Precious Metals Recovery LLC RCRA Permit Application Dry Hills ...
Precious Metals Recovery LLC RCRA Permit Application Dry Hills ... Precious Metals Recovery LLC RCRA Permit Application Dry Hills ...
7.2.13.3 If the initial liquid phase of the waste, as obtained from Section 7.2.7, is not or may not be compatible with the filtered liquid resulting from Section 7.2.12, do not combine these liquids. Analyze these liquids, collectively defined as the TCLP extract, and combine the results mathematically, as described in Section 7.2.14. 7.2.14 Following collection of the TCLP extract, the pH of the extract should be recorded. Immediately aliquot and preserve the extract for analysis. Metals aliquots must be acidified with nitric acid to pH
sample from which no additional liquid may be forced out by an applied pressure of 50 psi), due to the need to add an amount of extraction fluid equal to 20 times the weight of the solid phase. Charge the ZHE with sample only once and do not open the device until the final extract (of the solid) has been collected. Repeated filling of the ZHE to obtain 25 grams of solid is not permitted. Do not allow the waste, the initial liquid phase, or the extract to be exposed to the atmosphere for any more time than is absolutely necessary. Any manipulation of these materials should be done when cold (4 EC) to minimize loss of volatiles. 7.3.1 Pre-weigh the (evacuated) filtrate collection container ® (See Section 4.6) and set aside. If using a TEDLAR bag, express all liquid from the ZHE device into the bag, whether for the initial or final liquid/solid separation, and take an aliquot from the liquid in the bag for analysis. The containers listed in Section 4.6 are recommended for use under the conditions stated in Sections 4.6.1 - 4.6.3. 7.3.2 Place the ZHE piston within the body of the ZHE (it may be helpful first to moisten the piston O-rings slightly with extraction fluid). Adjust the piston within the ZHE body to a height that will minimize the distance the piston will have to move once the ZHE is charged with sample (based upon sample size requirements determined from Section 7.3, Section 7.1.1 and/or 7.1.2). Secure the gas inlet/outlet flange (bottom flange) onto the ZHE body in accordance with the manufacturer's instructions. Secure the glass fiber filter between the support screens and set aside. Set liquid inlet/outlet flange (top flange) aside. 7.3.3 If the waste is 100% solid (see Section 7.1.1), weigh out a subsample (25 gram maximum) of the waste, record weight, and proceed to Section 7.3.5. 7.3.4 If the waste contains < 0.5% dry solids (Section 7.1.2), the liquid portion of waste, after filtration, is defined as the TCLP extract. Filter enough of the sample so that the amount of filtered liquid will support all of the volatile analyses required. For wastes containing > 0.5% dry solids (Sections 7.1.1 and/or 7.1.2), use the percent solids information obtained in Section 7.1.1 to determine the optimum sample size to charge into the ZHE. The recommended sample size is as follows: 7.3.4.1 For wastes containing < 5% solids (see Section 7.1.1), weigh out a 500 gram subsample of waste and record the weight. 7.3.4.2 For wastes containing > 5% solids (see Section 7.1.1), determine the amount of waste to charge into the ZHE as follows: CD-ROM 1311- 15 Revision 0 July 1992
- Page 291 and 292: 2. PRODUCTS 2.1 Stonclad GS Stoncla
- Page 293 and 294: APPENDIX 2-A Waste Analysis Plan
- Page 295 and 296: WASTE ANALYSIS PLAN 1 PURPOSE AND S
- Page 297 and 298: Table 1: Analytical Methods for the
- Page 299 and 300: All wastes received will have been
- Page 301 and 302: Waste will not be accepted until th
- Page 303 and 304: Table 3: Waste Sampling Matrix Type
- Page 305 and 306: 9 LDR TREATMENT STANDARDS Waste Des
- Page 307 and 308: Drummed consolidation waste will be
- Page 309 and 310: eevaluated whenever the process tha
- Page 311 and 312: ATTACHMENT 2-A-1 Profile Instructio
- Page 313 and 314: PMR LLC 460 W. 50 North Suite 500 S
- Page 315 and 316: • Is the waste pyrophoric? a See
- Page 317 and 318: EPA's Chemical Compatibility Chart
- Page 319 and 320: 1.0 SCOPE AND APPLICATION METHOD 90
- Page 321 and 322: 7.2.3 Adjust the electrodes in the
- Page 323 and 324: METHOD 9045D SOIL AND WASTE pH 9045
- Page 325 and 326: NOTE: Combination electrodes incorp
- Page 327 and 328: 10.0 REFERENCES 1. National Bureau
- Page 329 and 330: 1.0 SCOPE AND APPLICATION METHOD 13
- Page 331 and 332: 4.2.2 Bottle Extraction Vessel. Whe
- Page 333 and 334: 4.10 Watchglass, appropriate diamet
- Page 335 and 336: 7.0 PROCEDURE 7.1 Preliminary Evalu
- Page 337 and 338: determine whether the solid materia
- Page 339 and 340: solids content of the waste sample
- Page 341: material into an extractor bottle.
- Page 345 and 346: slowly out of the ZHE device into a
- Page 347 and 348: ® TEDLAR bag is used, if the extra
- Page 349 and 350: 150% of the expected concentration
- Page 351 and 352: None of the parameters had a signif
- Page 353 and 354: Table 2. Suitable Rotary Agitation
- Page 355 and 356: Table 4. Suitable Filter Holders 1
- Page 357 and 358: Table 6. Multi-Laboratory TCLP Meta
- Page 359 and 360: Table 8. Multi-Laboratory Semi-Vola
- Page 361 and 362: Figure 1. Rotary Agitation Apparatu
- Page 363 and 364: METHOD 1311 (CONTINUED) TOXICITY CH
- Page 365 and 366: Designation: D4979 − 08 Standard
- Page 367 and 368: Designation: D4978 − 95 (Reapprov
- Page 369 and 370: FIG. 1 Method B, Sulfide Test Appar
- Page 371 and 372: TABLE 1 Determination of Bias, Pycn
- Page 373 and 374: for four known specific gravity lev
- Page 375 and 376: 21.7.1 To check the precision of sa
- Page 377 and 378: Designation: D4981 − 08 Standard
- Page 379 and 380: Designation: D5058 − 12 Standard
- Page 381 and 382: 11.6.1 Compare the temperature here
- Page 383 and 384: APPENDIX 2-E Characterization Data
- Page 385 and 386: 5. Fire-fighting measures General I
- Page 387 and 388: Carcinogenicity: CAS# 10112‐91‐
7.2.13.3 If the initial liquid phase of the waste, as<br />
obtained from Section 7.2.7, is not or may not be compatible with<br />
the filtered liquid resulting from Section 7.2.12, do not combine<br />
these liquids. Analyze these liquids, collectively defined as the<br />
TCLP extract, and combine the results mathematically, as described<br />
in Section 7.2.14.<br />
7.2.14 Following collection of the TCLP extract, the pH of the<br />
extract should be recorded. Immediately aliquot and preserve the extract<br />
for analysis. <strong>Metals</strong> aliquots must be acidified with nitric acid to<br />
pH
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