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ORNL-4191 - the Molten Salt Energy Technologies Web Site

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Fig. 18.5. Hasvellcy N (Titanium Modified, Heat 66-<br />

548) Annealed 1 hr at 215OoF, Aged 30 min at About<br />

1200" F.<br />

Typi caI precipi tote morphologies determined<br />

by extraction replica technique.<br />

been included. It can be seen in Fig. 18.73 that<br />

<strong>the</strong> Hastelloy N modified by reducing <strong>the</strong> molyb-<br />

denum content (No. 168) is superior to <strong>the</strong> corn-<br />

mercial inaterial (INSRE grade Hastelloy N). The<br />

addition of 0.5% Zr to <strong>the</strong> modified alloy lowers<br />

<strong>the</strong> ZDT by 225°F. As is shown in Fig. 18.7b,<br />

223<br />

Table 18.2. The Zero Ductility Temperature<br />

of <strong>the</strong> Base Materials Studied<br />

Identification Composition (wt X)<br />

1 Wuinber Ni Mo Cr Fe Zr ("F)<br />

K educ ti on<br />

ZDT in AreaB<br />

(a)<br />

IGR ha1 12 7 2350 22<br />

169 bal 12 7 0.1 2350 21<br />

170 bal 12 7 0.3 2125 20<br />

171 bal 12 7 0.5 2125 32<br />

172 bal 12 7 0.7 2120 5<br />

lllSRE grade bal 16 4 2300 3<br />

Hastelloy N<br />

aMeasured at 50°F below ZDT.<br />

<strong>the</strong> recovery of all four of <strong>the</strong>se alloys is quite<br />

good. Excellent recovery is exhibited by alloy<br />

174. Its recovery of ductility was nearly instan-<br />

taneous and to a ra<strong>the</strong>r high level; however, from<br />

<strong>the</strong> standpoint of weldability, its low ZDT is not<br />

acceptable.<br />

Fur<strong>the</strong>r efforts will be made to develop a zir-<br />

conium-bearing alloy with a higher ZDT. If we<br />

can find a combination of alloying elements that<br />

will raise <strong>the</strong> ZDT and retain <strong>the</strong> good recovery<br />

characteristics, we shall proceed fur<strong>the</strong>r with <strong>the</strong><br />

development of this alloy system.<br />

18.5. RESIDUAL STRESS MEASUREMENTS<br />

IN HASTELLOY N WELDS<br />

A. G. Cepolina<br />

Welding inherently leads to large residual<br />

stresses. These stresses can lead to dimensional<br />

changes and can even be large enough to cause<br />

cracks in <strong>the</strong> weldment. For <strong>the</strong>se reasons we<br />

have initiated a study to investigate <strong>the</strong> stress<br />

distribution in and near welds in Hastelloy N.<br />

A technique was developed which allowed con-<br />

tinuous reading of <strong>the</strong> stress values, thus making<br />

it possible to know, with sufficient precision, <strong>the</strong><br />

stress gradient adjacent to <strong>the</strong> weld axis. For<br />

this study, a 12-in.-diam, '/,-in.-thick piece of<br />

Hastelloy N base metal was used. Two circular<br />

bead-on-plate welds were simultaneously made,<br />

one on each side of <strong>the</strong> plate. 'The diameter of <strong>the</strong>

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