Precious Metals Recovery LLC RCRA Permit Application Dry Hills ...

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H - 340940 Precious Metals Recovery LLC Dry Hills Facility Project Stream Tables for RCRA Application Rev. C December 11, 2012 Flowsheet 1400-05-030-0003 Note 1 Note 2 Note 1 Stream Number 56 108 509 201 202 204 Stream Name Caustic Soda from Storage Tank Process Water Retort Off-gas Retort Off-gas to Scrubber Bypass Scrubber Outlet Gas Waste Solution from Scrubber Annual Throughput lb/yr 144,320 -- TBD -- -- 217,000 Slurry lb/yr 0 0 0 % Solids wt% -- -- -- Solids lb/yr 0 0 0 0 0 0 Hg2Cl2 wt% -- -- -- -- -- -- HgO wt% -- -- -- -- -- -- HgS wt% -- -- -- -- -- -- S wt% -- -- -- -- -- -- Solution lb/yr 144,320 0 TBD 0 0 217,000 Hg 2+ g/L 0.0 -- 0.0 -- -- 0.0 NaOH g/L 766.2 -- 0.0 -- -- TBD HCl g/L 0.0 -- 0.0 -- -- 0.0 Cl - g/L 0.0 -- 0.0 -- -- 0.0 pH 13.7 -- 7.0 -- -- TBD Elemental Mercury lb/yr 0 0 0 0 0 0 Gas (Annual Average) scfm 0 300 0 300 300 0 N2 vol% -- 75.1% -- 75.1% 75.8% -- O 2 vol% -- 23.1% -- 23.5% 22.8% -- Hg (v) vol% -- 0.0% -- 0.0% 0.0% -- H 2O (v) vol% -- 1.4% -- 1.4% 1.4% -- SO2 Notes: vol% -- 0.4% -- 0.0% 0.0% -- 1 - To be confirmed once vendor data is available. 2 - To be confirmed once vendor data is available. Assume 99% removal of SO 2 on an annual basis.
H - 340940 Precious Metals Recovery LLC Dry Hills Facility Project Stream Tables for RCRA Application Rev. C December 11, 2012 Flowsheet 1400-05-030-0004 Note 1 Note 1 Note 1 Note 2 Note 1 Note 1 Note 1 Notes 3, 4 Note 2 Note 1 Note 5 Note 5 Note 5 Note 2 Stream Number 109 159 204 251 252 253 254 257 258 259 260 360 361 362 455 Stream Name Waste Solution from Retort Caustic Leach Waste Solution Waste Solution from Oxidation Reactor Waste Solution from Laboratory Waste Water from Open Sumps Combined Waste Solution To Collection Tank Decanted Waste Solution from Settling Tank Waste Solution to Waste Solution Treatment Tank Tank Off-gas - Waste Solution Treatment Mercury Precipitate Treated Waste Solution from Activated Carbon Columns Compressed Air to Waste Solution Collection Pump Compressed Air to Decanted Waste Solution Pump Compressed Air to Waste Solution Settling Tank U/F Pump Annual Throughput lb/yr 8,000 734,195 217,000 TBD 3,831 229,000 734,000 229,000 -- TBD 734,000 TBD TBD TBD TBD Slurry lb/yr 0 734,195 0 TBD 0 0 0 TBD % Solids wt% -- 0.0% -- 30.0% -- -- -- TBD Solids lb/yr 0 195 0 0 0 0 0 0 0 TBD 0 0 0 0 TBD Hg 2Cl 2 wt% -- 0.0% -- -- -- -- -- -- -- TBD -- -- -- -- TBD HgO wt% -- 0.0% -- -- -- -- -- -- -- TBD -- -- -- -- TBD HgS wt% -- 0.0% -- -- -- -- -- -- -- TBD -- -- -- -- TBD S wt% -- 0.0% -- -- -- -- -- -- -- TBD -- -- -- -- TBD Solution lb/yr 8,000 734,000 217,000 TBD 3,831 229,000 734,000 229,000 0 TBD 734,000 0 0 0 TBD Hg 2+ g/L TBD TBD 0.0 TBD 0.0 TBD TBD TBD -- TBD 0.001 -- -- -- TBD NaOH g/L TBD TBD TBD TBD 0.0 TBD TBD TBD -- TBD TBD -- -- -- TBD HCl g/L TBD TBD 0.0 TBD 0.0 TBD TBD TBD -- TBD TBD -- -- -- TBD Cl - g/L TBD TBD 0.0 TBD 0.0 TBD TBD TBD -- TBD TBD -- -- -- TBD pH TBD TBD TBD TBD 7.0 TBD TBD TBD -- 7.0 TBD -- -- -- TBD Elemental Mercury lb/yr 0 0 0 0 0 0 0 0 0 TBD 0 0 0 0 TBD Gas (Annual Average) scfm 0 0 0 0 0 0 0 0 20 0 0 TBD TBD TBD 0 N2 vol% -- -- -- -- -- -- -- -- 78.1% -- -- 78.0% 78.0% 78.0% -- O 2 vol% -- -- -- -- -- -- -- -- 20.8% -- -- 21.0% 21.0% 21.0% -- Hg (v) vol% -- -- -- -- -- -- -- -- 0.0% -- -- 0.0% 0.0% 0.0% -- H 2O (v) vol% -- -- -- -- -- -- -- -- 1.2% -- -- 0.0% 0.0% 0.0% -- SO2 Notes: vol% -- -- -- -- -- -- -- -- 0.0% -- -- 0.0% 0.0% 0.0% -- 1 - Stream properties to be determined once vendor process data from retort and SO2 scrubber suppliers becomes available. 2 - To be determined in detailed engineering. 3 - Assume mercury level to be at 0.1 mg/Nm 3 (OSHA level) for design purposes. 4 - Assume tank ventilation gas to have a relative humidity of 50% 5 - Compressed air requirements for equipment to be determined in detailed engineering when vendor data becomes available. Off-Spec Treated Waste Solution - Waste Solution Settling Tank
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Precious Metals Recovery LLC RCRA P
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ITEM # REGULATIONS GENERAL DESCRIPT
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PMR Nevada RCRA Permit Application
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PMR Nevada RCRA Permit Application
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M-3 M-3 ITEM # REGULATIONS GENERAL
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OMB# 2050-0024; Expires ___________
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EPA ID Number OMB#: 2050-0024; Expi
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EPA ID Number ADDENDUM TO THE SITE
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This document is for reference purp
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A B C D E F $$W ATERMARKD$$ N 4,475
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Precious Metals Recovery LLC Dry Hi
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3.2 Barrier and Means to Control En
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19.0 APPROVAL OF PETITION FOR EXTEN
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LIST OF TABLES Table 1.2-1 Secondar
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Figure 23.1-1 Decomposition & Waste
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Section 10 Appendices 10-A Figures
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HVAC Heating, Ventilation, and Air
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GLOSSARY OF SELECTED TERMS [Authori
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INTRODUCTION Precious Metals Recove
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Pre-application Public Meeting - 40
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(Purity ≥ 99.5%, Directly Stored)
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Administration (MSHA) document, Con
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Fire Doors/Emergency Exit Doors Pr
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When leaving the plant spaces, work
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Infiltration Air Office Area Pig Pi
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personnel will be trained in respon
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Figure 1.2-1: Elemental Mercury Tra
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Tanks Or Containers Carbon Drums (n
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Figure 1.2-2: Calomel Feed Preparat
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Figure 1.2-3: Filter Press and Loca
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Activated carbon is used in the air
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Figure 1.2-5: SO2 Scrubber and Loca
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Above the retort tray/drum transfer
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Figure 1.2-8: Carbon Filter and Loc
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Figure 1.2-10: Overall Ventilation
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Wash water from open sumps. Safety
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1.3 Elemental Mercury Storage - 40
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The following items are located out
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Control System Architecture The pla
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will be supplied in accordance with
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Outdoor Material Storage A list of
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It is recognized that the fire prot
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Outdoor Areas Hydrants and hose bo
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the event of a security violation,
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2.3 Determination of Treatment Para
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Table 2.5-2: Test Methods Parameter
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Sampling Containerized Waste The te
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Process Waste Solution A discrete p
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ii. The sampling person removes a s
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2.9 Screening for Ignitable, Reacti
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3.0 SECURITY PLAN - 40 CFR 270.14(b
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4.0 INSPECTION PLAN - 40 CFR 270.14
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TSF, associated hazards, places whe
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Outside of working hours, a notific
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Damaged containers will be placed i
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7.0 PREVENTION AND SAFETY PROCEDURE
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8.0 PREVENTION OF ACCIDENTAL IGNITI
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10.0 TRAFFIC - 40 CFR 270.14(b)(10)
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Delivery frequency of reagents will
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10.3 Traffic Control Signs Traffic
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11.4 Surrounding Land Use - 40 CFR
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12.0 PERSONNEL TRAINING PLAN - 40 C
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that are not land based. Closure of
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13.4.6 Types of Off-site Waste Mana
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14.0 CLOSED HAZARDOUS WASTE DISPOSA
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storage area (e.g., storage racks),
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16.0 POST-CLOSURE ESTIMATES - 40 CF
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18.0 TOPOGRAPHICAL MAP - 40 CFR 270
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20.0 GROUNDWATER MONITORING - 40 CF
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22.0 CONTAINERS AND CONTAINMENT - 4
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Figure 22.1-2: Dedicated Transfer C
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Larger sized HDPE drums may be used
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22.3.2 Labeling Containers - 40 CFR
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22.5 Description of Secondary Conta
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will be done on the new waste strea
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23.0 TREATMENT AND STORAGE TANKS Me
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Figure 23.0-2: HCl Tank and Locatio
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Tank Dimensions Waste Solution Stor
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decomposed in the Decomposition Tan
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Figure 23.1-3: Waste Solution Stora
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The Water Storage Tank will supply
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Tank Caustic Soda Storage Tank* Hyd
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23.13 Recordkeeping A recordkeeping
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25.0 WASTE PILES - 40 CFR 270.18 &
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27.0 LAND TREATMENT - 40 CFR 270.20
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29.0 BOILERS/INDUSTRIAL FURNACE - 4
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30.1.3 Retort Operating Procedures
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of 13.5 feet long by 4.7 feet wide
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31.0 PROCESS VENTS - 40 CFR 270.24
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33.0 DRIP PADS - 40 CFR 270.26 & 26
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35.0 REFERENCES American Society of
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At the PMR Dry Hills Facility Open
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APPENDIX I-B Open House Comments
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APPENDIX 1-A Drawings Facility draw
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A B C D EF $ $ W A TERMARKA1$$ H340
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A B C D E F $$W ATERMARKD$$ 1 2 3 4
Page 225 and 226: A B C D E F $$W ATERMARKD$$ N 4,475
Page 227 and 228: A B C D E F $$W ATERMARKD$$ 1 2 3 4
Page 235 and 236: A B C D EF $ $ W A TERMARKA1$$ H340
Page 237 and 238: A B C D E F $$W ATERMARKD$$ H340940
Page 249 and 250: A B C D E F $$W ATERMARKD$$ NOTE: 1
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Page 259 and 260: APPENDIX 1-C Process Flow Diagrams
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Page 283 and 284: APPENDIX 1-D Floor and Wall Sealant
Page 285 and 286: C8 x 11.5 EPOXY COATING ON 2" THICK
Page 287 and 288: 8" THICK INSULATED PRECAST CONCRETE
Page 289 and 290: C8 x 11.5 EPOXY COATING ON 2" THICK
Page 291 and 292: 2. PRODUCTS 2.1 Stonclad GS Stoncla
Page 293 and 294: APPENDIX 2-A Waste Analysis Plan
Page 295 and 296: WASTE ANALYSIS PLAN 1 PURPOSE AND S
Page 297 and 298: Table 1: Analytical Methods for the
Page 299 and 300: All wastes received will have been
Page 301 and 302: Waste will not be accepted until th
Page 303 and 304: Table 3: Waste Sampling Matrix Type
Page 305 and 306: 9 LDR TREATMENT STANDARDS Waste Des
Page 307 and 308: Drummed consolidation waste will be
Page 309 and 310: eevaluated whenever the process tha
Page 311 and 312: ATTACHMENT 2-A-1 Profile Instructio
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Page 315 and 316: • Is the waste pyrophoric? a See
Page 317 and 318: EPA's Chemical Compatibility Chart
Page 319 and 320: 1.0 SCOPE AND APPLICATION METHOD 90
Page 321 and 322: 7.2.3 Adjust the electrodes in the
Page 323 and 324: METHOD 9045D SOIL AND WASTE pH 9045
Page 325 and 326: NOTE: Combination electrodes incorp
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10.0 REFERENCES 1. National Bureau
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1.0 SCOPE AND APPLICATION METHOD 13
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4.2.2 Bottle Extraction Vessel. Whe
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4.10 Watchglass, appropriate diamet
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7.0 PROCEDURE 7.1 Preliminary Evalu
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determine whether the solid materia
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solids content of the waste sample
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material into an extractor bottle.
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sample from which no additional liq
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slowly out of the ZHE device into a
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® TEDLAR bag is used, if the extra
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150% of the expected concentration
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None of the parameters had a signif
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Table 2. Suitable Rotary Agitation
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Table 4. Suitable Filter Holders 1
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Table 6. Multi-Laboratory TCLP Meta
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Table 8. Multi-Laboratory Semi-Vola
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Figure 1. Rotary Agitation Apparatu
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METHOD 1311 (CONTINUED) TOXICITY CH
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Designation: D4979 − 08 Standard
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Designation: D4978 − 95 (Reapprov
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FIG. 1 Method B, Sulfide Test Appar
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TABLE 1 Determination of Bias, Pycn
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for four known specific gravity lev
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21.7.1 To check the precision of sa
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11.6.1 Compare the temperature here
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APPENDIX 2-E Characterization Data
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5. Fire-fighting measures General I
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Carcinogenicity: CAS# 10112‐91‐
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Combined Hazen Solution Analysis pH
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irritation and possible burns. May
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OSHA Vacated PELs: Mercury: 0.05 mg
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Chemical waste generators must dete
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APPENDIX 4-A Inspection Plan
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1 INSPECTION PLAN This Inspection P
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Inspections are intended to detect
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Boilers and Industrial Furnaces Ins
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PMR Daily Inspection Form #1 Date:
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PMR Daily Inspection Form #2 Date:
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PMR Weekly Inspection Form #3 Date:
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damage or vandalism. Other Inspecti
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TABLE OF CONTENTS 1 CONTINGENCY PLA
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Potential Emergency Condition Fire,
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Other duties of the emergency coord
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Determine proper storage and placem
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Neoprene boots - protect feet. Res
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Fire Extinguishers. Absorbent pads
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Table 2: Coordinating Agency Contac
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Stay low in smoke filled areas. Co
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the area or the National Response C
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Description of the spilled material
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APPENDIX 6-B Emergency Coordinators
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Ambulance EXTERNAL CONTACTS Name Ti
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