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ORNL-2106 - the Molten Salt Energy Technologies Web Site

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and lose <strong>the</strong>ir hardness in <strong>the</strong> presence of Cellu-<br />

lube. These particular problems could be solved<br />

by using O-rings made from butyl rubber, but,<br />

unfortunately, butyl rubber suffers severe radia-<br />

tion damage. Tests to determine <strong>the</strong> radiation<br />

stability of Cellulube are planned for <strong>the</strong> near<br />

future.<br />

Dow<strong>the</strong>rm A, which is a good heat transfer<br />

medium but which has poor lubricating properties,<br />

was also selected for study because it is rela-<br />

tively stable upon exposure to radiation. Dow<strong>the</strong>rm<br />

A is a eutectic mixture containing 26.5% diphenyl<br />

and 73.5% diphenyloxide that is manufactured by<br />

<strong>the</strong> Dow Chemical Co, of Midland, Michigan. The<br />

only test run to date was terminated after 575 hr<br />

due to a motor failure, There was no transverse<br />

load applied during <strong>the</strong> test. The Dow<strong>the</strong>rm A<br />

operating temperature was 210 to 220'F. Both<br />

seals had well-developed wear patterns, The upper<br />

seal showed no leakage after <strong>the</strong> first 4 hr. The<br />

lower seal had no leakage for <strong>the</strong> first 150 hr, at<br />

which time it began to leak at a nearly uniform<br />

rate of 20 cm3/day. Upon examination, <strong>the</strong> lower<br />

seal rotor was found to have a light copper deposit.<br />

This is contrary to <strong>the</strong> information provided by Dow.<br />

The system used for this test had previously been<br />

operating with Cellulube, und, although it was<br />

carefully and thoroughly cleaned, it is possible<br />

that some Cellulube may have remained and caused<br />

<strong>the</strong> plating. This problem will be investigated in<br />

future tests,<br />

The process side of <strong>the</strong> seal nose had a black,<br />

gummy deposit, which proved to be virtually all<br />

carbon. Since <strong>the</strong>re was no evidence of physical<br />

damage to <strong>the</strong> Gaphitar seal nose, it is probable<br />

that this deposit was <strong>the</strong> residue from Dow<strong>the</strong>rm A<br />

which <strong>the</strong>rmally decomposed in leaking across <strong>the</strong><br />

seal interface. Ag <strong>the</strong> elastomer O-ring<br />

As originally designed <strong>the</strong> reactor pumps utilized,<br />

as <strong>the</strong> upper bearing, a spherical roller type of<br />

PERIOD ENDING JUNE 10, 1956<br />

antifrictioq bearing. In addition to providing ample<br />

thrust and radial load-carrying capacities, this<br />

type of bearing permitted shaft alignment with<br />

respect to <strong>the</strong> journal bearing without attendant<br />

shaft deflections. This design appeared to be ode-<br />

quate until tests of long duration on pump rotary<br />

elements revealed that <strong>the</strong> initial bearing end play<br />

of 0.0045 in. (maximum) had increased by a factor<br />

of 2 to 3. Such excessive end play is not con-<br />

ducive to good dynamic seal performance and it<br />

also interferes with <strong>the</strong> close axial tolerances<br />

required in <strong>the</strong>se pumps. The easiest solution to<br />

this problem, with respect to minimizing pump<br />

redesign, was to change to a double-row angular-<br />

contact bearing having convergent angles of con-<br />

tact. This has been done and, to date, all per-<br />

formance has been satisfactory. However, more<br />

operating time will be necessary to prove <strong>the</strong><br />

reliability of <strong>the</strong> redesigned bearing arrangement.<br />

A temporary impasse has been reached in <strong>the</strong><br />

development of seals for <strong>the</strong> NaK (primary and<br />

auxiliary) pumps. All <strong>the</strong> seals purchased for<br />

comparative testing have failed in operation. The<br />

seal obtained from <strong>the</strong> Sealol Corporation failed<br />

because <strong>the</strong> unhardened stainless steel wear ring<br />

rotor and <strong>the</strong> mating carbon ring wore out in less<br />

than 20 hr. The ceramic rotor of <strong>the</strong> seal obtained<br />

from <strong>the</strong> Durametallic Corporation disintegrated<br />

upon application of a 7OoF temperature differential<br />

to <strong>the</strong> lubricating oil. An attempt to correct this<br />

condition will be made by utilizing a thin ceramic<br />

facing on a steel-bodied rotor, The Byron Jackson<br />

Co. seals never developed full wear patterns, even<br />

after runs in excess of 300 hr. This condition<br />

apparently resulted from distortion of <strong>the</strong> relatively<br />

thin rotor. At no time during test operation with<br />

any of <strong>the</strong>se seals was Q satisfactory leakage rate<br />

Therefore efforts are being made to<br />

configuration similar to that being<br />

used on <strong>the</strong> fuel and sodium pumps. In addition,<br />

o<strong>the</strong>r promising types of commercially available<br />

seals will be investigated.<br />

Pump Lube-OiI System GarAttenuat<br />

5. M. DeCump<br />

he leakage tests of <strong>the</strong> seals<br />

MF-2 fuel pump<br />

tinued with Gulfspin 60 oil bein<br />

lubricant. For <strong>the</strong>se tests <strong>the</strong> temperature of <strong>the</strong><br />

%. M. Decamp, ANP Qwr. Prog. Rep. March 10, 1956,<br />

<strong>ORNL</strong>-2061, p 48.<br />

47

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