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LTCC PROCESSING INSTRUCTIONS For Ferro A6 and L8 Tape

LTCC PROCESSING INSTRUCTIONS For Ferro A6 and L8 Tape

LTCC PROCESSING INSTRUCTIONS For Ferro A6 and L8 Tape

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1.1 UNREEL TAPE<br />

<strong>LTCC</strong> <strong>PROCESSING</strong> <strong>INSTRUCTIONS</strong><br />

<strong>For</strong> <strong>Ferro</strong> <strong>A6</strong> <strong>and</strong> <strong>L8</strong> <strong>Tape</strong><br />

FERRO <strong>Tape</strong> is commonly removed from its polyester backing film at the first stage of<br />

processing. However, it is also possible with FERRO <strong>Tape</strong> to retain the backing film on the tape<br />

until the lamination stage of processing is reached. If the tape is removed from the backing film,<br />

this should be carried out in clean, dust free conditions. There is no requirement for the material<br />

to be aged prior to further processing for stabilization purposes, <strong>and</strong> heat treatment should be<br />

avoided, since it provides no benefit <strong>and</strong> may be detrimental to the materials further<br />

performance.<br />

1.2 BLANK TAPE TO SIZE<br />

The FERRO <strong>Tape</strong> may be blanked using st<strong>and</strong>ard techniques such as hot knife, die cutting, or<br />

lasering. Blanked tape should be used as soon as possible after blanking, <strong>and</strong> preferably within<br />

2 weeks.<br />

The lead free, non toxic nature of the FERRO <strong>Tape</strong> facilitates disposal of scrap tape.<br />

1.3 FRAME AND REGISTER<br />

Registration holes are commonly added to the material during blanking, or may be subsequently<br />

punched, drilled or lasered into the unfired tape.<br />

FERRO <strong>Tape</strong> may also be mounted onto support frames using rubber cements or similar<br />

adhesives.<br />

Cross plying of the FERRO <strong>Tape</strong> is not necessary.<br />

1.4 PUNCH VIAS/CAVITIES<br />

Vias may be formed in the FERRO <strong>Tape</strong> using mechanical punches, drills or lasers. Via<br />

diameters as small as 2 mil (50 μm) have been demonstrated in the FERRO <strong>A6</strong>-5-M tape, but<br />

for production purposes, a minimum via diameter of 4 mil (100 μm) is suggested. Maximum via<br />

diameters of up to 25 mil (625μm) have been demonstrated. <strong>Ferro</strong> recommends either a USHIO<br />

or Baccini punch.


1.5 FILL VIAS<br />

STENCILS<br />

At <strong>Ferro</strong> Electronic Materials, 3 mil thick brass stencils are used on an AMI printer, MP9156, to<br />

fill vias. The brass is punched on a Ushio MP7150 punch using tight tolerance dies with 5μm<br />

clearance <strong>and</strong> brass bottomed strippers. The brass is lightly oiled before punching <strong>and</strong> usually<br />

is punched twice to ensure good cone-free holes.<br />

The punched brass is mounted in a 12” x 12” frame on a stainless steel 325 mesh screen. First,<br />

the brass is cut to size <strong>and</strong> glue is spread on one side around the edge of the brass in a b<strong>and</strong><br />

about 1/2-inch wide. The brass is then pressed into the center of the bottom of the screen <strong>and</strong><br />

weights are put on the screen to ensure good contact of the brass <strong>and</strong> screen while the glue<br />

dries.<br />

After the glue has dried, the screen mesh is cut away from on top of the stencil. Some thin tape,<br />

such as Scotch tape, can be used to smooth the cut edge of the screen.<br />

PRINTER<br />

The printer used at <strong>Ferro</strong> Electronic Materials has a porous stone base through which a vacuum<br />

can be pulled. A backing paper is always used between the stone <strong>and</strong> the tape layer.<br />

The printer parameters are important. These are:<br />

PRINTING<br />

Squeegee 90 durometer, diamond 3/8 inches.<br />

Squeegee Set in the squeegee “down position” with the screen removed. The printer<br />

Pressure stage with paper <strong>and</strong> tape in place is positioned under the squeegee <strong>and</strong><br />

the squeegee pressure adjusted to 7.5 psi.<br />

Downstop This can be left open.<br />

Squeegee Set to 0.6 inches per second in both directions.<br />

Speed<br />

Print Mode Use print/print mode, i.e., print in both directions for each filling of vias.<br />

Vacuum Use 20-25 inches Hg. It is important that areas of the stone outside the<br />

tape <strong>and</strong> backing paper are covered to prevent vacuum leakage. Mylar<br />

can be used for this.<br />

Snap-Off With stencil in place, bring the screen slowly down until the vacuum just<br />

pulls it on to the stone with tape <strong>and</strong> backing paper on it. Then use this as<br />

zero set-point <strong>and</strong> make snap-off at 25 mils.<br />

Vias are filled using the print/print printer mode. After printing, the paper must stay in place<br />

beneath the tape during the drying stage to ensure good vias. So carefully lift the paper <strong>and</strong><br />

tape together from the printer stone stage <strong>and</strong> place in drying oven. Dry for 30 minutes at 70°C.<br />

Then pull tape from the paper. Only a very minor amount of paste will remain on the paper. Via<br />

filling is typically accomplished using modified on or off contact printing with metal or plastic


ased stencils. A vacuum pull through is typically used on the printing stage, <strong>and</strong> backing paper<br />

is typically used for backing the film during the via filling operation. Purpose built bladder type<br />

via filling equipment may also be used with the FERRO <strong>Tape</strong> <strong>and</strong> Via fill paste systems. Precise<br />

via filling conditions will depend on the number, size <strong>and</strong> mix of vias to be filled, <strong>and</strong> should be<br />

determined experimentally.<br />

1.6 DRY<br />

After completion of via filling the parts should be dried (backing paper still supporting the tape)<br />

in conventional drying ovens at a maximum temperature of 70°C for 20 to 30 minutes.<br />

1.7 PRINT CONDUCTORS<br />

Conductors are printed onto the tape using conventional screen printing techniques <strong>and</strong><br />

recommended screens (see individual product data sheets). Conductor prints may be dried in<br />

conventional drying ovens at a maximum temperature of 70°C for 10 minutes.<br />

1.8 DRY<br />

Dry in conventional drying ovens at a maximum temperature of 70°C for 10 to 20 minutes.<br />

1.9 PRINT RESISTORS<br />

All co-fireable resistors are printed onto the unfired tape using #325 screens. Target dried<br />

thickness is 25-28 μm. The resistors should be dried in conventional drying ovens at a<br />

maximum temperature of 70°C for 10 minutes.<br />

1.10 DRY<br />

Dry in conventional drying ovens at a maximum temperature of 70°C for 10 to 20 minutes.<br />

1.11 STACK LAYERS<br />

All layers should be inspected for visual acceptance <strong>and</strong> collated.<br />

1.12 INSERTS FOR CAVITY FORMATION<br />

Some general guidelines are offered in “<strong>Ferro</strong> <strong>LTCC</strong> H<strong>and</strong>ling <strong>and</strong> Design Recommendations.”<br />

These must be followed for best results.<br />

There are four principal types of cavity.<br />

1. Cavity with vertical walls but closed at bottom.<br />

2. Cavity with stepped walls, closed at bottom.<br />

3. Through cavity.


4. Through cavity with stepped walls.<br />

One other type of cavity has been produced <strong>and</strong> is a major problem to control. This cavity has a<br />

floor that is not at the bottom of the laminate, i.e. the cavity bottom is only supported where it<br />

joins the walls.<br />

At <strong>Ferro</strong> Electronic Materials the preferred approach to cavity formation is to punch the cavity<br />

layers before any metallization steps (vias, conductors, resistors). Because punching is used<br />

cavity geometries are limited to rectangular shapes with rounded corners.<br />

It must be recognized that removal of much of a tape layer for cavities can seriously weaken the<br />

green sheet <strong>and</strong> cause difficulties during subsequent processing. One approach to overcome<br />

this problem is to punch the tape cavities after metallization. Frames for this have been<br />

produced by UHT. Results using this method at <strong>Ferro</strong> Electronic Materials have not been good<br />

because alignment of vias were never as good as with the single punching step.<br />

PROCESS STEPS<br />

1. Punch each layer of tape. This punching will make both via holes <strong>and</strong> cut out the<br />

cavity.<br />

2. Fill vias.<br />

3. Print conductors.<br />

4. Print cofiring resistors.<br />

5. Stack layers on registration fixture.<br />

6. Put inserts in cavities (see below for inserts). Do not use top plate.<br />

7. Vacuum bag.<br />

8. Laminate.<br />

9. Remove from vacuum bag <strong>and</strong> remove from registration fixture.<br />

10. Remove inserts.<br />

11. Trim part to size.<br />

12. Fire.<br />

Some of the above steps may not be necessary, e.g. some layers may have no vias.<br />

INSERTS<br />

Inserts are essential to prevent the cavities from distortion during lamination. At its simplest this<br />

distortion will result in rounded cavity wall edges. At the most extreme, cavities will tend to close<br />

up <strong>and</strong> the bottom of the cavity will lift.<br />

The through cavities are easiest to deal with. Here inserts can be made from hard materials that<br />

can be machined to give a good fit.<br />

With other types of cavity the <strong>Ferro</strong> Electronic Materials preferred material for inserts is Silastic<br />

J RTV from Dow Corning. These inserts are made by preparing a dummy part with cavities but


no metallization, etc. Only minimum pressure is used to laminate this dummy part to avoid any<br />

cavity distortion. With <strong>Ferro</strong> <strong>Tape</strong>, 1000 psi has typically been used.<br />

Once the dummy laminate has been prepared, the Silastic J is cast in the cavities <strong>and</strong> allowed<br />

to cure. After curing, the inserts are removed <strong>and</strong> cleaned <strong>and</strong> are then ready for use.<br />

Other materials that can be used for inserts are pieces of latex <strong>and</strong> other soft rubber. Latex<br />

must be accurately cut to size however.<br />

STEPPED WALLS<br />

It is important to underst<strong>and</strong> that a major problem can arise with stepped walls. This occurs if<br />

inserts are too stiff <strong>and</strong> do not compress enough during the lamination step. Consequently the<br />

steps can receive greater or lesser pressure than the bulk of the laminate <strong>and</strong> during firing<br />

shrink at a different rate.<br />

A similar effect can occur with cavity bottoms if a top plate is used on the registration fixture that<br />

over compresses Silastic J or latex.<br />

1.13 LAMINATION<br />

Lamination may be carried out in either isostatic or uniaxial laminators. However, lamination is<br />

critical in achieving consistent green density, <strong>and</strong> hence consistent shrinkage, hermeticity <strong>and</strong><br />

electrical performance, <strong>and</strong> <strong>Ferro</strong> strongly recommends the use of isostatic lamination, which<br />

has been demonstrated to give the most consistent results.<br />

Recommended lamination conditions are a pressure of 3000 psi, a temperature of 70°C with a<br />

10 minute dwell time –no pressure followed by a lamination time of 10 minutes.<br />

<strong>Ferro</strong> will provide Lamination Pressure vs. Lamination Density curves for each lot of <strong>Ferro</strong> <strong>Tape</strong><br />

as a reference guide for processing.<br />

1.14 BURN-OUT / FIRING<br />

Organic burn out may be combined with the firing operation in both box <strong>and</strong> tunnel furnaces, or<br />

may be performed as a separate step.<br />

The unfired laminates are heated, on their setters, at a rate of 2°C/minute to peak temperature<br />

of 450°C, which should be maintained for a minimum of 2 hours, to ensure complete<br />

combustion of all organics. This burn out procedure should be considered a starting point,<br />

although it should be more than adequate for most requirements; fine tuning of the burnout<br />

procedure will depend on part size, number of layers, <strong>and</strong> amount of metallization.


<strong>For</strong> <strong>A6</strong> <strong>Tape</strong> use the following profile:<br />

Ramp for 450°C to 850°C at 6-8C per minute followed by a 10 minute dwell at 850C. The air<br />

flow should be set at 100 SCFH. It is critical that <strong>A6</strong> see 850C for a minimum of 10 minutes<br />

<strong>A6</strong> <strong>Tape</strong> Burn out & Firing Profile<br />

TemperatureC<br />

900<br />

800<br />

700<br />

600<br />

500<br />

400<br />

300<br />

200<br />

100<br />

25C<br />

St<strong>and</strong>ard Bakeout <strong>and</strong> Firing Profile for <strong>Ferro</strong> <strong>A6</strong>S <strong>Tape</strong> System<br />

450C<br />

0<br />

0 100 200 300 400 500 600 700<br />

450C<br />

Time in Minutes<br />

850C<br />

Firing Profile is 6C - 8C per minute from 450C-850C with a minimum 10 minute soak<br />

Bakeout Profile is 2C per minute from 250C to 450C with a 2 hour soak<br />

<strong>For</strong> <strong>L8</strong> <strong>Tape</strong> choose from the following profiles:<br />

Box- Ramp for 450°C to 850°C at 4- 8C per minute followed by a 30 minute dwell at 850C<br />

Belt- 16’ (7) Zone furnace with a 0.5” /minute belt speed <strong>and</strong> a set point of 850C –see <strong>L8</strong><br />

Belt profile below –contact <strong>Ferro</strong> for specific Zone air flow <strong>and</strong> temperature settings<br />

25C


<strong>L8</strong> <strong>Tape</strong> Burn out & Firing Profile Box Furnace<br />

Temperature C<br />

900<br />

800<br />

700<br />

600<br />

500<br />

400<br />

300<br />

200<br />

100<br />

0<br />

St<strong>and</strong>ard Bakeout <strong>and</strong> Firing Profile for <strong>Ferro</strong> <strong>L8</strong>- Box Kiln<br />

Firing Ramp Rate is 4C - 8C per minute from 450C - 850C with a 30 minute soak<br />

Bakeout Profile is 1C* per minute from 25C to 450C with a 2 hour soak<br />

* Bakeout ramp adjusted to 1C /min for Thicker Parts > 50-mils<br />

0 100 200 300 400 500 600<br />

Time in Minutes<br />

450C<br />

Parts less than 50 mils can generally use a 2C ramp for Bakeout depending<br />

upon metal loading<br />

<strong>L8</strong> <strong>Tape</strong> Burn out & Firing Profile Belt Furnace<br />

Temperature C<br />

900<br />

800<br />

700<br />

600<br />

500<br />

400<br />

300<br />

200<br />

100<br />

<strong>L8</strong> Belt Profile<br />

0<br />

0 50 100 150 200 250 300 350 400 450<br />

Time Minutes


1.15 FIRING<br />

RECOMMENDED SETTTERS<br />

Fused quartz for either <strong>L8</strong> or <strong>A6</strong> . Bare alumina setters are ok for <strong>L8</strong> but should not be used for<br />

<strong>A6</strong>M. In some cases Zirconia felt is better for full coverage ground plane metallization parts to<br />

improve air flow <strong>and</strong> reduce hot spots <strong>and</strong> ultimately warpage.<br />

RECOMMENDED SUPPLIERS<br />

Fused Quartz GE 124, 16 micro inch surface: Behm Quartz Industries,<br />

www.behmquartz.com 800.543.7875<br />

Zirconia Felt: Zicar Fibrous Ceramics, Part No. ZYF-50, Tel: 800.245.2562<br />

Alumina Setters, 96% Alumina, Coorstek www.coorstek.com<br />

1.16 CLEANING<br />

There is no cleaning solution for tape. Particulates are typically removed with an anti-static<br />

brush. We recommend using only reagent grade acetone for cleaning fired parts.


<strong>LTCC</strong> DESIGN<br />

RECOMMENDATIONS<br />

2.1 CONDUCTOR LAYOUT<br />

Conductor width <strong>and</strong> spacing<br />

A B C<br />

preferred 30 mils 20 mils 10 mils<br />

possible 4 mils 4 mils 4 mils<br />

Product Resistance normalized<br />

to 25.4 microns<br />

(mΩ/sq.)<br />

<strong>A6</strong> & <strong>L8</strong> All Au<br />

FX 30-025


<strong>L8</strong> All Ag<br />

CN33- 498 Ag


2.2 GROUND AND POWER PLANES<br />

IC Bonding Fingers<br />

FEATURE SURFACE PLANE BURIED PLANES<br />

SOLID GROUND/POWER<br />

PLANE<br />

COMPLETE COVERAGE 100 MIL WIDE STRIPS MAX<br />

GRID SIZE 10 MIL CONDUCTOR 10 MIL CONDUCTOR<br />

15 MIL SPACING<br />

15 MIL SPACING<br />

CASTELLATION N/A AT EDGES OF PART OR<br />

AT CAVITY WALL<br />

CASTELLATION<br />

N/A ENDS >10 MILS FROM<br />

CLEARANCE<br />

EDGE OR WALL<br />

GROUNDING<br />

N/A ENDS EXTEND >10 MILS<br />

CASTELLATION<br />

PAST EDGE<br />

FEED THROUGH<br />

CLEARANCE<br />

20 MILS ALL SIDES 20 MILS ALL SIDES<br />

TAPE LAYERS ABOVE OR OFFSET SPACE AND OFFSET SPACE AND<br />

BELOW GRID PLANES LINES BY 12 MILS<br />

LINES BY 12 MILS<br />

X-Y<br />

X-Y


2.3 CAVITIES


2.4 ELECTRICAL VIAS<br />

Electrical via to edge of substrate.<br />

Via<br />

A<br />

Recommended<br />

Thickness<br />

Diameter<br />

Min<br />

Punch Method<br />

2 mil >10 mil 25 mil Punch<br />

4-10 20 mil Punch<br />

10 mil 25 mil Punch<br />

4-10 20 mil Punch<br />

10 mil 25 mil Punch<br />

4-10 20 mil Punch<br />


2.6 THERMAL VIAS<br />

Product<br />

Dimensions of Thermal Via <strong>and</strong> Catch Pad<br />

Thermal Conductivity<br />

(W/m-k)<br />

Thermal<br />

Resistance<br />

<strong>A6</strong><br />

CN 30-078 (Au) >50


Thermal Hexagonal Via Pattern: Six mil vias only<br />

Thermal Rectangular Via Pattern: 6 or 10 mil vias


2.7 RESISTORS<br />

Technical Specification 87 Series Resistor System <strong>For</strong> <strong>A6</strong> <strong>Tape</strong><br />

Tolerance Hot TCR Cold TCR<br />

Resistor Type Ohms/square Specification (ppm/°C) (ppm/°C)<br />

FX 87-011 Buried 10 ±30% - -<br />

FX 87-011 Surface 10 ±30% - -<br />

FX 87-101 Surface 100 ±30% ±450 ±450<br />

FX 87-101 Buried 100 ±30% ±450 ±450<br />

FX 87-102 Surface 1000 ±30% ±200 ±200<br />

FX 87-102 Buried 1000 ±30% ±200 ±200<br />

FX 87-103 Surface 10,000 ±30% ±200 ±200<br />

FX 87-103 Buried 10,000 ±30% ±200 ±200<br />

Resistor Layout <strong>and</strong> Probe Area Layout


Resistor to conductor termination overlaps for surface <strong>and</strong> buried resistors<br />

Minimum Spacing Maximum Spacing<br />

Layout<br />

(mils)<br />

(mils)<br />

A 10 15<br />

B 15 20<br />

C 10 10


2.7 Resistors-cont.<br />

Ohms<br />

120<br />

100<br />

80<br />

60<br />

40<br />

20<br />

0<br />

Blending of the 87 Series<br />

Blend curve for 87-101Series Resistor Material with<br />

% Additions of 87-011 (40 x 40 mil resistor)<br />

0 20 40 60 80 100<br />

Percent by weight of 87-011

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