A solution and solid state study of niobium complexes University of ...
A solution and solid state study of niobium complexes University of ...
A solution and solid state study of niobium complexes University of ...
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Appendix A<br />
Table 2.3: Bond angles (°) for [Nb(acac)(OEt) 2(O)]4.<br />
Bond Angle (°)<br />
O(2)-C(1)-C(2) 124.6 (3)<br />
O(2)-C(1)-C(4) 116.2 (4)<br />
C(2)-C(1)-C(4) 119.2 (4)<br />
C(3)-C(2)-C(1) 124.5 (3)<br />
C(3)-C(2)-H(2) 117.8<br />
C(1)-C(2)-H(2) 117.8<br />
O(3)-C(3)-C(2) 124.7 (3)<br />
O(3)-C(3)-C(5) 114.9 (3)<br />
C(2)-C(3)-C(5) 120.4 (3)<br />
C(1)-C(4)-H(4A) 109.5<br />
C(1)-C(4)-H(4B) 109.5<br />
H(4A)-C(4)-H(4B) 109.5<br />
C(1)-C(4)-H(4C) 109.5<br />
H(4A)-C(4)-H(4C) 109.5<br />
H(4B)-C(4)-H(4C) 109.5<br />
C(3)-C(5)-H(5A) 109.5<br />
C(3)-C(5)-H(5B) 109.5<br />
H(5A)-C(5)-H(5B) 109.5<br />
C(3)-C(5)-H(5C) 109.5<br />
H(5A)-C(5)-H(5C) 109.5<br />
H(5B)-C(5)-H(5C) 109.5<br />
O(4)-C(6)-C(7) 112.4 (4)<br />
O(4)-C(6)-H(6A) 109.1<br />
C(7)-C(6)-H(6A) 109.1<br />
O(4)-C(6)-H(6B) 109.1<br />
C(7)-C(6)-H(6B) 109.1<br />
H(6A)-C(6)-H(6B) 107.9<br />
C(6)-C(7)-H(7A) 109.5<br />
C(6)-C(7)-H(7B) 109.5<br />
H(7A)-C(7)-H(7B) 109.5<br />
C(6)-C(7)-H(7C) 109.5<br />
H(7A)-C(7)-H(7C) 109.5<br />
H(7B)-C(7)-H(7C) 109.5<br />
O(6)-C(8)-C(9A) 112.0 (4)<br />
O(6)-C(8)-C(9B) 105.7 (9)<br />
C(9A)-C(8)-C(9B) 30.1 (7)<br />
O(6)-C(8)-H(8A) 109.2<br />
C(9A)-C(8)-H(8A) 109.2<br />
C(9B)-C(8)-H(8A) 84.9<br />
O(6)-C(8)-H(8B) 109.2<br />
C(9A)-C(8)-H(8B) 109.2<br />
C(9B)-C(8)-H(8B) 135.7<br />
H(8A)-C(8)-H(8B) 107.9<br />
103