Precious Metals Recovery LLC RCRA Permit Application Dry Hills ...

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2.0 WASTE CHARACTERISTICS The principal waste management activity at the proposed TSF will be processing mercurybearing wastes generated from Barrick mines and associated joint venture operations in the United States for the recovery and storage of elemental mercury. Mercury stored as a hazardous waste at the proposed TSF will be stored until it can be transferred to a National Repository for long-term storage and management. 2.1 Purpose – 40 CFR 270.14(b)(3) The purpose of this waste characterization plan is to specify the proper handling procedures, and effective treatment methodologies to be implemented at the proposed TSF. Adequate waste characterization processes will ensure appropriate information is available to manage mercury and mercury-bearing materials safely, and in accordance with the regulatory requirements. 2.2 Waste Analysis Plan – 40 CFR 270.14(b)(3) The Waste Analysis Plan (WAP) (see Appendix 2-A), presents the complete details of how waste will be characterized for treatment and storage. The WAP addresses wastes that will be received and generated by the proposed TSF. The WAP establishes the following items for inclusion in this application: Procedures for determining if a waste stream will be acceptable for management at the proposed TSF. Procedures for notifying the waste generator that the waste will be accepted. Procedures for characterizing wastes. Appropriate management strategies. Frequency of sampling and analyzing incoming loads of waste. Methods for sampling and analyzing incoming loads of waste. Analytical parameters for each waste. Rationale for the selection of analytical parameters. The WAP will be supported by SW-846 Methods, American Society for Testing and Materials (ASTM) Methods, and Standard Operating Procedures (SOPs) for the on-site laboratory. The proposed TSF’s laboratory personnel will use these supporting documents as detailed instructions for performing the necessary procedures. The incorporated SOPs may be updated as appropriate without modifying the WAP. PMR RCRA Permit Application, Dry Hills Facility Page 52 JBR Environmental Consultants, Inc. | HATCH March 2013
2.3 Determination of Treatment Parameters – 40 CFR 264.13(b)(1) & 270.14(b)(3) The proposed TSF may generate two general categories of non-liquid waste that, in accordance with 40 CFR 261, could be considered hazardous waste: Mercury-bearing waste that may be characteristic for the presence of mercury and other metals at concentrations above the established regulatory limit. Secondary materials that may be characteristic for mercury and/or other properties. 2.3.1 Characteristic Waste Mercury-bearing materials with leached mercury concentrations above the 0.2 milligrams per liter (mg/L) limit are characteristically hazardous for mercury toxicity per 40 CFR 261.24 Table 1. Analytical results, typically using the TCLP method, will be used to assess the toxicity of the generated waste stream (e.g., filter cake) and to determine the applicable waste code(s). As an alternative to the TCLP method, other approved analytical methods may be used to make this determination. Wastes that are less than 0.2 mg/L are not characteristic for mercury and will not carry a D009 waste code. Other potential waste codes may include D002 (corrosivity), D004 (arsenic), D007 (chromium), D008 (lead), D010 (selenium), and D011 (silver). 2.3.2 Hazardous Secondary Material Hazardous secondary material (e.g., spent material, byproduct, and sludge) include materials, that when discarded, would be identified as hazardous waste. The proposed TSF has process knowledge for all of its secondary material waste streams. An annual evaluation will be performed to verify chemical composition and concentration ranges. All new or modified secondary material waste streams will be initially assessed at the point of generation and annually thereafter to maintain proper characterization of all waste streams. 2.4 Rationale for Parameter Selection – 40 CFR 264.13(b)(1) & 270.14(b)(3) Analytical parameters have been specifically selected to identify the nature of the waste, the LDR status of the wastes generated at the proposed TSF, and the organic concentration of those wastes. Materials may enter the proposed TSF as wastes characteristically hazardous for mercury content, but after completing the treatment process the material may no longer demonstrate a characteristic for mercury. These materials will be analyzed for mercury as well as underlying hazardous constituents (UHCs) to determine the RCRA and LDR status of the materials. Table 2.4-1 presents the waste streams that are expected to be generated by the proposed TSF, the proposed analytical parameters, the proposed analytical methods, and the rationale for selection. PMR RCRA Permit Application, Dry Hills Facility Page 53 JBR Environmental Consultants, Inc. | HATCH March 2013
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Precious Metals Recovery LLC RCRA P
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ITEM # REGULATIONS GENERAL DESCRIPT
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PMR Nevada RCRA Permit Application
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PMR Nevada RCRA Permit Application
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M-3 M-3 ITEM # REGULATIONS GENERAL
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OMB# 2050-0024; Expires ___________
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EPA ID Number OMB#: 2050-0024; Expi
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EPA ID Number ADDENDUM TO THE SITE
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This document is for reference purp
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A B C D E F $$W ATERMARKD$$ N 4,475
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Precious Metals Recovery LLC Dry Hi
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3.2 Barrier and Means to Control En
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19.0 APPROVAL OF PETITION FOR EXTEN
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LIST OF TABLES Table 1.2-1 Secondar
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Figure 23.1-1 Decomposition & Waste
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Section 10 Appendices 10-A Figures
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HVAC Heating, Ventilation, and Air
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GLOSSARY OF SELECTED TERMS [Authori
Page 53 and 54: INTRODUCTION Precious Metals Recove
Page 55 and 56: Pre-application Public Meeting - 40
Page 57 and 58: (Purity ≥ 99.5%, Directly Stored)
Page 59 and 60: Administration (MSHA) document, Con
Page 61 and 62: Fire Doors/Emergency Exit Doors Pr
Page 63 and 64: When leaving the plant spaces, work
Page 65 and 66: Infiltration Air Office Area Pig Pi
Page 67 and 68: personnel will be trained in respon
Page 69 and 70: Figure 1.2-1: Elemental Mercury Tra
Page 71 and 72: Tanks Or Containers Carbon Drums (n
Page 73 and 74: Figure 1.2-2: Calomel Feed Preparat
Page 75 and 76: Figure 1.2-3: Filter Press and Loca
Page 77 and 78: Activated carbon is used in the air
Page 79 and 80: Figure 1.2-5: SO2 Scrubber and Loca
Page 81 and 82: Above the retort tray/drum transfer
Page 83 and 84: Figure 1.2-8: Carbon Filter and Loc
Page 85 and 86: Figure 1.2-10: Overall Ventilation
Page 87 and 88: Wash water from open sumps. Safety
Page 89 and 90: 1.3 Elemental Mercury Storage - 40
Page 91 and 92: The following items are located out
Page 93 and 94: Control System Architecture The pla
Page 95 and 96: will be supplied in accordance with
Page 97 and 98: Outdoor Material Storage A list of
Page 99 and 100: It is recognized that the fire prot
Page 101 and 102: Outdoor Areas Hydrants and hose bo
Page 103: the event of a security violation,
Page 107 and 108: Table 2.5-2: Test Methods Parameter
Page 109 and 110: Sampling Containerized Waste The te
Page 111 and 112: Process Waste Solution A discrete p
Page 113 and 114: ii. The sampling person removes a s
Page 115 and 116: 2.9 Screening for Ignitable, Reacti
Page 117 and 118: 3.0 SECURITY PLAN - 40 CFR 270.14(b
Page 119 and 120: 4.0 INSPECTION PLAN - 40 CFR 270.14
Page 121 and 122: TSF, associated hazards, places whe
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Page 125 and 126: Damaged containers will be placed i
Page 127 and 128: 7.0 PREVENTION AND SAFETY PROCEDURE
Page 129 and 130: 8.0 PREVENTION OF ACCIDENTAL IGNITI
Page 131 and 132: 10.0 TRAFFIC - 40 CFR 270.14(b)(10)
Page 133 and 134: Delivery frequency of reagents will
Page 135 and 136: 10.3 Traffic Control Signs Traffic
Page 137 and 138: 11.4 Surrounding Land Use - 40 CFR
Page 139 and 140: 12.0 PERSONNEL TRAINING PLAN - 40 C
Page 141 and 142: that are not land based. Closure of
Page 143 and 144: 13.4.6 Types of Off-site Waste Mana
Page 145 and 146: 14.0 CLOSED HAZARDOUS WASTE DISPOSA
Page 147 and 148: storage area (e.g., storage racks),
Page 149 and 150: 16.0 POST-CLOSURE ESTIMATES - 40 CF
Page 151 and 152: 18.0 TOPOGRAPHICAL MAP - 40 CFR 270
Page 153 and 154: 20.0 GROUNDWATER MONITORING - 40 CF
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22.0 CONTAINERS AND CONTAINMENT - 4
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Figure 22.1-2: Dedicated Transfer C
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Larger sized HDPE drums may be used
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22.3.2 Labeling Containers - 40 CFR
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22.5 Description of Secondary Conta
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will be done on the new waste strea
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23.0 TREATMENT AND STORAGE TANKS Me
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Figure 23.0-2: HCl Tank and Locatio
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Tank Dimensions Waste Solution Stor
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decomposed in the Decomposition Tan
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Figure 23.1-3: Waste Solution Stora
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The Water Storage Tank will supply
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Tank Caustic Soda Storage Tank* Hyd
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23.13 Recordkeeping A recordkeeping
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25.0 WASTE PILES - 40 CFR 270.18 &
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27.0 LAND TREATMENT - 40 CFR 270.20
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29.0 BOILERS/INDUSTRIAL FURNACE - 4
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30.1.3 Retort Operating Procedures
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of 13.5 feet long by 4.7 feet wide
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31.0 PROCESS VENTS - 40 CFR 270.24
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33.0 DRIP PADS - 40 CFR 270.26 & 26
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35.0 REFERENCES American Society of
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At the PMR Dry Hills Facility Open
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APPENDIX I-B Open House Comments
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APPENDIX 1-A Drawings Facility draw
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A B C D EF $ $ W A TERMARKA1$$ H340
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A B C D E F $$W ATERMARKD$$ 1 2 3 4
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A B C D E F $$W ATERMARKD$$ N 4,475
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A B C D EF $ $ W A TERMARKA1$$ H340
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A B C D E F $$W ATERMARKD$$ H340940
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A B C D E F $$W ATERMARKD$$ NOTE: 1
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B A B C D E F $$W ATERMARKD$$ H3409
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APPENDIX 1-C Process Flow Diagrams
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H - 340940 Precious Metals Recovery
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APPENDIX 1-D Floor and Wall Sealant
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C8 x 11.5 EPOXY COATING ON 2" THICK
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8" THICK INSULATED PRECAST CONCRETE
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C8 x 11.5 EPOXY COATING ON 2" THICK
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2. PRODUCTS 2.1 Stonclad GS Stoncla
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APPENDIX 2-A Waste Analysis Plan
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WASTE ANALYSIS PLAN 1 PURPOSE AND S
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Table 1: Analytical Methods for the
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All wastes received will have been
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Waste will not be accepted until th
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Table 3: Waste Sampling Matrix Type
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9 LDR TREATMENT STANDARDS Waste Des
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Drummed consolidation waste will be
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eevaluated whenever the process tha
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ATTACHMENT 2-A-1 Profile Instructio
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PMR LLC 460 W. 50 North Suite 500 S
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• Is the waste pyrophoric? a See
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EPA's Chemical Compatibility Chart
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1.0 SCOPE AND APPLICATION METHOD 90
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7.2.3 Adjust the electrodes in the
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METHOD 9045D SOIL AND WASTE pH 9045
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NOTE: Combination electrodes incorp
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10.0 REFERENCES 1. National Bureau
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1.0 SCOPE AND APPLICATION METHOD 13
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4.2.2 Bottle Extraction Vessel. Whe
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4.10 Watchglass, appropriate diamet
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7.0 PROCEDURE 7.1 Preliminary Evalu
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determine whether the solid materia
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solids content of the waste sample
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material into an extractor bottle.
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sample from which no additional liq
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slowly out of the ZHE device into a
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® TEDLAR bag is used, if the extra
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150% of the expected concentration
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None of the parameters had a signif
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Table 2. Suitable Rotary Agitation
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Table 4. Suitable Filter Holders 1
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Table 6. Multi-Laboratory TCLP Meta
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Table 8. Multi-Laboratory Semi-Vola
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Figure 1. Rotary Agitation Apparatu
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METHOD 1311 (CONTINUED) TOXICITY CH
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Designation: D4979 − 08 Standard
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Designation: D4978 − 95 (Reapprov
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FIG. 1 Method B, Sulfide Test Appar
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TABLE 1 Determination of Bias, Pycn
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for four known specific gravity lev
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21.7.1 To check the precision of sa
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11.6.1 Compare the temperature here
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APPENDIX 2-E Characterization Data
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5. Fire-fighting measures General I
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Carcinogenicity: CAS# 10112‐91‐
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Combined Hazen Solution Analysis pH
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irritation and possible burns. May
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OSHA Vacated PELs: Mercury: 0.05 mg
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Chemical waste generators must dete
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APPENDIX 4-A Inspection Plan
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1 INSPECTION PLAN This Inspection P
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Inspections are intended to detect
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Boilers and Industrial Furnaces Ins
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PMR Daily Inspection Form #1 Date:
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PMR Daily Inspection Form #2 Date:
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PMR Weekly Inspection Form #3 Date:
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damage or vandalism. Other Inspecti
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TABLE OF CONTENTS 1 CONTINGENCY PLA
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Potential Emergency Condition Fire,
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Other duties of the emergency coord
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Determine proper storage and placem
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Neoprene boots - protect feet. Res
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Fire Extinguishers. Absorbent pads
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Table 2: Coordinating Agency Contac
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Stay low in smoke filled areas. Co
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the area or the National Response C
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Description of the spilled material
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APPENDIX 6-B Emergency Coordinators
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Ambulance EXTERNAL CONTACTS Name Ti
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