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Ph.D. Thesis - Physics

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Spherical octagon, feedthroughs, and oven<br />

The spherical octagon is a stainless steel piece manufactured by Kimball physics (Part No.<br />

MCF450-SO20008). It has two 4 1/2 in. con-flat (CF) sealing surfaces, and eight 1 1/3 in.<br />

CF sealing surfaces. The top 4 1/2 in. surface is used for imaging. A anti-reflective (AR)<br />

coated fused silica viewport is used, while on the bottom there is another viewport, although<br />

it was not used in this work. The system used a total of three electrical feedthroughs. One<br />

provides the high-voltage rf signal to the trap. A separate feedthrough is used for this<br />

to limit stray capacitance that can adversely affect the Q factor of the rf resonance. The<br />

second feedthrough is a 9-pin sub-d connection that carries any dc voltages that may be<br />

needed for the trap. The setup in Ch. 6 is very similar to this one, and does make use of<br />

these connections. The final feedthrough holds the strontium oven and is used to supply it<br />

with current.<br />

The oven used in the experiments of Ch. 5 and 6 is made of a piece of thin tantalum<br />

foil that is folded into a tube. One end of the oven is spot-welded closed and then grains of<br />

strontium metal are added to the open end. This end is then spot-welded closed, and both<br />

ends of the oven are spot-welded directly to the stainless steel wires of the feedthrough. A<br />

hole is poked in the side of the oven that faces the ion trap; it is important that this be the<br />

only opening in the oven. A typical resistance for the finished oven, including feedthroughs,<br />

is about 0.5 Ω, and currents of 3 A are normally sufficient to load the trap.<br />

Vacuum pumps and pressure gauge<br />

Initial pumpdown of the system to O(10 −6 torr) is done with a turbomolecular pump backed<br />

by a roughing pump. After reaching this vacuum level, a valve to the turbo pump is closed<br />

and two pumps that are an integral part of the vacuum system are used.<br />

The ion pump is a Varian 60 l/s triode pump. The triode configuration pumps noble<br />

gases more efficiently than the original diode configuration, which is very useful in Ch. 6,<br />

but less essential here. A titanium sublimation pump (Ti-sub) is also used. It consists<br />

of a long titanium filament through which ≈ 40 A of current is flowed. Titanium is then<br />

deposited on the walls of the vacuum housing. A six-inch-diameter stainless steel nipple<br />

serves as this surface; it is significantly wider than the filament to increase the surface area<br />

on which titanium is deposited. As shown in Fig. 5-4, the filament is mounted at a right<br />

angle to the aperture that leads to the ion trap, reducing the chances of depositing titanium<br />

on the trap. The Ti-sub does not need to be fired continuously; typically, it is fired once a<br />

week (for 1-5 minutes) as long as some improvement in pressure is observed after firing.<br />

These two pumps are sufficient to reach pressures in the 10 −10 torr range after bakeout.<br />

Bakeout is a process in which the entire vacuum chamber is heated to around 200 ◦ C and<br />

pumped on. The higher temperature increases the outgassing rate of material adsorbed on<br />

surfaces within the chamber, and essentially speeds up the pumpdown. This is a standard<br />

procedure for ultra high vacuum (UHV) apparatus. A typical baking time is around 1-2<br />

112

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