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ORNL-1771 - Oak Ridge National Laboratory

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ANP QUARTERLY PROGRESS REPORT<br />

TABLE 6.3, RESULTS OF STATIC TESTS OF HASFELLOY R BN VARIOUS MEDlA AT 15QQaF FOR lQ0 hr<br />

Bath<br />

Weight Weight<br />

Change Change<br />

(%I (g/ i n. 2,<br />

N a F- Zr F 4- U F (50-46-4 mo I e %) - 0.05 -0.003 7<br />

NaOH<br />

Sodium<br />

Lithium<br />

Lead<br />

.........<br />

t7.9 +0.608a<br />

-0.06 -0.0021<br />

-0.07 -0.0047<br />

Metal I ographi c Notes<br />

Specimen unattacked except in one small area where<br />

voids extended to a depth of 1 mil; no attack on<br />

vapor zone of tube<br />

Specimen !'-in> square attacked throughout entire<br />

4<br />

thickness<br />

Specimen and bath zone attacked to a depth of<br />

0.25 to 0.5 mil in the form of voids; exposed<br />

surface of bath zone of container partly de-<br />

carburized to a depth of l mil<br />

Small voids to a depth of 0.25 mil in specimen and<br />

bath zone of tube; surface partly decarburized by<br />

lithium<br />

Specimen heavily attacked to a maximum depth of<br />

.<br />

3 mils (average 2 mils); bath zone attacked uni-<br />

formly to a depth of 1.5 mils; phase change prob-<br />

ably occurred in attacked areas; vapor zone<br />

unattacked<br />

0.004<br />

X<br />

0<br />

0<br />

E)<br />

0.002<br />

0.003<br />

Fig. 6.7. Ha5telloy R Exposed to Static NaF-ZrF,UF, (50-46-4 mole %) for 100 Rr at 1500OF. Etched<br />

with aqua regia.<br />

88<br />

1<br />

CJ<br />

z<br />

-

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