RED HERRING PROSPECTUS Dated August 24 ... - Globus Spirits

RED HERRING PROSPECTUS Dated August 24 ... - Globus Spirits RED HERRING PROSPECTUS Dated August 24 ... - Globus Spirits

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GRAIN PROCESS LIQUEFACTION FERMENTATION AND DISTILLATION PROCESS DESCRIPTION FOR GRAIN BASED LIQUEFACTION AND FERMENTATION: FLOW DIAGRAM FOR GRAIN SPIRIT PRODUCTION: Milling Section Slurry Preparation / Liquefaction Section Consisting of i. Grain storage (20 days capacity) ii. Magnetic separator iii. Vibratory Screen iv. Chain conveyor v. Bucket elevators vi. Hopper bins vii. Hammer mill Consisting of i. Mixing tank ii. Slurry tank iii. Jet cooker iv. Holding coil v. Flash tank / holding tank vi. Liquefaction tank vii. Slurry coolers Fermentation Section Consisting of additional equipment for the Existing fermentation section like i. Fermentors ii. Wash re circulation pumps iii. Fermented wash coolers iv. Suitable modifications in piping / equipment, etc. A) MILLING AND FLOUR HANDLING: The incoming grain is first cleaned with the help of destoner and magnetic separators to remove stones and other material, which may damage the hammers during milling. The grain is fed to hammer mill in controlled manner. In milling, grain is crushed to flour of uniform size. Oversized screening rejects are segregated with the help of vibratory screen. These are taken to coarse bin before sending it to mill again. Intermediate hopper is provided for buffer capacity for flour storage. The flour addition is metered through a weigh feeder with load cell arrangement before transferring to the mixing tank for slurry preparation process. B) SLURRY PREPARATION / LIQUEFACTION: Grain flour is fed at controlled rate to mixing tank and then to agitated slurry tank where some amount of water and enzyme stabilizing chemicals is added. A portion of the liquefying enzyme is also added here. This slurry is then “cooked” in the jet cooker. The slurry is continuously pumped to a steam jet cooker where high-pressure steam at 7 bar (g) / 170 °C rapidly raises the slurry temperature. The mixture of slurry and steam is then passed through the holding coil which has several “U” bends in series and sufficient capacity to provide the desired retention time at a given flow rate. The cooked mash is discharged to a flash tank. The cooking process, accomplished in the above manner, 83

converts the slurry into a hydrated, sterilized suspension (as starch molecule is solubilized) and is therefore susceptible to enzyme attack for liquefaction. The gelatinized mash from the flash tank is liquefied in a liquefaction tank where liquefying enzyme (alpha-amylase) is added. Then the liquefied mash is cooled in slurry cooler to about 60 °C and transferred to partial pre-Saccharification tank where the Saccharifying enzyme (Glucosidase) is added. This process initiates the formation of sugar. The mash is then cooled and transferred to fermentors. C) SACCHARIFICATION AND FERMENTATION: Yeast Propagation: Yeast seed material is prepared in water-cooled vessels by inoculating sterilized mash with culture yeast. Optimum temperature is maintained by cooling water. The contents of the yeast vessel are then transferred to Prefermentor. The prefermentors are filled with mash and loaded with contents of the yeast vessel. The purpose of the aerated pre-fermentation is to allow time for the yeast cells to multiply and reduce the chances of contamination in fermentors. When the prefermentor contents are transferred to the main fermentors, the concentration of yeast cells is high enough to substantially reduce the lag time associated with yeast growth in fermentation. GRAIN BASED FERMENTATION: The purpose of fermentation is to convert the fermentable substrate into alcohol. To prepare the mash for fermentation, it may have to be diluted with water. The pH of the mash is adjusted by recycled slops (which also provides for nutrients) and by the addition of acid. At the start of the cycle, the fermentor is charged with mash and contents of the prefermentor. Significant heat release takes place during fermentation. This is removed by forced circulation cooling in external heat exchangers to maintain an optimum temperature of 30°C. The re-circulating pumps also serve to empty the fermentors into beer well. After the fermentors are emptied, they are cleaned with water and caustic solutions and sterilized for the next batch. The carbon dioxide evolved during the process is scrubbed to prevent ethanol emissions by process water, which is taken to beer well. FOR GRAIN BASED THIN SLOP CONCENTRATION: First effect is forced circulation type, where as second, third and fourth effects are Falling Film type. The Thin Slop at 60 – 65 0 C from Distillation section is first taken in to feed tank and then after preheating fed to evaporation system in 4 th effect backward feed mode and it flows from Fourth to third to second to first. The concentrated Syrup with 28–30% w/w total solids is taken out from the First effect. The low-pressure steam shall be supplied to the First effect shell side. Vapours generated in the First effect are used as a heating medium in the second effect and vapours generated in the second effect are used as a heating medium in the Third effect vapours generated in the third effect are used as heating medium in the fourth effect. The feed shall be concentrated from the initial concentration of 7–7.2% w/w Total Spirit to 28- 30% w/w Total Spirit as it travels forward through all effects. The vapours evolved from the final effect are condensed in surface condensers. Each effect is provided with recirculation pump. The first effect steam condensate can be recycled back to 84

converts the slurry into a hydrated, sterilized suspension (as starch molecule is<br />

solubilized) and is therefore susceptible to enzyme attack for liquefaction.<br />

The gelatinized mash from the flash tank is liquefied in a liquefaction tank where<br />

liquefying enzyme (alpha-amylase) is added. Then the liquefied mash is cooled in slurry<br />

cooler to about 60 °C and transferred to partial pre-Saccharification tank where the<br />

Saccharifying enzyme (Glucosidase) is added. This process initiates the formation of<br />

sugar. The mash is then cooled and transferred to fermentors.<br />

C) SACCHARIFICATION AND FERMENTATION:<br />

Yeast Propagation:<br />

Yeast seed material is prepared in water-cooled vessels by inoculating sterilized mash<br />

with culture yeast. Optimum temperature is maintained by cooling water. The contents<br />

of the yeast vessel are then transferred to Prefermentor.<br />

The prefermentors are filled with mash and loaded with contents of the yeast vessel.<br />

The purpose of the aerated pre-fermentation is to allow time for the yeast cells to<br />

multiply and reduce the chances of contamination in fermentors. When the<br />

prefermentor contents are transferred to the main fermentors, the concentration of<br />

yeast cells is high enough to substantially reduce the lag time associated with yeast<br />

growth in fermentation.<br />

GRAIN BASED FERMENTATION:<br />

The purpose of fermentation is to convert the fermentable substrate into alcohol. To<br />

prepare the mash for fermentation, it may have to be diluted with water. The pH of the<br />

mash is adjusted by recycled slops (which also provides for nutrients) and by the<br />

addition of acid.<br />

At the start of the cycle, the fermentor is charged with mash and contents of the prefermentor.<br />

Significant heat release takes place during fermentation. This is removed by<br />

forced circulation cooling in external heat exchangers to maintain an optimum<br />

temperature of 30°C. The re-circulating pumps also serve to empty the fermentors into<br />

beer well. After the fermentors are emptied, they are cleaned with water and caustic<br />

solutions and sterilized for the next batch.<br />

The carbon dioxide evolved during the process is scrubbed to prevent ethanol emissions<br />

by process water, which is taken to beer well.<br />

FOR GRAIN BASED THIN SLOP CONCENTRATION:<br />

First effect is forced circulation type, where as second, third and fourth effects are Falling Film<br />

type.<br />

The Thin Slop at 60 – 65 0 C from Distillation section is first taken in to feed tank and then after<br />

preheating fed to evaporation system in 4 th effect backward feed mode and it flows from Fourth<br />

to third to second to first.<br />

The concentrated Syrup with 28–30% w/w total solids is taken out from the First effect. The<br />

low-pressure steam shall be supplied to the First effect shell side. Vapours generated in the First<br />

effect are used as a heating medium in the second effect and vapours generated in the second<br />

effect are used as a heating medium in the Third effect vapours generated in the third effect are<br />

used as heating medium in the fourth effect.<br />

The feed shall be concentrated from the initial concentration of 7–7.2% w/w Total Spirit to 28-<br />

30% w/w Total Spirit as it travels forward through all effects.<br />

The vapours evolved from the final effect are condensed in surface condensers. Each effect is<br />

provided with recirculation pump. The first effect steam condensate can be recycled back to<br />

84

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