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ORNL-1816 - the Molten Salt Energy Technologies Web Site

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-:<br />

PERIOD ENDING DECEMBER 70, 7954<br />

TABLE 6.6. RESULTS OF STATIC TESTS OF BRAZED A-NICKEL T-JOINTS IN<br />

NaF-ZrF4-UF4 (53.5-40-6.5 mole X) AT 150OoF FOR 100 hr<br />

Brazing Alloy Weight Weight<br />

Corn pas it i on Change Change Metal lographic Notes<br />

(wt %) (9) (%)<br />

69 Ni-20 Cr-11 Si -0.0017 -0.055<br />

100 cu -0.0006 -0.019<br />

82 Au-18 Ni -0.001 -0.036<br />

80 Au-20 Cu<br />

90 Ni-10 P -0.0004 -<br />

60 Pd-40 Ni -0.0016 -<br />

60 Pd-37 Ni-3 Si + 0.0008 + 0.027<br />

Surface attack to a depth of 16 mils along entire braze fillet<br />

Surface attack to a depth of 0.5 mil along entire braze fillet<br />

Braze fillet appeared to be unattacked<br />

No attack on braze fillet surface<br />

No attack on braze fillet surface<br />

No attack on braze fillet surface<br />

No attack on braze fillet surface<br />

TABLE 6.7. RESULTS OF STATIC TESTS OF BRAZED A-NICKEL T-JOINTS IN<br />

SODIUM HYDROXIDE FOR 100 hr AT 1100 AND 150OoF<br />

4 Brazing Allay Weight Weight Test<br />

%- Composition Change Change Temperature Metallographic Notes<br />

- * (wt %) (9) (%I (OF)<br />

t-<br />

+3<br />

d<br />

- . t<br />

69 Ni-20 Cr-11 Si 1500 Braze failed completely<br />

+ 0.0024 + 0.093 1100 Braze ottacked completely<br />

100 cu - .0.0118 -0.408 1500 Braze attacked completely; large voids appear<br />

throughout<br />

-0.001 1 -0.038 1100 Uniform surface attack on braze to a deDth of 3 mils<br />

82 Au-18 Ni -0.00.4 -0.144 1500 Nonuniform surface attack on braze to depth of 1 mil<br />

-0.0007 -0.022 1100 No attack on surface of braze<br />

60 Pd-3 of 6 mills<br />

J<br />

83

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