Precious Metals Recovery LLC RCRA Permit Application Dry Hills ...
Precious Metals Recovery LLC RCRA Permit Application Dry Hills ... Precious Metals Recovery LLC RCRA Permit Application Dry Hills ...
Table 2.6-1: Sampling and Analytical Methods Parameter Sampling Type Analytical Method Container Weight N/A Scale Physical Description N/A Visual observation in container Specific Gravity Composite ASTM Method 5057 Free Liquids Grab SW-846 Method 9095 pH (corrosivity determination) Grab or Composite SW-846 Method 9040 (liquids) SW-846 Method 9045 (nonliquids) Mercury TCLP Grab or Composite SW-846 Method 7470 or 7471 Mercury (Total) Grab Residue Metals (Total) SW-846 Method 7473 SW-846 Method 6200 (XRF) PMR RCRA Permit Application, Dry Hills Facility Page 56 JBR Environmental Consultants, Inc. | HATCH March 2013 Grab SW-846 Method 1311/6010/7060/7061 Metals (Total) Grab Method 6200 (XRF) Leachable Metals Grab SW-846 Method 6010 Zinc Grab SW-846 Method 6010 Organics (Total) Grab SW-846 Method 8260 (volatiles) SW-846 Method 8270 (semivolatiles) Moisture Content Grab EPA Method 600/4-79-020 Ash Composite ASTM Method D482-87 Ignitability Composite ASTM D93-11 Water Reactivity Grab SW-846 Method 1110A Cyanide Reactivity Grab EPA Method 600/4-79-020 #335.2 Sulfides Grab SW-846 Method 9031
Sampling Containerized Waste The term “container” refers to receptacles designed for transporting materials (e.g., drums, flasks, and pigs). Sampling devices include Composite Liquid Waste Samplers (COLIWASAs), tubes, trowel, drum thieves, and tube samplers. Sampling of Tanks A representative sample of the waste will be collected from the side or bottom of each tank. Samples will be collected such that various depths in the tank will be evaluated if the material phase separates or contains multiple batches. Multiple grab samples may be composited to obtain a weighted representation of the tank contents. Sampling SOPs for each process tank will be developed and reviewed by the laboratory staff when necessary. Frozen Waste The proposed TSF will not sample waste that is frozen. The waste will be held in the truck unloading area until the waste can be sampled. A sample will then be collected as outlined in this section. 2.7 Waste Characterization & Frequency of Analysis – 40 CFR 270.14(b)(2) & 264.13(b)(4) Waste characterization data can be found in Appendix 2-E. 2.7.1 Routine Wastes Process Wastes The processes at the proposed TSF will generate a number of routine waste streams. These waste streams will be evaluated initially at the beginning of operations and annually updated to verify accuracy. The waste characterization will also be re-evaluated whenever the process that generated the waste changes or there is an unresolved discrepancy on a shipment. Elemental Mercury The chemical composition of the recovered elemental mercury is well known and consistent. As discussed above, the proposed TSF will use waste generator knowledge to characterize this material. Elemental mercury purity will be evaluated based on weight. While these waste streams will not be routinely analyzed prior to being stored, the proposed TSF will review all waste streams on an annual basis or any time the waste generating process changes. Calomel The chemical composition of the calomel is well known and is within the process design range. As discussed above, the proposed TSF will use waste generator knowledge to characterize this material. While this waste stream will not be routinely analyzed prior to being treated, the proposed TSF will review all waste streams on an annual basis or any time the waste generating process changes. PMR RCRA Permit Application, Dry Hills Facility Page 57 JBR Environmental Consultants, Inc. | HATCH March 2013
- Page 57 and 58: (Purity ≥ 99.5%, Directly Stored)
- Page 59 and 60: Administration (MSHA) document, Con
- Page 61 and 62: Fire Doors/Emergency Exit Doors Pr
- Page 63 and 64: When leaving the plant spaces, work
- Page 65 and 66: Infiltration Air Office Area Pig Pi
- Page 67 and 68: personnel will be trained in respon
- Page 69 and 70: Figure 1.2-1: Elemental Mercury Tra
- Page 71 and 72: Tanks Or Containers Carbon Drums (n
- Page 73 and 74: Figure 1.2-2: Calomel Feed Preparat
- Page 75 and 76: Figure 1.2-3: Filter Press and Loca
- Page 77 and 78: Activated carbon is used in the air
- Page 79 and 80: Figure 1.2-5: SO2 Scrubber and Loca
- Page 81 and 82: Above the retort tray/drum transfer
- Page 83 and 84: Figure 1.2-8: Carbon Filter and Loc
- Page 85 and 86: Figure 1.2-10: Overall Ventilation
- Page 87 and 88: Wash water from open sumps. Safety
- Page 89 and 90: 1.3 Elemental Mercury Storage - 40
- Page 91 and 92: The following items are located out
- Page 93 and 94: Control System Architecture The pla
- Page 95 and 96: will be supplied in accordance with
- Page 97 and 98: Outdoor Material Storage A list of
- Page 99 and 100: It is recognized that the fire prot
- Page 101 and 102: Outdoor Areas Hydrants and hose bo
- Page 103 and 104: the event of a security violation,
- Page 105 and 106: 2.3 Determination of Treatment Para
- Page 107: Table 2.5-2: Test Methods Parameter
- Page 111 and 112: Process Waste Solution A discrete p
- Page 113 and 114: ii. The sampling person removes a s
- Page 115 and 116: 2.9 Screening for Ignitable, Reacti
- Page 117 and 118: 3.0 SECURITY PLAN - 40 CFR 270.14(b
- Page 119 and 120: 4.0 INSPECTION PLAN - 40 CFR 270.14
- Page 121 and 122: TSF, associated hazards, places whe
- Page 123 and 124: Outside of working hours, a notific
- Page 125 and 126: Damaged containers will be placed i
- Page 127 and 128: 7.0 PREVENTION AND SAFETY PROCEDURE
- Page 129 and 130: 8.0 PREVENTION OF ACCIDENTAL IGNITI
- Page 131 and 132: 10.0 TRAFFIC - 40 CFR 270.14(b)(10)
- Page 133 and 134: Delivery frequency of reagents will
- Page 135 and 136: 10.3 Traffic Control Signs Traffic
- Page 137 and 138: 11.4 Surrounding Land Use - 40 CFR
- Page 139 and 140: 12.0 PERSONNEL TRAINING PLAN - 40 C
- Page 141 and 142: that are not land based. Closure of
- Page 143 and 144: 13.4.6 Types of Off-site Waste Mana
- Page 145 and 146: 14.0 CLOSED HAZARDOUS WASTE DISPOSA
- Page 147 and 148: storage area (e.g., storage racks),
- Page 149 and 150: 16.0 POST-CLOSURE ESTIMATES - 40 CF
- Page 151 and 152: 18.0 TOPOGRAPHICAL MAP - 40 CFR 270
- Page 153 and 154: 20.0 GROUNDWATER MONITORING - 40 CF
- Page 155 and 156: 22.0 CONTAINERS AND CONTAINMENT - 4
- Page 157 and 158: Figure 22.1-2: Dedicated Transfer C
Table 2.6-1: Sampling and Analytical Methods<br />
Parameter Sampling Type Analytical Method<br />
Container Weight N/A Scale<br />
Physical Description N/A Visual observation in container<br />
Specific Gravity Composite ASTM Method 5057<br />
Free Liquids Grab SW-846 Method 9095<br />
pH (corrosivity determination) Grab or Composite<br />
SW-846 Method 9040 (liquids)<br />
SW-846 Method 9045 (nonliquids)<br />
Mercury TCLP Grab or Composite SW-846 Method 7470 or 7471<br />
Mercury (Total) Grab<br />
Residue <strong>Metals</strong> (Total)<br />
SW-846 Method 7473<br />
SW-846 Method 6200 (XRF)<br />
PMR <strong>RCRA</strong> <strong>Permit</strong> <strong>Application</strong>, <strong>Dry</strong> <strong>Hills</strong> Facility Page 56<br />
JBR Environmental Consultants, Inc. | HATCH March 2013<br />
Grab<br />
SW-846 Method<br />
1311/6010/7060/7061<br />
<strong>Metals</strong> (Total) Grab Method 6200 (XRF)<br />
Leachable <strong>Metals</strong> Grab SW-846 Method 6010<br />
Zinc Grab SW-846 Method 6010<br />
Organics (Total) Grab<br />
SW-846 Method 8260 (volatiles)<br />
SW-846 Method 8270 (semivolatiles)<br />
Moisture Content Grab EPA Method 600/4-79-020<br />
Ash Composite ASTM Method D482-87<br />
Ignitability Composite ASTM D93-11<br />
Water Reactivity Grab SW-846 Method 1110A<br />
Cyanide Reactivity Grab EPA Method 600/4-79-020 #335.2<br />
Sulfides Grab SW-846 Method 9031
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