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PRACTICE C—WATER COMPATIBILITY 19. Significance and Use 19.1 This practice is intended for use by those in the waste management industries. 19.2 This practice is used to determine whether a waste has the potential to generate extreme heat or violent reactions, and produce fumes, dusts, gases, or other products when mixed with water. 19.3 This practice is designed to determine water compatibility of a waste. 19.4 This practice can be used to qualitatively judge the solubility and apparent density of waste (if immiscible) relative to water. 20. Interferences 20.1 The generation of colorless fumes or gases, pressure buildup without visible bubbling, mild effervescence, or heat may go undetected. 21. Apparatus 21.1 Disposable Beakers, test tubes, or similar equipment. 21.2 Disposable Pipet (5-mL capacity). 21.3 Spatula. 21.4 Thermometer, 20 to 110°C or equivalent with 0.5°C divisions. 21.5 Vortex Mixer (optional). 22. Reagents and Materials 22.1 Reagent Water. 23. Hazards 23.1 Avoid inhalation of and skin and eye contact with any hazardous waste. 23.2 This procedure must be performed within a laboratory fume hood with the sash down as far as possible. 23.3 Warning—By keeping the sample size small and by first screening for very reactive wastes, the overall hazard is D5058 − 12 small. The small hazard is justified due to the much larger hazard of mishandling reactive waste at plant scale. 24. Procedure 24.1 Keep thermometer in water at room temperature until ready for use. Note temperature of water in degrees Celsius or Fahrenheit. 24.2 Bring sample to room temperature, if necessary. 24.3 Place a small amount (approximately 10 mL) of water into a disposable beaker or test tube. 24.4 Introduce approximately 1 mL of waste into the beaker or test tube and mix well. Note any violent reactions, fumes, dusts or gases, and any precipitates or emulsions, and record observations. 24.5 If any such reactions are noted, the waste fails the water compatibility test. 24.6 Once it has been determined that no violent reaction is occurring, and as soon as possible after 24.4, place the thermometer into the beaker or test tube and note any temperature change (increase ( + ) or decrease (−)), recording the change in temperature in degrees Celsius or Fahrenheit (see Note 1). 24.7 Some reactions may have a latent period or accelerate as they proceed. Retain the mixed sample for 5 or 10 min, then observe it and record its temperature again. 24.8 If no reactions were observed and no significant temperature change is noted, the waste has passed the water compatibility test. 24.9 Report the miscibility and apparent density of the sample as immiscible or miscible and lighter or heavier than water. 25. Precision and Bias 25.1 No statement is made about either the precision or bias of this practice since the result merely states whether there is conformance to the criteria for success specified in the procedure. 26. Keywords 26.1 compatibility; waste screening ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentioned in this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the risk of infringement of such rights, are entirely their own responsibility. This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years and if not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standards and should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of the responsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you should make your views known to the ASTM Committee on Standards, at the address shown below. This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the above address or at 610-832-9585 (phone), 610-832-9555 (fax), or service@astm.org (e-mail); or through the ASTM website (www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/ COPYRIGHT/). Copyright by ASTM Int'l (all rights reserved); Fri Oct 26 11:50:51 EDT 2012 4 Downloaded/printed by Sue Terry (Jbr+Environmental+Consultants) pursuant to License Agreement. No further reproductions authorized.
APPENDIX 2-E Characterization Data
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Precious Metals Recovery LLC RCRA P
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ITEM # REGULATIONS GENERAL DESCRIPT
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ITEM # REGULATIONS GENERAL DESCRIPT
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PMR Nevada RCRA Permit Application
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PMR Nevada RCRA Permit Application
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ITEM # REGULATIONS GENERAL DESCRIPT
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ITEM # REGULATIONS GENERAL DESCRIPT
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ITEM # REGULATIONS GENERAL DESCRIPT
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ITEM # REGULATIONS GENERAL DESCRIPT
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M-3 M-3 ITEM # REGULATIONS GENERAL
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OMB# 2050-0024; Expires ___________
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EPA ID Number OMB#: 2050-0024; Expi
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EPA ID Number ADDENDUM TO THE SITE
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EPA ID Number OMB#: 2050-0024; Expi
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EPA ID Number OMB#: 2050-0024; Expi
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EPA ID Number OMB#: 2050-0024; Expi
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This document is for reference purp
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A B C D E F $$W ATERMARKD$$ N 4,475
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Precious Metals Recovery LLC Dry Hi
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3.2 Barrier and Means to Control En
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19.0 APPROVAL OF PETITION FOR EXTEN
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LIST OF TABLES Table 1.2-1 Secondar
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Figure 23.1-1 Decomposition & Waste
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Section 10 Appendices 10-A Figures
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HVAC Heating, Ventilation, and Air
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GLOSSARY OF SELECTED TERMS [Authori
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INTRODUCTION Precious Metals Recove
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Pre-application Public Meeting - 40
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(Purity ≥ 99.5%, Directly Stored)
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Administration (MSHA) document, Con
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Fire Doors/Emergency Exit Doors Pr
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When leaving the plant spaces, work
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Infiltration Air Office Area Pig Pi
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personnel will be trained in respon
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Figure 1.2-1: Elemental Mercury Tra
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Tanks Or Containers Carbon Drums (n
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Figure 1.2-2: Calomel Feed Preparat
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Figure 1.2-3: Filter Press and Loca
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Activated carbon is used in the air
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Figure 1.2-5: SO2 Scrubber and Loca
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Above the retort tray/drum transfer
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Figure 1.2-8: Carbon Filter and Loc
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Figure 1.2-10: Overall Ventilation
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Wash water from open sumps. Safety
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1.3 Elemental Mercury Storage - 40
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The following items are located out
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Control System Architecture The pla
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will be supplied in accordance with
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Outdoor Material Storage A list of
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It is recognized that the fire prot
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Outdoor Areas Hydrants and hose bo
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the event of a security violation,
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2.3 Determination of Treatment Para
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Table 2.5-2: Test Methods Parameter
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Sampling Containerized Waste The te
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Process Waste Solution A discrete p
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ii. The sampling person removes a s
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2.9 Screening for Ignitable, Reacti
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3.0 SECURITY PLAN - 40 CFR 270.14(b
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4.0 INSPECTION PLAN - 40 CFR 270.14
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TSF, associated hazards, places whe
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Outside of working hours, a notific
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Damaged containers will be placed i
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7.0 PREVENTION AND SAFETY PROCEDURE
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8.0 PREVENTION OF ACCIDENTAL IGNITI
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10.0 TRAFFIC - 40 CFR 270.14(b)(10)
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Delivery frequency of reagents will
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10.3 Traffic Control Signs Traffic
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11.4 Surrounding Land Use - 40 CFR
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12.0 PERSONNEL TRAINING PLAN - 40 C
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that are not land based. Closure of
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13.4.6 Types of Off-site Waste Mana
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14.0 CLOSED HAZARDOUS WASTE DISPOSA
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storage area (e.g., storage racks),
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16.0 POST-CLOSURE ESTIMATES - 40 CF
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18.0 TOPOGRAPHICAL MAP - 40 CFR 270
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20.0 GROUNDWATER MONITORING - 40 CF
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22.0 CONTAINERS AND CONTAINMENT - 4
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Figure 22.1-2: Dedicated Transfer C
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Larger sized HDPE drums may be used
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22.3.2 Labeling Containers - 40 CFR
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22.5 Description of Secondary Conta
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will be done on the new waste strea
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23.0 TREATMENT AND STORAGE TANKS Me
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Figure 23.0-2: HCl Tank and Locatio
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Tank Dimensions Waste Solution Stor
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decomposed in the Decomposition Tan
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Figure 23.1-3: Waste Solution Stora
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The Water Storage Tank will supply
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Tank Caustic Soda Storage Tank* Hyd
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23.13 Recordkeeping A recordkeeping
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25.0 WASTE PILES - 40 CFR 270.18 &
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27.0 LAND TREATMENT - 40 CFR 270.20
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29.0 BOILERS/INDUSTRIAL FURNACE - 4
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30.1.3 Retort Operating Procedures
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of 13.5 feet long by 4.7 feet wide
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31.0 PROCESS VENTS - 40 CFR 270.24
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33.0 DRIP PADS - 40 CFR 270.26 & 26
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35.0 REFERENCES American Society of
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At the PMR Dry Hills Facility Open
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APPENDIX I-B Open House Comments
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APPENDIX 1-A Drawings Facility draw
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A B C D EF $ $ W A TERMARKA1$$ H340
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A B C D E F $$W ATERMARKD$$ 1 2 3 4
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A B C D E F $$W ATERMARKD$$ N 4,475
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A B C D EF $ $ W A TERMARKA1$$ H340
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A B C D E F $$W ATERMARKD$$ H340940
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A B C D E F $$W ATERMARKD$$ NOTE: 1
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B A B C D E F $$W ATERMARKD$$ H3409
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APPENDIX 1-C Process Flow Diagrams
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H - 340940 Precious Metals Recovery
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H - 340940 Precious Metals Recovery
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H - 340940 Precious Metals Recovery
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H - 340940 Precious Metals Recovery
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H - 340940 Precious Metals Recovery
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APPENDIX 1-D Floor and Wall Sealant
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C8 x 11.5 EPOXY COATING ON 2" THICK
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8" THICK INSULATED PRECAST CONCRETE
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C8 x 11.5 EPOXY COATING ON 2" THICK
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2. PRODUCTS 2.1 Stonclad GS Stoncla
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APPENDIX 2-A Waste Analysis Plan
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WASTE ANALYSIS PLAN 1 PURPOSE AND S
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Table 1: Analytical Methods for the
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All wastes received will have been
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Waste will not be accepted until th
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Table 3: Waste Sampling Matrix Type
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9 LDR TREATMENT STANDARDS Waste Des
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Drummed consolidation waste will be
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eevaluated whenever the process tha
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ATTACHMENT 2-A-1 Profile Instructio
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PMR LLC 460 W. 50 North Suite 500 S
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• Is the waste pyrophoric? a See
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EPA's Chemical Compatibility Chart
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1.0 SCOPE AND APPLICATION METHOD 90
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7.2.3 Adjust the electrodes in the
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METHOD 9045D SOIL AND WASTE pH 9045
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NOTE: Combination electrodes incorp
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10.0 REFERENCES 1. National Bureau
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1.0 SCOPE AND APPLICATION METHOD 13
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4.2.2 Bottle Extraction Vessel. Whe
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4.10 Watchglass, appropriate diamet
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7.0 PROCEDURE 7.1 Preliminary Evalu
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determine whether the solid materia
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solids content of the waste sample
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material into an extractor bottle.
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sample from which no additional liq
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slowly out of the ZHE device into a
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® TEDLAR bag is used, if the extra
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150% of the expected concentration
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None of the parameters had a signif
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Table 2. Suitable Rotary Agitation
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Table 4. Suitable Filter Holders 1
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Table 6. Multi-Laboratory TCLP Meta
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Table 8. Multi-Laboratory Semi-Vola
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Figure 1. Rotary Agitation Apparatu
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METHOD 1311 (CONTINUED) TOXICITY CH
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Designation: D4979 − 08 Standard
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Designation: D4978 − 95 (Reapprov
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FIG. 1 Method B, Sulfide Test Appar
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TABLE 1 Determination of Bias, Pycn
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for four known specific gravity lev
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21.7.1 To check the precision of sa
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Designation: D4981 − 08 Standard
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Designation: D5058 − 12 Standard
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11.6.1 Compare the temperature here
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5. Fire-fighting measures General I
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Carcinogenicity: CAS# 10112‐91‐
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Combined Hazen Solution Analysis pH
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irritation and possible burns. May
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OSHA Vacated PELs: Mercury: 0.05 mg
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Chemical waste generators must dete
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APPENDIX 4-A Inspection Plan
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1 INSPECTION PLAN This Inspection P
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Inspections are intended to detect
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Boilers and Industrial Furnaces Ins
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PMR Daily Inspection Form #1 Date:
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PMR Daily Inspection Form #2 Date:
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PMR Weekly Inspection Form #3 Date:
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damage or vandalism. Other Inspecti
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TABLE OF CONTENTS 1 CONTINGENCY PLA
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Potential Emergency Condition Fire,
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Other duties of the emergency coord
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Determine proper storage and placem
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Neoprene boots - protect feet. Res
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Fire Extinguishers. Absorbent pads
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Table 2: Coordinating Agency Contac
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Stay low in smoke filled areas. Co
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the area or the National Response C
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Description of the spilled material
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APPENDIX 6-B Emergency Coordinators
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Ambulance EXTERNAL CONTACTS Name Ti
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