm 

AXIAL PLAY: 0.21 mm 



Nº UNITS: 2 

K-6601 Compressor 6600 – Gas Refrigeration Unit 

ITEM: K-6601 

NAME: GAS REFRIGERATION UNIT COMPRESSOR 

SUPPLIER: COSMOTEC Srl 

COOLING POWER: 4,400 W 

SIZE: 735 x 860 x 1,500 mm 

ABSORBED POWER: 2,500 W 

COOLING LOAD: 2.4 Kg of R314 

HIGH/LOW PRESSURE SWITCH REG.: 2.4/0.04 mPa 

MAXIMUM WORKING PRESSURE: 1 mPa 

PUMP FLOW: 25 litres/min 

WEIGHT: 140 Kg

11.- VENTILATORS 

V-6201 Ventilator 6200 – Effluent Degassing 

ITEM: V-6201 

NAME: DEGASSING VENTILATOR 

SUPPLIER: TURBOVENT, S.A. 

MODEL: VR 35S17U315K 

MATERIAL: CARBON STEEL 

FLOW: 100 m3/h 

TOTAL PRESSURE: 140 mmWC 


ABSORBED POWER: 0.1 CV 

RECOMMENDED POWER: 2 CV 



ROTATION: R-3

12.- HEATERS 

H-2501 Thermal Oil p.m. Heater 2500- Thermal Oil Circuit 

ITEM: H-2501 

NAME: THERMAL OIL P.M. HEATER 

SURFACE: 7.8 M2 

OPERATING TEMPERATURE: 20 – 250º C 

POWER: 1.11 E5 KCAL/H 

TYPE OF INSULATION: 150 R 

MOTOR: 1 OF 129 kW 

OPERATING PRESSURE: 2.6 kg/cm2 g 

SIZE: 


- Diameter: 0.49 m 

H-6301 Thermal Oil Heater 6300 – Sulphuric Acid Regeneration 

ITEM: H-6301 

NAME: EFFLUENT DME BURNER 

SUPPLIER: ELMESS 

TYPE: DHFB3-30-T5 

SIZE: B3 

SIZE: 

- Resistance length: 1,200 mm 

- Total length: 1,460 mm 

- Resistance packet diameter: 120 mm 

- Flange: DN 150

13.- FILTERS / TUBS 

F-1201 -1/S Methyl Chloride Filter 1200 - Chlorination 

ITEM: F-1201-1/S NAME: METHYL CHLORIDE FILTER 






MATERIALS: 

- FERRULE AND FLOORS: A-240 Tp.304L 

- TUBES: A-312 Tp.304L 

- SEALS: SPIROMETALLIC S.S. Tp 304 AND TEFLON 

- FILTER: CERAMIC 

SIZE: 



Nº UNITS: 2 

F-1202 -1/S Chlorine Filter 1200 - Chlorination 

ITEM: F-1202-1/S NAME: CHLORINE FILTER 

LIQUID: CHLORINE 



SERVICE PRESSURE: 29 kg/cm2 g 


MATERIALS: 


- TUBES: A-312 Tp.304L 



SIZE: 



Nº UNITS: 2

F-1203 -1/S Crude Filter 1200 - Chlorination 

ITEM: F-1203-1/S 

NAME: CRUDE FILTER 

LIQUID: CRUDE 





MATERIALS: 


- TUBES: A-312 Tp.304L 



SIZE: 



Nº UNITS: 2 

F-2101 -1/S Demineralised Water Filter 2100 – Demineralised Water 

ITEM: F-2101-1/S NAME: DEMINERALISED WATER FILTER 

SUPPLIER: CIDA HIDROQUIMICA, S.A. 

LIQUID: WATER 


CALCULATION TEMPERATURE: AMBIENT 



MATERIALS: 

- FERRULE AND FLOORS: A-42b 

- TUBES: St.35 

- SEALS: SYNTHETIC RUBBER 

- FILTER: FLINT 

SIZE: 

- Total height: 3,030 mm 


Nº UNITS: 2

F-6501 -1/S Chloromethane Filter 6500 – Chemical Drainage Treatment 

ITEM: F-6501-1/S NAME: CHLOROMETHANE DRYING CARTRIDGE 

FILTER 






MATERIALS: 

- FERRULE AND FLOORS: A-285 Gr.C 

- TUBES: A-106 Gr.B 


- INTERNAL FILLING: GRANULATED Cl2Ca 

SIZE: 



Nº UNITS: 2 

F-6502 Chloromethane Filter 6500 – Chemical Drainage Treatment 

ITEM: F-6502 

NAME: CHLOROMETHANE DRYING CARTRIDGE 

FILTER 




SERVICE PRESSURE: 4 kg/cm2 g 


MATERIALS: 

- FERRULE AND FLOORS: A-240 Tp.304 L 

- TUBES: A-312 Tp.304 L 


- INTERNAL FILLING: GRANULATED Cl2Ca 

SIZE: 



Nº UNITS: 1

E-5202 Drying Tub 5200 – Regenerated Sulphuric 

ITEM: E-5202 

NAME: REGENERATED SULPHURIC TANK DRYING 

TUB 

SUPPLIER: CASALS CARDONA 

TYPE: MOISTURE DRYER 

LIQUID: SULPHURIC ACID 

MATERIALS: 

- Chemical barrier: PVDF 

- Mechanical reinforcement: orthophthalic resin with glass 

mats and fabrics 

SIZE: 

- Total height: 675 mm 


Nº UNITS: 1

4.- INSTRUMENTATION INVENTORY 

CHLORINE GAS VORTEX FLOWMETERS 

Two Vortex flowmeters with the following specifications: 

FT-1205 

TAG 

Manufacturer 

YOKOGAWA 

PROCESS DATA 

Liquid 

Chlorine gas 

Measurement range 0 – 1800 Nm 3 

Operating temperature 

112º C 

Operating pressure 29 kg/cm 2 

Density 3.17 kg/Nm 3 

Viscosity 

0.018 Cp 

MEASURER 

Model 

YF104-AGSE5D-S3S3*C/CES 

Type 

Vortex 

Connection to process 

DN-40 PN64 V13 shape 

Body material 

A-351 CF 8M 

Sensor material 

Stainless steel 

Output signal 

4 – 20 mA 

Power supply 

24 Vcc (two-thread system) 

Electrical protection 

Class I zone 2 group IIB T4 

Amplifier assembly 

Integrated 

Local indicator 

Yes 

FT-1205

FT-1206 

TAG 

Manufacturer 

YOKOGAWA 

PROCESS DATA 

Liquid 

Chlorine gas 

Measurement range 0 – 650 Nm 3 


112º C 


Density 3.17 kg/Nm 3 

Viscosity 

0.018 Cp 

MEASURER 

Model 

YF102-AGSE5D-S3S3*C/CES 

Type 

Vortex 


DN-25 PN64 V13 shape 

Body material 

A-351 CF 8M 

Sensor material 

Stainless steel 

Output signal 

4 – 20 mA 

Power supply 

24 Vcc (two-thread system) 



Amplifier assembly 

Integrated 

Local indicator 

Yes 

FT-1206

CHLORINE GAS MASS FLOWMETERS 

Nine Rosemunt (Micromotion) mass flowmeters with the following technical 

specifications: 

FT-1101 

TAG 

Manufacturer 

Rosemunt 

PROCESS DATA 

Liquid 

Methanol 

Measurement range 

0 – 1.8 m3/h 


12º C 

Operating pressure 3.5 kg/cm 2 

Model 

Type 


Wet part material 

Sensor housing material 


MEASURER 

Type D25/40 SS 

Mass 

DN15 PN16 C-shaped flange 

AISI-316 L 

AISI-304 


FT-1101 

Model 

Assembly 

Distance 

Power supply 

Output signal 

TRANSMITTER 

RFT-9712-2-P-N 

In control room 

150 m 

230 VAC 

4 – 20 mA

FT-1112 

TAG 

Manufacturer 

Rosemunt 

PROCESS DATA 

Liquid 

Methyl chloride 


0 – 3 m3/h 


40º C 


MEASURER 

Model Type D25/40 

Type 

Mass 


DN15 PN40 E-shaped flange 


AISI-316 L 


AISI-304 



FT-1112 

Model 

Assembly 

Distance 

Power supply 

Output signal 

TRANSMITTER 

RFT-9712-2-P-N 


150 m 

230 VAC 

4 – 20 mA

FT-1202 

TAG 

Manufacturer 

Rosemunt 

PROCESS DATA 

Liquid 

Liquid chloride 


0 – 4 m3/h 


15º C 


Model 

Type 





MEASURER 

Type D-100SS 

Mass 

DN15 PN40 R13-shaped flange 

AISI-316 L 

AISI-304 


FT-1202 

Model 

Assembly 

Distance 

Power supply 

Output signal 

TRANSMITTER 

RFT-9712-2-P-N 


150 m 

230 VAC 

4 – 20 mA

FT-1226 

TAG 

Manufacturer 

Rosemunt 

PROCESS DATA 

Liquid 



0 – 0.6 m3/h 


32º C 


Model 

Type 





MEASURER 

Type D25/40 SS 

Mass 


AISI-316 L 

AISI-304 


FT-1226 

Model 

Assembly 

Distance 

Power supply 

Output signal 

TRANSMITTER 

RFT-9712-2-P-N 


150 m 

230 VAC 

4 – 20 mA

FT-1231 

TAG 

Manufacturer 

Rosemunt 

PROCESS DATA 

Liquid 

Chloroform 


0 – 2.5 m3/h 


40º C 


Model 

Type 





MEASURER 

Type D-100SS 

Mass 


AISI-316 L 

AISI-304 


FT-1231 

Model 

Assembly 

Distance 

Power supply 

Output signal 

TRANSMITTER 

RFT-9712-2-P-N 


150 m 

230 VAC 

4 – 20 mA

FT-8100 

TAG 

Manufacturer 

Rosemunt 

PROCESS DATA 

Liquid 



0 – 65 m3/h 


32º C 


Model 

Type 





MEASURER 

Type D300-SS 

Mass 


AISI-316 L 

AISI-304 


FT-8100 

Model 

Assembly 

Distance 

Power supply 

Output signal 

TRANSMITTER 

RFT-9712-2-P-N 


100 m 

230 VAC 

4 – 20 mA

FT-8101 

TAG 

Manufacturer 

Rosemunt 

PROCESS DATA 

Liquid 

chloroform 


0 – 65 m3/h 


40º C 


Model 

Type 





MEASURER 

Type D300-SS 

Mass 


AISI-316 L 

AISI-304 


FT-8101 

Model 

Assembly 

Distance 

Power supply 

Output signal 

TRANSMITTER 

RFT-9712-2-P-N 


100 m 

230 VAC 

4 – 20 mA

O FLIX

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