Liquefaction co-processing of coal shale oil at - Argonne National ...
Liquefaction co-processing of coal shale oil at - Argonne National ... Liquefaction co-processing of coal shale oil at - Argonne National ...
Experiment No. 2 4 5 14 7 13 9 10 11 12 Fraction Feed Dewaxed Wax Feed Dewaxed Wax Feed Dewaxed Wax Feed Dewaxed Wax Feed oewaxed Wax Feed Dewaxed Wax Feed Dewaxed Wax Feed Dewaxed Wax Feed Dewaxed Wax Feed Dewaxed Wax TABLE 3 ANALYSES OF FEEDS AND PRODUCTS Hydrogen Types by 'H-NHR. % Aromatic Paraffinic -~ - C - H -- N S 14.6 17.0 2.6 14.6 19.5 2.2 14.6 19.3 2.7 9.3 15.3 4.1 10.8 12.5 4.6 10.8 14.1 5.0 21.3 22.9 0.3 21.3 24.6 1.9 25.9 26.9 0.8 20.7 23.8 2.8 42.6 34.2 82.5 42.6 32.5 88.4 42.6 28.8 71.2 49.4 33.6 62.0 40.7 38.4 57.6 42.5 35.2 55.4 40.3 35.6 91.3 40.3 32.5 90.9 31.4 30.1 86.7 33.8 26.4 76.9 Elwnental Analysis, rt 8 (a) 89.1 10.0 0.3 c0.1 88.4 9.8 0.4
la Figure 1. lH-NMR spectra of samples from experiment 5. (a) feed oil. (b) wax, (c) dewaxed oil. TMS - tetramethylsilane internal reference, SSB - spinning side band. 266
- Page 63 and 64: Figure 1. SCHEMATIC OF LCI CO-PROCE
- Page 65 and 66: SIMULATION OF A COAL/PETROLEuII RES
- Page 67 and 68: 20 pseudocomponents was developed t
- Page 69 and 70: ottoms is less sensitive to the num
- Page 71 and 72: Low Pressure Separator A temperatur
- Page 73 and 74: 7. Gallier, P.W., Boston, J.F., Wu,
- Page 75 and 76: I I I I I I I I I 100- --- Experime
- Page 77 and 78: Coprocessing Schemes The coprocessi
- Page 79 and 80: processing 25,000 and 150,000 bbl/d
- Page 81 and 82: FIGURE 1 I DISTRIBUTION OF REFINERI
- Page 83 and 84: Table 1. Samples Analyzed PNLNumber
- Page 85 and 86: the coal itself. The chemical compo
- Page 87 and 88: - - ITSL PAH Fraction PAH Fraction
- Page 89 and 90: PROCESS DEVELOPMENT STUDIES OF TWO-
- Page 91 and 92: SUMMARY e The major effect of close
- Page 93 and 94: omw '??h 4NO WNID ?N? 000 wmm c9'1'
- Page 95 and 96: tl f 246
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- Page 99 and 100: qkCqQ r! o! 0 0 0 0 0 0 0 I-UH ')I
- Page 101 and 102: Materials The catalyst was shell 32
- Page 103 and 104: CONCLUSIONS Separation of a light h
- Page 105 and 106: Table 3. Results of activity testin
- Page 107 and 108: feed coal and plant configuration a
- Page 109 and 110: P1 #2 #3 114 115 #6 ITSL subbitumin
- Page 111 and 112: temperature, time and solvent power
- Page 113: TABLE 1 EXPERIMENTAL CONDITIONS AND
- Page 117 and 118: PERFORMANCE OF THE LOW TEMPERATURE
- Page 119 and 120: BENCH UNIT DESCRIPTION Process deve
- Page 121 and 122: Recycle Residuum Hydrogenati On Res
- Page 123 and 124: FIRST STAGE HRI'S CATALYTIC TWO STA
- Page 125 and 126: FIRST-STAQ COAL CONVERSION (W I IIA
- Page 127 and 128: REACTOR SOLIOS HTOROGEN/CARBON ATOl
- Page 129 and 130: TRANSPORTATION FUELS FROM TWO-STAGE
- Page 131 and 132: Process Identification LV% Of AS- R
- Page 133 and 134: Table I11 HYDROTREATING TESTS WITH
- Page 135 and 136: Table IV HYDROTREATING TO 0.2 PPM N
- Page 137 and 138: Table VI EFFECT OF BOILING RANGE ON
- Page 139 and 140: (4) In all cases studied, the jet f
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- Page 143 and 144: INTEGRATED TWO-STAGE LIQUEFACTION:
- Page 145 and 146: are over-riding features in its fav
- Page 147 and 148: Complementary fundamental studies o
- Page 149 and 150: Comparative Economics of Two-Stage
- Page 151 and 152: The variation in hydrotreating cost
- Page 153 and 154: FIGURE 1: COMPARISONS OF ILLINOIS N
- Page 155 and 156: Process TABLE 1: TWO-STAGE PROCESSE
- Page 157 and 158: Abstract Temperature-Staged Catalyt
- Page 159 and 160: Results and Discussion Reactions in
- Page 161 and 162: 2. 3. 4. 5. 6. Derbyshire, F. J. an
- Page 163 and 164: I LL a rJJW ., .. ;> 0 i s W 8 a 31
Experiment<br />
No.<br />
2<br />
4<br />
5<br />
14<br />
7<br />
13<br />
9<br />
10<br />
11<br />
12<br />
Fraction<br />
Feed<br />
Dewaxed<br />
Wax<br />
Feed<br />
Dewaxed<br />
Wax<br />
Feed<br />
Dewaxed<br />
Wax<br />
Feed<br />
Dewaxed<br />
Wax<br />
Feed<br />
oewaxed<br />
Wax<br />
Feed<br />
Dewaxed<br />
Wax<br />
Feed<br />
Dewaxed<br />
Wax<br />
Feed<br />
Dewaxed<br />
Wax<br />
Feed<br />
Dewaxed<br />
Wax<br />
Feed<br />
Dewaxed<br />
Wax<br />
TABLE 3<br />
ANALYSES OF FEEDS AND PRODUCTS<br />
Hydrogen Types<br />
by 'H-NHR. %<br />
Arom<strong>at</strong>ic Paraffinic<br />
-~ - C - H --<br />
N S<br />
14.6<br />
17.0<br />
2.6<br />
14.6<br />
19.5<br />
2.2<br />
14.6<br />
19.3<br />
2.7<br />
9.3<br />
15.3<br />
4.1<br />
10.8<br />
12.5<br />
4.6<br />
10.8<br />
14.1<br />
5.0<br />
21.3<br />
22.9<br />
0.3<br />
21.3<br />
24.6<br />
1.9<br />
25.9<br />
26.9<br />
0.8<br />
20.7<br />
23.8<br />
2.8<br />
42.6<br />
34.2<br />
82.5<br />
42.6<br />
32.5<br />
88.4<br />
42.6<br />
28.8<br />
71.2<br />
49.4<br />
33.6<br />
62.0<br />
40.7<br />
38.4<br />
57.6<br />
42.5<br />
35.2<br />
55.4<br />
40.3<br />
35.6<br />
91.3<br />
40.3<br />
32.5<br />
90.9<br />
31.4<br />
30.1<br />
86.7<br />
33.8<br />
26.4<br />
76.9<br />
Elwnental Analysis,<br />
rt 8 (a)<br />
89.1 10.0 0.3 c0.1<br />
88.4 9.8 0.4
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